Polymer crystallization: observations, concepts and interpretations
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2003
|
| Schriftenreihe: | Lecture notes in physics
606 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XVII, 386 S. Ill., graph. Darst. : 24 cm |
| ISBN: | 3540443428 |
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Datensatz im Suchindex
| _version_ | 1804130083787505664 |
|---|---|
| adam_text | G. REITER J.-U. SOMMER (EDS.)
POLYMER CRYSTALLIZATION
OBSERVATIONS, CONCEPTS AND INTERPRETATIONS
SPRINGER
TABLE OF CONTENTS
1 INTRODUCTION
JENS-UWE SOMMER AND GUENTER REITER 1
2 POLYMER CRYSTALLIZATION VIEWED IN THE GENERAL CONTEXT
OF PARTICLE FORMATION AND CRYSTALLIZATION
JENS RIEGER 7
2.1 INTRODUCTION 7
2.2 CLASSICAL NUCLEATION THEORY 8
2.3 PRECURSORS 9
2.4 SPINODAL VS. BINODAL PHASE SEPARATION 11
2.5 COMPUTER SIMULATIONS OF THE EARLY STAGES OF PARTICLE FORMATION
AND CRYSTALLIZATION 11
2.6 CONTROL OF CRYSTALLIZATION BY ADDITIVES 12
2.7 OSTWALD S RULE OF STAGES 13
2.8 OSTWALD RIPENING VS. SECONDARY CRYSTALLIZATION 14
2.9 DISCUSSION 14
REFERENCES 14
3 ROLE OF METASTABLE PHASES IN POLYMER CRYSTALLIZATION;
EARLY STAGES OF CRYSTAL GROWTH
SANJAY RASTOGI 17
3.1 INTRODUCTION 17
3.2 EXPERIMENTAL SECTION 19
3.2.1 MATERIALS 19
3.2.2 HIGH PRESSURE CELL 19
3.2.3 POLARISING OPTICAL MICROSCOPY 19
3.2.4 WIDE ANGLE X-RAY SCATTERING 20
3.3 RESULTS AND DISCUSSION 20
3.3.1 POLYETHYLENE - A SUMMARY OF PREVIOUSLY REPORTED RESULTS
ON CRYSTALLISATION OF SINGLE CRYSTALS IN POLYETHYLENE MELTS.... 20
3.3.2 EXPERIMENTAL OBSERVATIONS ON A CRYSTAL
AFTER ITS TRANSFORMATION FROM THE METASTABLE HEXAGONAL PHASE
INTO THE THERMODYNAMICALLY STABLE ORTHORHOMBIC PHASE 21
3.3.3 MULTILAYERING: PRIMARY AND SECONDARY THICKENING 25
VIII TABLE OF CONTENTS
3.3.4 SIZE INFLUENCE IN PHASE TRANSFORMATION:
STAHLE, METASTABLE AND TRANSIENT STATES OF A PHASE 28
3.3.5 IMPLICATIONS TO CRYSTALLISATION AT ATMOSPHERIC PRESSURE 38
3.3.6 AN APPLICATION OF ENHANCED CHAIN MOBILITY IN THE TRANSIENT
PHASE OF ULTRA HIGH MOLECULAR WEIGHT POLYETHYLENE 41
3.4 CONCLUSIONS 44
REFERENCES 46
4 A COMPARATIVE STUDY OF THE MECHANISMS
OF INITIAL CRYSTALLIZATION AND RECRYSTALLIZATION
AFTER MELTING IN SYNDIOTACTIC POLYPROPENE AND ISOTACTIC POLYSTYRENE
MAHMOUD AI-HUSSEIN, GERT STROBL 48
4.1 INTRODUCTION 48
4.2 EXPERIMENTAL 50
4.2.1 SAMPLE CHARACTERISTICS AND PREPARATION 50
4.2.2 SAXS MEASUREMENTS 50
4.3 RESULTS 52
4.4 DISCUSSION 60
REFERENCES 62
5 POLYMER CRYSTALLIZATION VIEWED BY MAGNETIC ALIGNMENT
