Melt crystallization: fundamentals, equipment and applications
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2003
|
| Schriftenreihe: | Berichte aus der Verfahrenstechnik
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XII, 255 S. Ill., graph. Darst. |
| ISBN: | 3832215336 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV017175768 | ||
| 003 | DE-604 | ||
| 005 | 20040216 | ||
| 007 | t | ||
| 008 | 030527s2003 gw ad|| |||| 00||| eng d | ||
| 016 | 7 | |a 967619602 |2 DE-101 | |
| 020 | |a 3832215336 |9 3-8322-1533-6 | ||
| 035 | |a (OCoLC)54928651 | ||
| 035 | |a (DE-599)BVBBV017175768 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a eng | |
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| 049 | |a DE-703 |a DE-29T |a DE-634 | ||
| 084 | |a VN 7260 |0 (DE-625)147614:253 |2 rvk | ||
| 245 | 1 | 0 | |a Melt crystallization |b fundamentals, equipment and applications |c Joachim Ulrich ... (ed.) |
| 264 | 1 | |a Aachen |b Shaker |c 2003 | |
| 300 | |a XII, 255 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Berichte aus der Verfahrenstechnik | |
| 500 | |a Literaturangaben | ||
| 650 | 0 | 7 | |a Schmelzkristallisation |0 (DE-588)4243444-0 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Schmelzkristallisation |0 (DE-588)4243444-0 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Ulrich, Joachim |e Sonstige |4 oth | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010352815&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-010352815 | |
Datensatz im Suchindex
| _version_ | 1808044836384669696 |
|---|---|
| adam_text |
CONTENTS
V
CONTENTS
PREFACE
III
CONTRIBUTORS
XI
1.
INTRODUCTION
1
JOACHIM
ULRICH
1.1
DEFINITIONS
1
1.2
BENEFITS
OF
MELT
CRYSTALLIZATION
2
REFERENCES
5
2.
PHASE
DIAGRAMS
7
AXEL
KONIG
2.1
INTRODUCTION
7
2.2
PHASE
EQUILIBRIUM
8
2.2.1
CONDITIONS
8
2.2.2
GIBBS
PHASE
RULE
9
2.2.3
GRAPHICAL
REPRESENTATION
10
2.2.3.1
ONE-COMPONENT
SYSTEM
10
2.2.3.2
TWO-COMPONENT
SYSTEM
11
2.2.3.3
THREE-COMPONENT
SYSTEM
12
2.3
CRYSTALLIZATION IN
TWO-COMPONENT
SYSTEMS
16
2.3.1
SOLID
SOLUTION
TYPE
16
2.3.2
EUTECTIC
TYPE
19
2.3.3
COMPOUND
FORMATION
TYPE
22
2.3.4
PERITECTIC
TYPE
24
2.4
CRYSTALLIZATION
IN
THREE-COMPONENT
SYSTEMS
25
2.4.1
ONE-SOLID
FORMATION
25
2.4.2
EUTECTIC
TYPE
26
2.4.3
SOLID
SOLUTION
TYPE
28
2.4.4
COMPOUND
FORMATION
29
VI
CONTENTS
2.5
PHASE
EQUILIBRIA
DETECTION
30
2.5.1
EXPERIMENTAL
30
2.5.2
CALCULATION
31
2.6
REAL
PHASE
DIAGRAM
34
NOMENCLATURE
38
REFERENCES
39
3.
KINETICS:
FUNDAMENTALS
OF
NUCLEATION
AND
CRYSTAL
GROWTH
41
ANGELO
CHIANESE,
MARIAPAOLA
PARISI
3.1
INTRODUCTION
41
3.1.1
THE
DRIVING
FORCE
42
3.1.2
SUPERSATURATION
UNITS
43
3.2
NUCLEATION
44
3.2.1
METASTABLE
ZONE
45
3.2.2
PRIMARY
NUCLEATION
46
3.2.3
SECONDARY
NUCLEATION
50
3.3
CRYSTAL
GROWTH
52
3.3.1
CRYSTAL
GROWTH
RATE
53
3.3.2
CRYSTAL
GROWTH
KINETICS
55
3.3.2.1
INTEGRATION
OF
THE
GROWTH
UNITS
IN
THE
CRYSTAL
55
3.3.2.2
GROWTH
THEORIES
AND
FUNDAMENTAL
GROWTH
RATE
EXPRESSIONS
58
3.3.2.3
INFLUENCE
OF
THE
TRANSPORT
PHENOMENA
61
3.3.3
NON-EQUILIBRIUM
GROWTH
IN
A
MELT
CRYSTALLIZER
64
NOMENCLATURE
67
REFERENCES
69
4.
