Optimal operation of batch cooling crystallizers:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
2002
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | München, Techn. Univ., Diss., 2002 |
| Beschreibung: | 166 S. Ill., graph. Darst. |
Internformat
MARC
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| 100 | 1 | |a Löffelmann, Michael |d 1970- |e Verfasser |0 (DE-588)12444511X |4 aut | |
| 245 | 1 | 0 | |a Optimal operation of batch cooling crystallizers |c Michael Löffelmann |
| 264 | 1 | |c 2002 | |
| 300 | |a 166 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a München, Techn. Univ., Diss., 2002 | ||
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Datensatz im Suchindex
| _version_ | 1807593308760834048 |
|---|---|
| adam_text |
CONTENTS
1
INTRODUCTION
1
2
FUNDAMENTALS
4
2.1
THE
DRIVING
FORCE:
CHEMICAL
POTENTIAL
AND
SUPERSATURATION
4
2.2
NUCLEATION:
THE
BIRTH
OF
A
CRYSTAL
10
2.2.1
HOMOGENEOUS
NUCLEATION
11
2.2.2
HETEROGENEOUS
NUCLEATION
14
2.2.3
SURFACE
OR
SECONDARY
NUCLEATION
20
2.2.4
ATTRITION
INDUCED
NUCLEATION
21
2.3
CRYSTAL
GROWTH:
FROM
NUCLEUS
TO
CRYSTAL
27
2.3.1
DIFFUSION
CONTROLLED
GROWTH
28
2.3.2
INTEGRATION
CONTROLLED
GROWTH
29
2.3.3
GENERAL
CHARACTERIZATION
OF
CRYSTAL
GROWTH
RATES
31
2.4
METASTABLE
ZONE
AND
INDUCTION
TIME:
WHAT
WE
STILL
CANNOT
SEE!
32
2.5
AGGLOMERATION
-
HOW
PARTICLES
STICK
TOGETHER
37
3
OPERATIONAL
MODES
AND
CONTROL
OF
COOLING
CRYSTALLIZERS
40
4
OPTIMAL
PROCESS
MANAGEMENT
53
4.1
COOLING
OR
EVAPORATION
CRYSTALLIZATION?
53
4.2
OPTIMAL
SUPERSATURATION
FOR
COARSE
CRYSTALLINE
PRODUCTS
57
5
INNOVATIVE
SUPERSATURATION
MEASURING
SYSTEM
64
5.1
MEASUREMENT
METHOD
64
5.2
SENSOR
68
5.2.1
INTERDIGITAL
TRANSDUCER
(IDT)
68
5.2.2
SURFACE
ACOUSTIC
WAVE
(SAW)
69
5.2.3
PELTIER
ELEMENT
70
5.2.4
SENSOR
SETUP
71
6
EXPERIMENTS
82
6.1
MEASUREMENT
SIGNALS
82
6.2
BEAKER
GLASS
EXPERIMENTS
87
6.3
CRYSTALLIZER
EXPERIMENTS
94
6.4
FURTHER
EXPERIMENTS
WITH
OTHER
SYSTEMS
102
7
THEORETICAL
APPROACH
108
7.1
MODEL
OF
METASTABILITY
108
7.2
SIMPLIFIED
CRITERIA
FOR
THE
ESTIMATION
OF
THE
FIELD
OF
APPLICATION
117
CONTENTS
8
CONCLUSION
125
9
NOTATION
127
10
REFERENCES
132
11
APPENDIX
141
11.1
COMPARISON
OF
THE
DEPENDENCE
OF
THE
PRE-EXPONENTIAL
FACTOR
ON
SUPERSATURATION
S
141
11.2
CONVERSION
OF
THE
RATE
BHET
OF
HETEROGENEOUS
NUCLEATION
INTO
THE
RATE
BHOM
OF
HOMOGENEOUS
NUCLEATION
FOR
THE
MODELS
OF
SCHUBERT
AND
HEYER
142
11.3
SYSTEM
PROPERTIES
144
11.4
EXPERIMENTAL
RESULTS
145
11.5
CALCULATED
HETEROGENEOUS
NUCLEATION
RATES
B
HET
152
11.6
CALCULATION
OF
O
MET
FOR
PRIMARY
HETEROGENEOUS
NUCLEATION
153
11.7
FURTHER
POSSIBILITIES
FOR
IMPROVEMENT
AND
ADDITIONAL
SENSOR
CONCEPTS
154
11.7.1
DESIGN
IMPROVEMENT
OF
THE
EXISTING
SENSOR
154
11.7.2
SENSOR
FOR
SYSTEMS
WITH
FLAT
SOLUBILITY
CURVES
155
11.7.3
EQUILIBRIUM
STATE
SENSOR
158 |
| any_adam_object | 1 |
| author | Löffelmann, Michael 1970- |
| author_GND | (DE-588)12444511X |
| author_facet | Löffelmann, Michael 1970- |
| author_role | aut |
| author_sort | Löffelmann, Michael 1970- |
| author_variant | m l ml |
| building | Verbundindex |
| bvnumber | BV017168568 |
