Newer methods of volumetric chemical analysis:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York
van Nostrand
1938
|
| Ausgabe: | 2. print. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIII, 268 S. |
Internformat
MARC
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| 050 | 0 | |a QD111 B83 2nd 1938 | |
| 130 | 0 | |a Neuere maßanalytische Methoden | |
| 245 | 1 | 0 | |a Newer methods of volumetric chemical analysis |c Wilhelm Böttger, ed. |
| 250 | |a 2. print. | ||
| 264 | 1 | |a New York |b van Nostrand |c 1938 | |
| 300 | |a XIII, 268 S. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Volumetric analysis | |
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Datensatz im Suchindex
| _version_ | 1804129785160400896 |
|---|---|
| adam_text | CONTENTS
PART PAGE
I. ELIMINATION OF THE TITRATION ERROR IN ACIDI-
METRIC AND ALKALIMETRIC TITRATIONS
BY DR. ERNA BRENNECKE,
ASSISTANT AT THE FRESENIUS CHEMI
CAL LABORATORY, WIESBADEN, GERMANY
GENERAL
CONSIDERATIONS OF THE BEHAVIOR
OF ACIDIMETRIC
INDICATORS
3
THE TRANSITION RANGE 3
THE INDICATOR CONCENTRATION 5
THE NEUTRAL SALT EFFECT 5
THE EFFECT OF ALCOHOL 7
GENERAL
CONSIDERATIONS
OF THE USE OF INDICATORS
IN ACIDIMETRY
AND ALKALIMETRY 8
THE APPLICATION
OF INDICATOR
CORRECTIONS
10
THE TITRATION OF SODIUM CARBONATE WITH HYDROCHLORIC ACID 11
THE TITRATION OF SULFURIC ACID WITH HYDROXIDES AND VICE VERSA 12
THE TITRATION OF BORAX 14
THE USE OF INDICATOR CORRECTIONS UNDER MORE SPECIAL TITRATION CON- .
DITIONS 15
THE ACIDIMETRIC DETERMINATION OF OXALIC ACID 15
THE TITRATION IN ALCOHOLIC SOLUTIONS 16
THE MICRO-TITRATION OF STRONG ACIDS . 17
MIXED
INDICATORS
18
FLUORESCENT AND
TURBIDITY
INDICATORS
19
BIBLIOGRAPHY
20
II. CERIC SULFATE AS A VOLUMETRIC OXIDIZING
AGENT
BY DR. N. HOWELL FURMAN,
PROFESSOR OF CHEMISTRY,
PRINCETON UNIVERSITY, PRINCETON,
N. J.
INTRODUCTION
27
PREPARATION
OF CERIC
SULFATE SOLUTIONS
27
PREPARATION FROM PURE EERIE SALT : 27
VII
HTTP://D-NB.INFO/1037804287
VIII
CONTENTS
PART PAGE
PREPARATION FROM EERIE OXIDE, CE0
2
28
PREPARATION FROM COMMERCIAL CEROUS OXALATE 28
STANDARDIZATION OF CERIC SULFATE SOLUTIONS
29
ARSENIOUS OXIDE AS PRIMARY STANDARD 29
SODIUM OXALATE AS PRIMARY STANDARD 30
ELECTROLYTIC IRON AS PRIMARY STANDARD 31
THE STABILITY OF CERIC SULFATE SOLUTIONS 31
STABILITY AT THE BOILING POINT 32
INDICATORS FOR TITRATIONS WITH CERIC SULFATE
32
DETERMINATIONS WITH CERIC SULFATE SOLUTION
35
INORGANIC SUBSTANCES
35
ANTIMONY P. 35*ARSENIC P. 36*LEAD PEROXIDE (INDIRECT)