SOLID
LAYER
CRYSTALLIZATION
71
JOACHIM
ULRICH
4.1
INTRODUCTION
71
4.1.1
ADVANTAGES
72
4.1.2
LIMITATIONS
73
4.2
CONCEPTS
OF
EXISTING PLANTS
74
4.3
THE
SWEATING
STEP
79
4.4
THE
WASHING
STEP
82
4.5
CONTINUOUS
PLANTS
86
4.5.1
ADVANTAGES
86
4.5.2
PROCESS
CONCEPTS
86
CONTENTS
VII
4.6
SUMMARY
AND
A
VIEW
TO
THE
FUTURE
87
NOMENCLATURE
88
REFERENCES
89
5.
SUSPENSION-BASED
MELT
CRYSTALLIZATION:
PRINCIPLES,
EQUIPMENT,
APPLICATIONS
93
DIRK
VERDOES,
MICHIEL
NIENOORD
5.1
INTRODUCTION
93
5.2
ADVANTAGES
AND
DISADVANTAGES
OF
SUSPENSION
MELT
CRYSTALLIZATION
95
5.3
SIMILARITIES
AND
DIFFERENCES IN
BASIC
PRINCIPLES,
MATERIAL PROPERTIES
AND
MODELS
FOR
SOLUTION
AND
MELT
CRYSTALLIZATION
96
5.4
STATE
OF
THE
ART
OF
SUSPENSION
MELT
CRYSTALLIZERS:
INDUSTRIAL
EQUIPMENT
AND
APPLICATIONS
101
5.5
SOLID-LIQUID
SEPARATION
IN
SUSPENSION
MELT
CRYSTALLIZATION
108
5.6
SUMMARY
124
NOMENCLATURE
126
REFERENCES
126
6.
LABORATORY
TESTS
FOR
MELT
CRYSTALLIZATION
129
HEIKE
GLADE,
JOACHIM
ULRICH
6.1
INTRODUCTION
129
6.2
SUSPENSION
AND
SOLID
LAYER
MELT
CRYSTALLIZATION
129
6.3
A
STEP-BY-STEP
APPROACH
TO
DETERMINE
THE
TECHNICAL
FEASIBILITY
OF
MELT
CRYSTALLIZATION
133
6.3.1
STAGE
1:
JUDGMENT
OF
PHYSICAL
PROPERTIES
135
6.3.2
STAGE
2:
TESTS
FOR
SUSPENSION
AND
LAYER
MELT
CRYSTALLIZATION
138
6.3.2.1
SUSPENSION
CRYSTALLIZATION
138
6.3.2.1.1
ZONE
MELTING
(STAGE
2,
SUSPENSION)
138
6.3.2.
1.
2
SINGLE
CRYSTAL
METHOD
(STAGE
2,
SUSPENSION)
140
6.3.2.1.3
METASTABLE ZONE
WIDTH
(STAGE
2,
SUSPENSION)
141
6.3.2.1.4
BATCH
EXPERIMENTS
ON
SMALL
SCALE
(STAGE
2,
SUSPENSION)
143
6.3.2.2
SOLID
LAYER
CRYSTALLIZATION
146
6.3.2.2.