| classification_tum | CIT 210d |
| ctrlnum | (OCoLC)76487588 (DE-599)BVBBV017168568 |
| discipline | Chemie-Ingenieurwesen |
| format | Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV017168568 |
| illustrated | Illustrated |
| indexdate | 2024-08-17T00:41:52Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010351498 |
| oclc_num | 76487588 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-91G DE-BY-TUM DE-12 |
| owner_facet | DE-91 DE-BY-TUM DE-91G DE-BY-TUM DE-12 |
| physical | 166 S. Ill., graph. Darst. |
| publishDate | 2002 |
| publishDateSearch | 2002 |
| publishDateSort | 2002 |
| record_format | marc |
| spelling | Löffelmann, Michael 1970- Verfasser (DE-588)12444511X aut Optimal operation of batch cooling crystallizers Michael Löffelmann 2002 166 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier München, Techn. Univ., Diss., 2002 Chargenbetrieb (DE-588)4147586-0 gnd rswk-swf Übersättigung (DE-588)4260615-9 gnd rswk-swf Prozessoptimierung (DE-588)4176074-8 gnd rswk-swf Kühlungskristallisation (DE-588)4298107-4 gnd rswk-swf Sensor (DE-588)4038824-4 gnd rswk-swf Prozessregelung (DE-588)4222919-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Kühlungskristallisation (DE-588)4298107-4 s Chargenbetrieb (DE-588)4147586-0 s Prozessoptimierung (DE-588)4176074-8 s Prozessregelung (DE-588)4222919-4 s Übersättigung (DE-588)4260615-9 s Sensor (DE-588)4038824-4 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010351498&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Löffelmann, Michael 1970- Optimal operation of batch cooling crystallizers Chargenbetrieb (DE-588)4147586-0 gnd Übersättigung (DE-588)4260615-9 gnd Prozessoptimierung (DE-588)4176074-8 gnd Kühlungskristallisation (DE-588)4298107-4 gnd Sensor (DE-588)4038824-4 gnd Prozessregelung (DE-588)4222919-4 gnd |
| subject_GND | (DE-588)4147586-0 (DE-588)4260615-9 (DE-588)4176074-8 (DE-588)4298107-4 (DE-588)4038824-4 (DE-588)4222919-4 (DE-588)4113937-9 |
| title | Optimal operation of batch cooling crystallizers |
| title_auth | Optimal operation of batch cooling crystallizers |
| title_exact_search | Optimal operation of batch cooling crystallizers |
| title_full | Optimal operation of batch cooling crystallizers Michael Löffelmann |
| title_fullStr | Optimal operation of batch cooling crystallizers Michael Löffelmann |
| title_full_unstemmed | Optimal operation of batch cooling crystallizers Michael Löffelmann |
| title_short | Optimal operation of batch cooling crystallizers |
| title_sort | optimal operation of batch cooling crystallizers |
| topic | Chargenbetrieb (DE-588)4147586-0 gnd Übersättigung (DE-588)4260615-9 gnd Prozessoptimierung (DE-588)4176074-8 gnd Kühlungskristallisation (DE-588)4298107-4 gnd Sensor (DE-588)4038824-4 gnd Prozessregelung (DE-588)4222919-4 gnd |
| topic_facet | Chargenbetrieb Übersättigung Prozessoptimierung Kühlungskristallisation Sensor Prozessregelung Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010351498&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT loffelmannmichael optimaloperationofbatchcoolingcrystallizers |