P. 36*CALCIUM (INDIRECT) P. 36*CHROMIUM (INDIRECT)
P. 36*IRON P. 37*FERROCYANIDE P. 38*IODIDE P. 38*
POTASSIUM (INDIRECT) P. 39*CUPROUS SALT P. 39*MOLYB
DENUM P. 39^*SODIUM (INDIRECT) P. 40*NITRITE P. 40*
MERCUROUS SALT P. 41*HYDRAZOIC ACID (HN
3
) AND AZIDES
P. 41*TELLUROUS ACID P. 42*THALLIUM P. 42*THIOSULFATE
P. 43*TITANIUM P. 43*URANIUM P. 43*VANADIUM*
P. 44*HYDROGEN PEROXIDE P. 44*TIN P. 45
ORGANIC MATERIALS
45
HYDROQUINONE P. 45*ORGANIC ACIDS P. 45*OXALIC ACID
P. 46*PYRUVIC ACID P. 47*REDUCING SUGARS P. 47
BIBLIOGRAPHY
48
III. ALKALINE PERMANGANATE SOLUTION AS VOLU
METRIC OXIDIZING AGENT
BY DR. HELLMUTH STAMM,
ASSISTANT AT THE CHEMICAL INSTI
TUTE OF THE UNIVERSITY OF HALLE, GERMANY
EXPERIMENTAL LIMITS OF THE OLDER METHODS OF PERMANGANATE
TITRATION
55
PRINCIPLE AND SCOPE OF THE NEW PROCEDURE
. . 56
CONTENTS IX
PART PAGE
GENERAL
DISCUSSION
OP THE METHOD OF CARRYING OUT THE NEW
PROCEDURE
58
WORKING
DIRECTIONS 61
PROCEDURE
I
: BACK-TITRATION WITH FORMATE IN ALKALINE MEDIUM....
61
PROCEDURE
II
: BACK-TITRATION WITH OXALIC ACID IN ACID MEDIUM...
63
DETERMINATION OF THE BLANK CONSUMPTION 63
TITRATION PROCEDURE 64
EXAMPLES OP THE APPLICATION
OF THE METHOD
64
IV. IODATE AND BROMATE METHODS, INCLUDING MAN-
CHOT S BROMOMETRIC METHOD
BY DR. RUDOLF LANG,
PRIVATDOZENT AT THE TECHNICAL HIGH
SCHOOL, BRIINN, CZECHOSLOVAKIA
IODATE
METHODS
69
METHODS
BASED
ON THE REDUCTION
OP IODATE
TO IODIDE
AND FTTEE
IODINE 69
METHODS BASED
ON THE REDUCTION
OF IODATE TO POSITIVE
UNIVALENT
IODINE
70
THE ANDREWS
METHOD
71
THE IODINE MONOCHLORIDE PROCEDURE 71
THE IODINE BROMIDE PROCEDURE 73
LANG S IODINE
CYANIDE
METHOD
76
BERG S IODO-ACETONE
METHOD
79
TITRATIONS IN THE PRESENCE OF MERCURIC SALT 81
PARTICULAR
DETERMINATIONS
82
IODIDE AND IODINE P. 83*TWO OXIDATION STAGES OF IODINE P. 83*
DIFFICULTLY SOLUBLE IODIDES P. 84*IODIDE AND BROMIDE IN THE PRES
ENCE OF EACH OTHER P. 85*CYANIDE P. 85*THIOCYANATE P. 85*
THIOCYANATE AND IODIDE TOGETHER P. 86*THIOCYANATE AND
CYANIDE TOGETHER P. 86*FERROCYANIDE P. 87*THIOCYANATE,
CYANIDE AND FERROCYANIDE TOGETHER P. 87*HYDROGEN PEROXIDE
P. 88*HYDRAZINE AND ITS DERIVATIVES P. 88*HYDRAZINE AND
AZIDE P. 88*HYDRAZINE AND HYDROXYLAMINE TOGETHER P. 89*
SELENIUM P. 89*SULFUR COMPOUNDS P. 90*HYPOPHOSPHOROUS
AND PHOSPHOROUS ACIDS P. 90*CHLORATE, CHROMATE AND VANADATE
X
CONTENTS
PART PAGE
P. 90*ARSENIOUS AND ANTIMONOUS SALT P. 91*ARSINE AND FREE
ARSENIC P. 91*TIN P. 92*TIN AND ANTIMONY TOGETHER P. 92*
COPPER P. 93*IRON P. 94*FERROUS AND ARSENIOUS SALTS TO