TSUNEHISA KIMURA 64
5.1 INTRODUCTION 64
5.2 PRINCIPLE OF DIAMAGNETIC ALIGNMENT 65
5.3 MESOPHASE DETECTED BY MAGNETIC ALIGNMENT 68
5.4 MOLTEN STATES 75
5.5 MAGNETO-CLAPEYRON : 78
5.6 CONCLUDING REMARKS 79
REFERENCES 80
6 FOLLOWING CRYSTALLIZATION IN POLYMERS USING AFM
JAMIE K. HOBBS 82
6.1 BACKGROUND 82
6.2 THE USE OF AFM TO FOLLOW CRYSTALLIZATION 85
6.2.1 SAMPLE PREPARATION 88
6.3 RESULTS AND DISCUSSION 88
6.3.1 THE CRYSTAL MELT INTERFACE 89
6.3.2 ON THE SURFACE TEXTURE OF POLYETHYLENE LAMELLAE 92
6.3.3 THE MELTING OF ISOLATED LAMELLAE 93
6.4 CONCLUSIONS 95
REFERENCES 96
TABLE OF CONTENTS IX
7 ATOMIC FORCE MICROSCOPY STUDIES
OF SEMICRYSTALLINE POLYMERS AT VARIABLE TEMPERATURE
DIMITRI A. IVANOV, SERGEI N. MAGONOV 98
7.1 INTRODUCTION 98
7.2 STUDIES OF POLYMERS IN TAPPING MODE 100
7.2.1 TIP-SAMPLE FORCES 100
7.2.2 IMAGE RESOLUTION 102
7.2.3 SAMPLE PREPARATION 103
7.3 PRACTICAL EXAMPLES OF IMAGING
OF SEMI-CRYSTALLINE POLYMERS AT VARIABLE TEMPERATURE 103
7.3.1 FLEXIBLE CHAIN POLYMERS 104
7.3.2 SEMI-RIGID CHAIN POLYMERS 116
7.4 CONCLUSIONS 127
REFERENCES 127
8 CRYSTALLIZATION OF POLYMERS IN THIN FILMS:
MODEL EXPERIMENTS
GUENTER REITER, GILLES CASTELEIN, JENS-UWE SOMMER 131
8.1 INTRODUCTION 131
8.2 EXPERIMENTAL SECTION 133
8.2.1 POLYMERS 133
8.2.2 SAMPLE PREPARATION 134
8.2.3 OBSERVATION TECHNIQUES 135
8.3 RESULTS AND DISCUSSION 136
8.3.1 CRYSTALLIZATION OF ADSORBED PEO HOMOPOLYMER MONOLAYERS . . 136
8.3.2 RELAXATIONS OF POLYMER CRYSTALS AFTER FORMATION 141
8.3.3 DISCRETE VARIATION OF LAMELLAR SPACINGS WITH TEMPERATURE
IN BLOCK COPOLYMER SYSTEMS 144
8.3.4 INDIVIDUAL CRYSTALLIZATION AND MELTING
OF POLYMER NANOCRYSTALS 147
8.4 CONCLUSIONS . . 150
REFERENCES 151
9 A GENERIC MODEL FOR GROWTH AND MORPHOGENESIS
OF POLYMER CRYSTALS IN TWO DIMENSIONS
JENS-UWE SOMMER, GUENTER REITER 153
9.1 INTRODUCTION 153
9.2 A LATTICE MODEL FOR CRYSTALLIZATION IN POLYMER MONOLAYERS 158
9.3 GROWTH MORPHOLOGIES 162
9.4 SELF-ORGANIZED CRYSTAL THICKNESS AND GROWTH VELOCITY 165
9.5 REORGANIZATION OF THE POLYMER CRYSTAL 168
9.6 ANNEALING AND MORPHOGENESIS - THE CRYSTALLINE LIQUID STATE 171
9.7 HEATING WITH A CONSTANT RATE AND THE ROLE OF MORPHOGENESIS 173
9.8 CONCLUSIONS 175
REFERENCES 176
X TABLE OF CONTENTS
10 STRUCTURE FORMATION AND CHAIN-FOLDING
IN SUPERCOOLED POLYMER MELTS. SOME IDEAS
FROM MD SIMULATIONS WITH A COARSE-GRAINED MODEL
HENDRIK MEYER 177
10.1 INTRODUCTION 177
10.1.1 THE MODEL CG-PVA: EXCLUDED VOLUME, CONNECTIVITY
AND ROTATIONAL ISOMERIC STATES 178
10.1.2 SIMULATION DETAILS 179