1
BOTTLE
TEST
(STAGE
2,
LAYER
CRYSTALLIZATION)
147
6.3.2.2.2
COLD
FINGER
EXPERIMENTS
(STAGE
2,
LAYER
CRYSTALLIZATION)
147
6.3.3
STAGE
3:
TESTS
FOR
SUSPENSION
AND
LAYER
MELT
CRYSTALLIZATION
150
6.3.3.1
CONTINUOUS
SUSPENSION
CRYSTALLIZATION
ON
3
LITER
SCALE
(STAGE
3,
SUSPENSION)
150
VIII
CONTENTS
63.3.2
POST-CRYSTALLIZATION
TREATMENT
FOR
LAYERS:
SWEATING
AND
WASHING
(STAGE
3,
LAYER
CRYSTALLIZATION)
154
6.33.2.1
SWEATING
(DRY)
154
6.33.2.2
WASHING
155
6.3.4
STAGE
4:
TESTS
ON
SOLID-LIQUID
SEPARATION
IN
SUSPENSION
CRYSTALLIZATION
156
6.3.5
SOLIDIFICATION
OF
(PURIFIED)
MELTS
161
6.4
CONCLUSION
162
NOMENCLATURE
162
REFERENCES
162
7.
SEPARATE
ORGANICS
BY
MELT
CRYSTALLIZATION:
A
GUIDE
TO
WHEN
AND
HOW
TO
USE
THIS
TECHNIQUE
167
MANFRED
STEPANSKI,
ERIK
SCHAFER
7.1
INTRODUCTION
167
7.2
LAYER
CRYSTALLIZATION
168
7.2.1
STATIC
CRYSTALLIZATION
169
7.2.2
FALLING
FILM
CRYSTALLIZATION
170
7.2.3
LAYER
DRAINING
AND
SWEATING
171
7.2.4
MULTISTAGING
FOR
INCREASED
PURITY
172
7.2.5
RESIDUE
STRIPPING
TO
IMPROVE
RECOVERY
173
7.2.6
PLANT
DESIGN CONSIDERATIONS
173
7.3
APPROACH
FOR
NEW
APPLICATIONS
175
7.3.1
INITIAL
CONSIDERATIONS
175
7.3.2
PRELIMINARY
INVESTIGATION
176
7.3.3
DESIGN
DATA
ACQUISITION
AND
MODELING
177
7.33.1
MODELING
OF
CRYSTALLIZATION
IN
LAYER
GROWTH
PROCESSES
177
7.33.2
MODELING
OF
SWEATING
179
7.3.33
MODELING
OF
A
COMPLETE
SEPARATION
PROCESS
181
7.4
EXAMPLE
OF
PROCESS
DESIGN
182
7.5
INDUSTRIAL
APPLICATIONS
186
NOMENCLATURE
187
REFERENCES
188
8.
SEPARATE
ORGANICS
BY
SUSPENSION
CRYSTALLIZATION
191
REINHARD
SCHOLZ,
RAY
RUEMEKORF
8.1
INTRODUCTION
191
8.2
THE CRYSTALLIZATION
STEP
191
CONTENTS
IX
8,3
THE
CRYSTAL-LIQUID
SEPARATION
194
8.3.1
CONVENTIONAL
SOLID-LIQUID
SEPARATION
194
8.3.2
WASH
COLUMN
SEPARATION
196
8.3.3
COMPARISON
OF
DIFFERENT
SEPARATION
TECHNOLOGIES
198
8.4
WASH
COLUMN TECHNOLOGY
200
8.4.1
GRAVITY
WASH
COLUMNS
201
8.4.2
HYDRAULIC
WASH
COLUMNS
202
8.4.3
MECHANICAL WASH
COLUMNS
202
8.4.3.1
PISTON
TYPE
WASH
COLUMNS
202
8.4.3.2
THE
NIROYY PURIFIER
203
8.4.4
IMPORTANT
PROCESS
PARAMETERS
205
8.5
GROWING
APPLICATION
BASE
208
8.6
INVESTIGATING
FEASIBILITY
OF
NEW
APPLICATIONS
210
NOMENCLATURE
211
REFERENCES
212
9.
UPDATE
ON
PERFORMANCE
OF
MELT
STATIC
CRYSTALLIZATION
213
RENE
GENIN
9.1
INTRODUCTION
213
9.2
PROCESS FEATURES
213
9.2.1
GENERAL
213
9.2.2
PRODUCT PURIFICATION
215
9.2.2.1
PRODUCT
PURIFICATION
BY
SWEATING
216
9.2.2.2
PRODUCT
PURIFICATION
BY
COUNTER
CURRENT
WASHING
217
9.2.3
SUPERCHARGING
218
9.3
EXAMPLES
OF
INDUSTRIAL
APPLICATION
219
9.3.1
DCNB
ISOMER
SEPARATION
219
9.3.2
ODCB/PDCB/MDCB
ISOMER
SEPARATION
220
9.3.3
NAPHTHALENE
AND
ANTHRACENE
PURIFICATION
223
9.4
PROCESS
PERFORMANCES
224
9.5
CONCLUSION
225
REFERENCES
225
10.
