Catalytic distillation: dynamic modelling, simulation, and experimental validation
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Düsseldorf
VDI-Verl.
2003
|
| Ausgabe: | Als Ms. gedr. |
| Schriftenreihe: | Fortschritt-Berichte VDI
Reihe 3, Verfahrenstechnik ; 784 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XII, 133 S. graph. Darst. |
| ISBN: | 3183784033 |
Internformat
MARC
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| 100 | 1 | |a Noeres, Christoph |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Catalytic distillation |b dynamic modelling, simulation, and experimental validation |c Christoph Noeres |
| 250 | |a Als Ms. gedr. | ||
| 264 | 1 | |a Düsseldorf |b VDI-Verl. |c 2003 | |
| 300 | |a XII, 133 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik |v 784 | |
| 502 | |a Zugl.: Dortmund, Univ., Diss., 2002 | ||
| 650 | 4 | |a Reaktivdestillation - Katalyse | |
| 650 | 0 | 7 | |a Katalyse |0 (DE-588)4029921-1 |2 gnd |9 rswk-swf |
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Datensatz im Suchindex
| _version_ | 1808135277418381312 |
|---|---|
| adam_text |
CONTENTS
V
CONTENTS
CONTENTS
V
NOTATION
VII
1
INTRODUCTION
AND
OBJECTIVES
1
2
STATE
OF
THE
ART
4
2.1
REACTIVE
SEPARATION
PROCESSES
4
2.2
INTERNALS
FOR
CATALYTIC
DISTILLATION
10
2.3
MODELLING
OF
REACTIVE
DISTILLATION
14
2.3.1
EQUILIBRIUM
STAGE
MODEL
15
2.3.2
RATE-BASED
MODELS
15
2.3.3
CHEMICAL
REACTION
18
2.3.4
FLOW
MODELS
20
2.3.5
FLOW
REGIMES
IN
PACKED
COLUMNS
29
2.3.6
DYNAMIC
MODELLING
31
3
DYNAMIC
MODELLING
OF
CATALYTIC
DISTILLATION
PROCESSES
32
3.1
DYNAMIC
RATE-BASED
MODEL
32
3.1.1
DYNAMIC
BALANCES
33
3.1.2
RATE
EQUATIONS
35
3.1.3
CHEMICAL
REACTION
36
3.2
PERIPHERAL
COLUMN
ELEMENTS
37
3.3
NUMERICAL
SOLUTION
38
3.4
CONCLUDING
REMARKS
40
4
CHARACTERISTICS
OF
THE
CATALYTIC
PACKING
MULTIPAK
41
4.1
EXPERIMENTAL
EQUIPMENT
AND
PROCEDURE
41
4.1.1
CATALYTIC
PACKING
MULTIPAK
41
4.1.2
EXPERIMENTAL
SET-UP
&
METHODOLOGY
42
4.2
EXPERIMENTAL
RESULTS
46
4.2.1
NON-IDEAL
FLOW
BEHAVIOUR
46
VI
CONTENTS
4.2.2
LIQUID
HOLD-UP,
PRESSURE
DROP
&
MASS
TRANSFER
51
4.3
CONCLUDING
REMARKS
52
5
CHEMICAL
REACTION
SYSTEMS
55
5.1
REACTIVE
TEST
SYSTEM
SELECTION
55
5.2
METHYL
ACETATE
SYNTHESIS
56
5.2.1
REACTION
SYSTEM
56
5.2.2
EXPERIMENTAL
SET-UP
57
5.2.3
ADSORPTION
EQUILIBRIA
57
5.2.4
REACTION
KINETICS
61
5.3
DIETHYL
CARBONATE
SYNTHESIS
66
5.3.1
REACTION
SYSTEM
66
5.3.2
REACTION
KINETICS
66
5.4
CONCLUDING
REMARKS
69
6
EXPERIMENTAL
CD
MODEL
VALIDATION
-
METHYL
ACETATE
SYNTHESIS
70
6.1
EXPERIMENTAL
SET-UP
70
6.2
RESULTS
71
6.3
CONCLUDING
REMARKS
81
7
THEORETICAL
ANALYSIS
82
7.1
METHYL
ACETATE
SYNTHESIS
82
7.1.1
STEADY-STATE
AND
DYNAMIC
PROCESS
BEHAVIOUR
83
7.1.2
SENSITIVITY
ANALYSIS
84
7.2
DIETHYL
CARBONATE
SYNTHESIS
91
7.2.1
STEADY-STATE
AND
DYNAMIC
PROCESS
BEHAVIOUR
92
7.2.2
SENSITIVITY
ANALYSIS
98
7.3
CONCLUDING
REMARKS
104
8
CONCLUSIONS
AND
OUTLOOK
106
A
EXPERIMENTAL
DATA
110
A.L
CATALYST
SPECIFICATION
OF
LEWATIT
K2621
110
A.2
CATALYST
PREPARATION
111
A.3
REACTION
KINETICS
OF
METHYL
ACETATE
SYNTHESIS
113
A.4
COMPOSITION
ANALYSIS
113
A.4.1
GAS-CHROMATOGRAPH
(GC)
113
A.4.2
NEAR
INFRARED
SPECTROMETER
(NIR)
116
A.5
HEAT
LOSSES
117
A.6
PHOTOS
OF
EXPERIMENTAL
SET-UPS