10.2 STRUCTURE FORMATION IN A MELT OF SHORT CHAMS 179
10.2.1 HOMOGENEOUS NUCLEATION 181
10.2.2 POSITIONAL, ORIENTATIONAL AND CONFORMATIONAL ORDER 182
10.3 CHAIN-LENGTH DEPENDENCE OF CRYSTALLIZATION
AND MELTING TEMPERATURES 185
10.4 CHAIN-FOLDING IN ISOTHERMAL RELAXATION OF LONG CHAINS 187
10.4.1 SLIGHTLY ENTANGLED CHAINS (N = 100) 187
10.4.2 ENTANGLED CHAINS (TV = 400) 191
10.5 DISCUSSION AND CONCLUSIONS 192
REFERENCES 195
11 LAMELLAR ETHYLENE OXIDE*BUTADIENE BLOCK COPOLYMER FILMS
AS MODEL SYSTEMS FOR CONFLNED CRYSTALLISATION
WIM H. DE JEU 196
11.1 INTRODUCTION 196
11.2 EXPERIMENTAL SITUATION 197
11.3 DISCUSSION AND MODELLING 202
11.4 CONCLUSIONS AND OPEN QUESTIONS 205
REFERENCES 207
12 CRYSTALLIZATION KINETICAL PECULIARITIES IN POLYMER BLENDS
BERND-J. JUNGNICKEL 208
12.1 INTRODUCTION 208
12.2 IMMISCIBLE BLENDS: FRACTIONATED CRYSTALLIZATION 210
12.3 BLENDS WITH MISCIBILITY GAP: INTERFACE CROSSING CRYSTALLIZATION 214
12.4 MISCIBLE CRYSTALLIZING BLENDS: PSEUDOEUTECTIC BEHAVIOUR 215
12.5 MISCIBLE BLENDS: CRYSTALLIZATION INDUCED
COMPOSITION INHOMOGENEITIES 219
12.6 MISCIBLE BLENDS: COMPETITION BETWEEN
CRYSTALLIZATION AND VITRIFICATION 225
12.7 BLENDS WITH MISCIBILITY GAP:
COMPETITION BETWEEN CRYSTALLIZATION AND MIXING/DEMIXING 229
12.8 PICTURE GALLERY 231
12.9 CONCLUDING REMARKS 236
REFERENCES 236
TABLE OF CONTENTS XI
13 DENDRITIC GROWTH OF POLYETHYLENE OXIDE
ON PATTERNED SURFACES
HANS-GEORG BRAUN, EVELYN MEYER, MINGTAI WANG 238
13.1 INTRODUCTION 238
13.2 CREATION OF DEFINED MICROMETERSIZED PATTERNS
BY CHEMICAL SURFACE HETEROGENISATION 239
13.3 PREPARATION OF ULTRATHIN MICROPATTERNED AMORPHOUS
POLYETHYLENE OXIDE (PEO) LAYERS BY CONTROLLED DEWETTING
ON HETEROGENEOUS SURFACES 240
13.4 CHARACTERISTIC GROWTH PATTERNS OF PEO LAMELLAE
ON MICROPATTERNED SURFACE AREAS 243
13.4.1 BASIC IDEAS ON DIFFUSION CONTROLLED CRYSTALLISATION 243
13.4.2 BRANDUNG STRUCTURES OF PEO CRYSTALLISED
IN ULTRATHIN MICRO-PATTERNED FILMS 245
13.4.3 CRYSTALLISATION OF PEO IN MICRODROPLETS OBTAINED
BY DEWETTING ON HETEROGENEOUS SURFACES 249
13.5 SUMMARY 250
REFERENCES 250
14 VITRIFICATION AND DEVITRIFICATION OF THE RIGID AMORPHOUS
FRACTION IN SEMICRYSTALLINE POLYMERS REVEALED
FROM FREQUENCY DEPENDENT HEAT CAPACITY
CHRISTOPH SCHICK, ANDREAS WURM, ALAA MOHAMMED 252
14.1 INTRODUCTION 252
14.2 DETERMINATION OF THE RIGID AMORPHOUS FRACTION 255
14.3 EXPERIMENTAL 258
14.4 RESULTS 261
14.5 DISCUSSION 267
14.6 CONCLUSION 271
REFERENCES 272
15 PROBING CRYSTALLIZATION
STUDYING AMORPHOUS PHASE EVOLUTION