MELT
SOLIDIFICATION
AND
GRANULATION
TECHNOLOGY
227
HENRIK
C.
BULAU,
ANDREAS
ROBENS
10.1
INTRODUCTION
10.2
SOLIDIFICATION
AND
GRANULATION
PROCESSES
227
228
X
CONTENTS
10.2.1
INDIRECT
COOLING
228
10.2.1.1
PASTILLATION
229
10.2.1.1.1
PASTILLATION
SYSTEMS
229
10.2.1.1.2
COOLING
DRUM
PASTILLATION
234
10.2.1.1.3
COOLING
DISK
PASTILLATION
235
10.2.1.1.4
COOLING
BELT
PASTILLATION
235
10.2.1.2
COOLING
BELT
STRIP
FORMING
237
10.2.1.3
COOLING
BELT
FILM
CASTING
239
10.2.1.4
DOUBLE
COOLING
BELT
FILM
CASTING
240
10.2.1.5
SLAB
MOULDING
240
10.2.2
DIRECT
COOLING
241
10.2.2.1
CRYOGENIC
GRANULATION
242
10.2.2.2
UNDER
WATER
GRANULATION
243
10.2.2.3
UNDER
WATER
STRING
GRANULATION
244
10.2.3
SPECIAL
SOLIDIFICATION EQUIPMENT
245
10.2.3.1
SILICONIZED
PAPER
CARTON
BOX
FILLING
245
10.2.3.2
FORM
FILL
AND
SEAL
PROCESS
246
10.2.3.3
PILLOW-FORMING
PROCESS
247
10.3
LAYOUT
OF
SOLIDIFICATION
EQUIPMENT
248
10.4
SUMMARY
AND
CONCLUSION
251
REFERENCES
251
KEYWORD
INDEX
253 |
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| id | DE-604.BV017175768 |
| illustrated | Illustrated |
| indexdate | 2024-08-22T00:18:42Z |
| institution | BVB |
| isbn | 3832215336 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010352815 |
| oclc_num | 54928651 |
| open_access_boolean | |
| owner | DE-703 DE-29T DE-634 |
| owner_facet | DE-703 DE-29T DE-634 |
| physical | XII, 255 S. Ill., graph. Darst. |
| publishDate | 2003 |
| publishDateSearch | 2003 |
| publishDateSort | 2003 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Verfahrenstechnik |
| spelling | Melt crystallization fundamentals, equipment and applications Joachim Ulrich ... (ed.) Aachen Shaker 2003 XII, 255 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Verfahrenstechnik Literaturangaben Schmelzkristallisation (DE-588)4243444-0 gnd rswk-swf Schmelzkristallisation (DE-588)4243444-0 s DE-604 Ulrich, Joachim Sonstige oth DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010352815&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Melt crystallization fundamentals, equipment and applications Schmelzkristallisation (DE-588)4243444-0 gnd |
| subject_GND | (DE-588)4243444-0 |
| title | Melt crystallization fundamentals, equipment and applications |
| title_auth | Melt crystallization fundamentals, equipment and applications |
| title_exact_search | Melt crystallization fundamentals, equipment and applications |
| title_full | Melt crystallization fundamentals, equipment and applications Joachim Ulrich ... (ed.) |
| title_fullStr | Melt crystallization fundamentals, equipment and applications Joachim Ulrich ... (ed.) |
| title_full_unstemmed | Melt crystallization fundamentals, equipment and applications Joachim Ulrich ... (ed.) |
| title_short | Melt crystallization |
| title_sort | melt crystallization fundamentals equipment and applications |
| title_sub | fundamentals, equipment and applications |
| topic | Schmelzkristallisation (DE-588)4243444-0 gnd |
| topic_facet | Schmelzkristallisation |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010352815&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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