GETHER P. 94*TITANIUM, VANADIUM, MOLYBDENUM, TUNGSTEN,
URANIUM P. 94*THALLIUM P. 95*MERCURY P. 95*ZINC P. 96*
CADMIUM AND BISMUTH P. 96*ORGANIC COMPOUNDS P. 97
BROMATE METHODS
98
PARTICULAR DETERMINATIONS
101
ARSENIC AND ANTIMONY P. 101*ARSINE P. 103*TIN P. 103*ANTI
MONY AND TIN TOGETHER P. 103*ARSENIC, ANTIMONY AND TIN IN
THE PRESENCE OF EACH OTHER P. 104*COPPER AND BISMUTH*
P. 105*IRON P. 105*THALLIUM P. 106*HYDRAZINE P. 107*
HYDROXYLAMINE P. 107*HYDRAZINE AND HYDROXYLAMINE TO
GETHER P. 107*NITRITE P. 107*SELENIUM DIOXIDE P. 107*SULFUR
COMPOUNDS P. 108*CARO S ACID, PERSULFURIC ACID AND HYDRO
GEN PEROXIDE TOGETHER P. 109*IODIDE, BROMIDE AND CHLORIDE
P. 109
ORGANIC COMPOUNDS 110
OXIDIZING ACTIONS 110
ADDITION REACTIONS ILL
SUBSTITUTION REACTIONS ILL
PHENOLS AND AROMATIC AMINES P. ILL*O-(8)-OXYQUINOLINE
P. 113*ANTHRANILIC ACID P. 114*FURFUROL P. 115
MANCHOT S BROMOMETRIC METHOD
116
PARTICULAR DETERMINATIONS
117
ANTIMONY AND TIN P. 117*IRON P. 117*CHLORIDE OF LIME,
SODIUM HYPOCHLORITE, CHLORINE WATER P. 117*PYROLUSITE, LEAD
DIOXIDE, BICHROMATE, PERMANGANATE P. 118*OZONE P. 118*
SULFUROUS ACID, HYDROGEN SULFIDE AND THIOSULFATE P. 118*
PHOSPHOROUS AND HYPOPHOSPHOROUS ACIDS P. 119*NITRITE
P. 119*AMMONIA P. 119*UREA P. 119*HYDROGEN PEROXIDE
P.
120*THIOCYANATE, CYANIDE, FERROCYANIDE P. 120*FORMIC
ACID P. 120*ORGANIC ADDITION AND SUBSTITUTION REACTIONS
P. 120
BIBLIOGRAPHY
121
CONTENTS XI
PART PAGE
V. CHROMOUS SOLUTIONS AS VOLUMETRIC REDUCING
AGENTS
BY DR. ERNA BRENNECKE
GENERAL
CONSIDERATIONS
131
CHARACTERISTIC PROPERTIES OF CHROMOUS SOLUTIONS 131
THE PREPARATION AND STABILITY OF CHROMOUS SOLUTIONS 133
APPARATUS AND PROCEDURE 136
THE STANDARDIZATION OF CHROMOUS SOLUTIONS 138
SPECIAL
SECTION
139
DETERMINATION OF COPPER : 139
DETERMINATION OF MERCURY 142
DETERMINATION OF SILVER 145
DETERMINATION OF BICHROMATE 146
DETERMINATION OF TIN 147
THE DETERMINATION
OF SEVERAL
METALS BY A SINGLE TITRATION
149
BIBLIOGRAPHY
150
VI. OXIDATION-REDUCTION INDICATORS
BY DR. ERNA BRENNECKE
GENERAL
CONSIDERATIONS
155
GENERAL CHARACTERIZATIOIJ OF OXIDATION-REDUCTION INDICATORS 156
SECTION I. DIPHENYLAMINE, DIPHENYLBENZIDINE, DIPHENYLAMINE
SULFONIC
ACID
159
GENERAL PROPERTIES OF DIPHENYLAMINE AND ITS DERVATIVES ....... 159
DIPHENYLAMINE 159
DIPHENYLBENZIDINE 162
DIPHENYLAMINE-P-SULFONIC ACID 162
USE OF DIPHENYLAMINE AND ITS DERIVATIVES IN OXIDIMETRIC VOLU
METRIC ANALYSIS 163
THE TITRATION OF FERROUS SALT WITH POTASSIUM BICHROMATE AND
VICE VERSA 163