TIBERIO A. EZQUERRA, AURORA NOGALES 275
15.1 INTRODUCTION 275
15.2 BRIEF DESCRIPTION OF DIELECTRIC SPECTROSCOPY 277
15.3 INFLUENCE OF CRYSTALLINITY ON THE SEGMENTAL RELAXATION 278
15.4 INFLUENCE OF CRYSTALLINITY ON THE SEGMENTAL COOPERATIVITY 282
15.5 CRYSTALLIZATION AS REVEALED BY THE TIME EVOLUTION
OF THE CRYSTALLINE AND THE AMORPHOUS PHASES 284
15.5.1 LAMELLAR STRUCTURE FORMATION 284
15.5.2 CRYSTALLIZATION INDUCED EFFECTS IN THE AMORPHOUS PHASE 288
15.5.3 COMBINED PICTURE ABOUT CRYSTALLIZATION
FROM THE STRUCTURE-DYNAMICS RELATIONSHIPS 291
15.6 CONCLUSIONS 294
XII TABLE OF CONTENTS
16 MODELING POLYMER CRYSTALLIZATION: DSC APPROACH
JOAN JOSEP SUFIOL 297
16.1 INTRODUCTION 297
16.2 KINETIC ANALYSIS 298
16.3 SPECIFIC SURFACE ENERGY 306
16.4 CONCLUSIONS 308
REFERENCES 310
17 A COMPUTATIONAL MODEL FOR PROCESSING OF SEMICRYSTALLINE
POLYMERS: THE EFFECTS OF FLOW-INDUCED CRYSTALLIZATION
GERRIT W.M. PETERS 312
17.1 INTRODUCTION 312
17.2 MODELLING 313
17.2.1 BALANCE EQUATIONS 313
17.2.2 CONSTITUTIVE EQUATIONS 313
17.3 RESULTS 318
17.4 CONCLUSIONS 323
REFERENCES 324
18 PHYSICAL CROSS LINKS IN AMORPHOUS PET,
INFLUENCE OF COOLING RATE AND AGEING
STEFANO PICCAROLO, ELENA VASSILEVA, ZEBENE KIFIIE 325
18.1 INTRODUCTION 325
18.2 CONTINUOUS COOLING TRANSFORMATION (CCT) OF PET 326
18.3 PHYSICAL CROSS LINKS VS ENTANGLEMENTS 327
18.4 SAMPLE PREPARATION AND TEST PROCEDURE . 329
18.5 ISOTHERMAL CRYSTALLIZATION OF GLASSY PET 330
18.6 REJUVENATION PROCEDURE 331
18.7 RESULTS 332
18.8 CONCLUSIONS 340
REFERENCES 341
19 MAXIMUM CRYSTAL GROWTH RATE
AND ITS CORRESPONDING STATE IN POLYMERIE MATERIALS
NORIMASA OKUI, SUSUMU UMEMOTO 343
19.1 INTRODUCTION 343
19.2 TEST OF WLF AND ARRHENIUS EXPRESSIONS 344
19.3 MASTER CURVE FOR CRYSTAL GROWTH RATE 347
19.4 MOLECULAR WEIGHT DEPENDENCE OF CRYSTAL GROWTH RATE 350
19.4.1 EFFECT OF SUPER COOLING
ON THE MOLECULAR WEIGHT DEPENDENCE OF GROWTH RATE 353
19.4.2 MOLECULAR WEIGHT DEPENDENCE
OF MAXIMUM CRYSTAL GROWTH RATE 354
19.5 RELATIONSHIP BETWEEN T AND T
CMAX
357
TABLE OF CONTENTS XIII
19.5.1 RATIO OF AE AND AH
M
359
19.5.2 RATIO OF A AND AH
M
360
19.6 RELATIONSHIP AMONG THERMODYNAMIC TRANSITION TENIPERATURES 360
19.7 CONCLUSIONS 363
REFERENCES 364
20 LAMELLAR GROWTH IN MELT-CRYSTALLIZING POLYMERS:
SOME EFFECT RELATED TO A NUCLEATING AGENT
GAETANO DI MARCO, MARCO PIERUCCINI 366
20.1 INTRODUCTION 366
20.2 PRELIMINARY ANALYSIS 367
20.3 THERMODYNAMIC VIEWPOINT 368
20.4 LATTICE MODEL 371
20.5 SAXS ANALYSIS 374
20.6 CONCHIDING RCMARKS 376