118
REFERENCES
121 |
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| author | Noeres, Christoph |
| author_facet | Noeres, Christoph |
| author_role | aut |
| author_sort | Noeres, Christoph |
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| bvnumber | BV017401371 |
| classification_rvk | VN 7227 |
| ctrlnum | (OCoLC)249430773 (DE-599)BVBBV017401371 |
| discipline | Chemie / Pharmazie |
| edition | Als Ms. gedr. |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV017401371 |
| illustrated | Illustrated |
| indexdate | 2024-08-23T00:16:13Z |
| institution | BVB |
| isbn | 3183784033 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010485640 |
| oclc_num | 249430773 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-210 DE-634 DE-83 |
| owner_facet | DE-91G DE-BY-TUM DE-210 DE-634 DE-83 |
| physical | XII, 133 S. graph. Darst. |
| publishDate | 2003 |
| publishDateSearch | 2003 |
| publishDateSort | 2003 |
| publisher | VDI-Verl. |
| record_format | marc |
| series | Fortschritt-Berichte VDI |
| series2 | Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik |
| spelling | Noeres, Christoph Verfasser aut Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres Als Ms. gedr. Düsseldorf VDI-Verl. 2003 XII, 133 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Fortschritt-Berichte VDI : Reihe 3, Verfahrenstechnik 784 Zugl.: Dortmund, Univ., Diss., 2002 Reaktivdestillation - Katalyse Katalyse (DE-588)4029921-1 gnd rswk-swf Reaktivdestillation (DE-588)4491776-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Reaktivdestillation (DE-588)4491776-4 s Katalyse (DE-588)4029921-1 s DE-604 Fortschritt-Berichte VDI Reihe 3, Verfahrenstechnik ; 784 (DE-604)BV001897067 784 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010485640&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Noeres, Christoph Catalytic distillation dynamic modelling, simulation, and experimental validation Fortschritt-Berichte VDI Reaktivdestillation - Katalyse Katalyse (DE-588)4029921-1 gnd Reaktivdestillation (DE-588)4491776-4 gnd |
| subject_GND | (DE-588)4029921-1 (DE-588)4491776-4 (DE-588)4113937-9 |
| title | Catalytic distillation dynamic modelling, simulation, and experimental validation |
| title_auth | Catalytic distillation dynamic modelling, simulation, and experimental validation |
| title_exact_search | Catalytic distillation dynamic modelling, simulation, and experimental validation |
| title_full | Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres |
| title_fullStr | Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres |
| title_full_unstemmed | Catalytic distillation dynamic modelling, simulation, and experimental validation Christoph Noeres |
| title_short | Catalytic distillation |
| title_sort | catalytic distillation dynamic modelling simulation and experimental validation |
| title_sub | dynamic modelling, simulation, and experimental validation |
| topic | Reaktivdestillation - Katalyse Katalyse (DE-588)4029921-1 gnd Reaktivdestillation (DE-588)4491776-4 gnd |
| topic_facet | Reaktivdestillation - Katalyse Katalyse Reaktivdestillation Hochschulschrift |
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