INDICATOR: DIPHENYLAMINE 163
PROCEDURE P. 164*BEHAVIOR OF THE INDICATOR P. 166*THE
USE OF DIPHENYLAMINE IN TITRATION OF IRON WITH BICHRO
MATE IN SPECIAL CASES P. 168
XII CONTENTS
PART PAGE
INDICATOR: DIPHENYLBENZIDINE 169
INDICATOR: DIPHENYLAMINE SULFONIC ACID 169
THE TITRATION OF VANADIC ACID WITH FERROUS SULFATE SOLUTION . . . 171
DIPHENYLAMINE P. 172*DIPHENYLBENZIDINE P. 172*DI
PHENYLAMINE SULFONIC ACID P. 174*COMPARISON OF THE
VARIOUS INDICATOR CORRECTIONS P. 174
THE TITRATION OF ZINC WITH POTASSIUM FERROCYANIDE 176
PROCEDURE P. 176*BEHAVIOR OF THE INDICATOR P. 178
FURTHER POSSIBILITIES OF USING DIPHENYLAMINE, DIPHENYLBENZI
DINE AND DIPHENYLAMINE SULFONATE AS INDICATORS IN REDOX
TITRATIONS 178
TITRATIONS WITH BICHROMATE, FERROCYANIDE AND VANADATE AS
OXIDIZING AGENTS . 178
TITRATIONS WITH EERIE SALT AS OXIDIZING AGENT . 179
TITRATIONS WITH PERMANGANATE 180
SECTION II. ERIOGLAUCIN, ERIOGREEN, SETOGLAUCIN AND RELATED
COMPOUNDS
181
GENERAL PROPERTIES OF THE TRIARYLMETHANE REDOX INDICATORS 181
USE OF REDOX INDICATORS OF THE TRIARYLMETHANE GROUP 184
THE TITRATION OF IRON WITH PERMANGANATE ^ 184
THE TITRATION OF POTASSIUM FERROCYANIDE WITH PERMANGANATE. . 186
THE TITRATION OF FERROUS SULFATE WITH EERIE SULFATE 187
SECTION
III. TRI-ORTHO-PHENANTI-IROLLNE-FERROUS SULFATE
187
GENERAL PROPERTIES OF TRI-O-PHENANTHROLINE-FERROUS SULFATE 188
THE USE OF TRI-O-PHENANTHROLINE-FERROUS SULFATE 189
THE TITRATION OF IRON WITH BICHROMATE 189
THE TITRATION OF IRON WITH POTASSIUM PERMANGANATE 190
TITRATIONS WITH EERIE SOLUTIONS 191
BIBLIOGRAPHY
192
VII. ADSORPTION INDICATORS FOR PRECIPITATION
TITRATIONS
BY DR. KASIMIR FAJANS,
PROFESSOR AT THE UNIVERSITY OF
MICHIGAN, ANN ARBOR, MICHIGAN
INTRODUCTION
203
DEVELOPMENT OF THE METHOD 203
PRINCIPLE OF THE METHOD 204
CONTENTS XM
PART PAGE
THEORY
OF THE ADSORPTION
INDICATORS
206
GENERAL CONSIDERATIONS CONCERNING THE ADSORPTION OF IONS ON POLAR
ADSORBENTS 206
COMPARISON OF THE ADSORBABILITY OF DYESTUFFS 210
COMPARISON OF THE ADSORBABILITY OF THE HALIDE IONS 212
THE SURFACE DEVELOPMENT OF THE ADSORBENTS ACTIVE IN THE TITRATION,
AND THE QUANTITIES OF INDICATOR TO BE EMPLOYED 214
GENERAL CONSIDERATION OF THE COURSE OF TITRATION CURVES WITH ADSORP
TION INDICATORS 215
SEVERAL EXAMPLES OF THE DISPLACEMENT OF DYESTUFF IONS BY IONS OF
LIKE SIGN 220
THE EFFECT OF AN EXCESS OF AN OPPOSITELY CHARGED ION ON THE ADSORP
TION OF THE INDICATOR 222
DETERMINATION OF IODIDE IN THE PRESENCE OF CHLORIDE 223
THE COLOR CHANGE ACCOMPANYING ADSORPTION 226