REFERENCES 377
21 OUTLOOK AND OPEN QUESTIONS: A PERSONAL VIEW
GUENTER REITER, JENS-UWE SOMMER 378
SUBJECT INDEX 383
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| series | Lecture notes in physics |
| series2 | Lecture notes in physics Physics and astronomy online library |
| spelling | Polymer crystallization observations, concepts and interpretations G. Reiter ... (ed.) Berlin [u.a.] Springer 2003 XVII, 386 S. Ill., graph. Darst. : 24 cm txt rdacontent n rdamedia nc rdacarrier Lecture notes in physics 606 Physics and astronomy online library Literaturangaben Física larpcal Crystalline polymers Crystallization Polymers Polymere (DE-588)4046699-1 gnd rswk-swf Kristallisation (DE-588)4033215-9 gnd rswk-swf Polymere (DE-588)4046699-1 s Kristallisation (DE-588)4033215-9 s DE-604 Reiter, Günter Sonstige oth Lecture notes in physics 606 (DE-604)BV000003166 606 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010387829&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Polymer crystallization observations, concepts and interpretations Lecture notes in physics Física larpcal Crystalline polymers Crystallization Polymers Polymere (DE-588)4046699-1 gnd Kristallisation (DE-588)4033215-9 gnd |
| subject_GND | (DE-588)4046699-1 (DE-588)4033215-9 |
| title | Polymer crystallization observations, concepts and interpretations |
| title_auth | Polymer crystallization observations, concepts and interpretations |
| title_exact_search | Polymer crystallization observations, concepts and interpretations |
| title_full | Polymer crystallization observations, concepts and interpretations G. Reiter ... (ed.) |
| title_fullStr | Polymer crystallization observations, concepts and interpretations G. Reiter ... (ed.) |
| title_full_unstemmed | Polymer crystallization observations, concepts and interpretations G. Reiter ... (ed.) |
| title_short | Polymer crystallization |
| title_sort | polymer crystallization observations concepts and interpretations |
| title_sub | observations, concepts and interpretations |
| topic | Física larpcal Crystalline polymers Crystallization Polymers Polymere (DE-588)4046699-1 gnd Kristallisation (DE-588)4033215-9 gnd |
| topic_facet | Física Crystalline polymers Crystallization Polymers Polymere Kristallisation |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010387829&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000003166 |
| work_keys_str_mv | AT reitergunter polymercrystallizationobservationsconceptsandinterpretations |