THEORY OF THE BASIC ADSORPTION INDICATORS AND THE SPECIAL BEHAVIOR
OF PHENOSAFRANIN AS INDICATOR IN ARGENTOMETRIC TITRATION 230
TITRATIONS
WITH ADSORPTION
INDICATORS
233
GENERAL CONSIDERATIONS 233
SURVEY OF THE METHODS TESTED IN PRACTICE 235
BEHAVIOR OF SOME INDICATORS 240
FLUORESCEIN AND ITS HALOGENATED DERIVATIVES 240
FLUORESCEIN * 242
DICHLOR (R) FLUORESCEIN 243
BOSIN 244
TARTRAZINE 244
PHENOSAFRANIN 245
RHODAMINE 246
BIBLIOGRAPHY
247
INDEX
251
|
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| id | DE-604.BV016451696 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T19:10:39Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010172324 |
| oclc_num | 596967 |
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| owner | DE-91 DE-BY-TUM |
| owner_facet | DE-91 DE-BY-TUM |
| physical | XIII, 268 S. |
| publishDate | 1938 |
| publishDateSearch | 1938 |
| publishDateSort | 1938 |
| publisher | van Nostrand |
| record_format | marc |
| spelling | Neuere maßanalytische Methoden Newer methods of volumetric chemical analysis Wilhelm Böttger, ed. 2. print. New York van Nostrand 1938 XIII, 268 S. txt rdacontent n rdamedia nc rdacarrier Volumetric analysis Maßanalyse (DE-588)4037863-9 gnd rswk-swf Maßanalyse (DE-588)4037863-9 s 1\p DE-604 Böttger, Carl Wilhelm 1871-1949 Sonstige (DE-588)116226404 oth DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010172324&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Newer methods of volumetric chemical analysis Volumetric analysis Maßanalyse (DE-588)4037863-9 gnd |
| subject_GND | (DE-588)4037863-9 |
| title | Newer methods of volumetric chemical analysis |
| title_alt | Neuere maßanalytische Methoden |
| title_auth | Newer methods of volumetric chemical analysis |
| title_exact_search | Newer methods of volumetric chemical analysis |
| title_full | Newer methods of volumetric chemical analysis Wilhelm Böttger, ed. |
| title_fullStr | Newer methods of volumetric chemical analysis Wilhelm Böttger, ed. |
| title_full_unstemmed | Newer methods of volumetric chemical analysis Wilhelm Böttger, ed. |
| title_short | Newer methods of volumetric chemical analysis |
| title_sort | newer methods of volumetric chemical analysis |
| topic | Volumetric analysis Maßanalyse (DE-588)4037863-9 gnd |
| topic_facet | Volumetric analysis Maßanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010172324&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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