Introduction to thermal analysis: techniques and applications
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Dordrecht [u.a.]
Kluwer Acad. Publ.
2001
|
| Ausgabe: | 2. ed. |
| Schriftenreihe: | Hot topics in thermal analysis and calorimetry
1 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XI, 264 S. Ill., graph. Darst. |
| ISBN: | 1402002114 1402004729 |
Internformat
MARC
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| 245 | 1 | 0 | |a Introduction to thermal analysis |b techniques and applications |c ed. by Michael E. Brown |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a Dordrecht [u.a.] |b Kluwer Acad. Publ. |c 2001 | |
| 300 | |a XI, 264 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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| 490 | 1 | |a Hot topics in thermal analysis and calorimetry |v 1 | |
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Datensatz im Suchindex
| _version_ | 1804129675412242432 |
|---|---|
| adam_text | Titel: Introduction to thermal analysis
Autor: Brown, Michael E.
Jahr: 2001
CONTENTS
Preface to the First Edition, Chapman Hall, London, 1988.................................ix
About the First Edition of this Book............................................................................÷
Preface to the Second Edition.....................................................................................xi
1. INTRODUCTION
1.1 Definition and History.......................................... 1
1.2 Thermal Analysis Instruments.................................... 4
References ......................................................... 11
2. THERMAL EVENTS
2.1 Introduction................................................. 13
2.2 The Solid State............................................... 13
2.3 Reactions of Solids ........................................... 14
2.4 Decomposition of Solids....................................... 15
2.5 Reaction with the Surrounding Atmosphere ........................ 16
2.6 Solid-Solid Interactions........................................ 16
References ......................................................... 17
3. THERMOGRAVIMETRY (TG)
3.1 Introduction................................................. 19
3.2 The Balance................................................. 19
3.3 Heating the Sample ........................................... 21
3.4 The Atmosphere.............................................. 24
3.5 The Sample ................................................. 26
3.6 Temperature Measurement ..................................... 26
3.7 Temperature Control .......................................... 28
3.8 Sample Controlled Thermal Analysis (SCTA) ...................... 29
3.9 Calibration.................................................. 36
3.10 Presentation of TG Data ....................................... 37
3.11 Automation of TG............................................ 40
3.12 Thermomagnetometry (TM) .................................... 43
3.13 Interpretation of TG and DTG Curves............................. 44
3.14 Applications of Thermogravimetry (TG)........................... 46
3.15 Applications of Thermomagnetometry (TM)........................ 49
References ......................................................... 52
í
VI
4. DIFFERENTIAL THERMAL ANALYSIS (DTA) AND
DIFFERENTIAL SCANNING CALORIMETRY (DSC)
4.1 Classical DTA............................................... 55
4.2 Calorimetric DTA or heat-flux DSC ............................. 57
4.3 Differential Scanning Calorimetry (DSC).......................... 57
4.4 Comparison of the Principles of DTA and DSC..................... 58
4.5 Modulated Temperature Differential Scanning Calorimetry (mt-DSC) ... 61
4.6 Sample Containers and Sampling ................................ 64
4.7 Quantitative Aspects of DTA and DSC curves...................... 65
4.8 Interpretation of DSC and DTA curves............................ 76
4.9 Determination of Phase Diagrams................................ 78
4.10 General Applications of DSC and DTA ........................... 80
4.11 Automation ................................................. 88
References ......................................................... 89
5. THERMOPTOMETRY
5.1 Introduction................................................. 91
5.2 Thermomicroscopy ........................................... 92
5.3 Thermophotometry............................................ 92
5.4 Thermoluminescence.......................................... 94
5.5 Combination of Thermomicroscopy with DSC (or DTA).............. 95
5.6 Combination of Thermomicroscopy with TG ....................... 96
5.7 Other techniques combined with Thermomicroscopy................. 97
5.8 Some Applications of the techniques of Thermoptometry ............. 97
5.9 Electron Microscopy.......................................... 98
5.10 Micro Thermal Analysis ....................................... 99
References........................................................ 102
6. THERMOMECHANOMETRY
6.1 Definitions and scope ........................................ 105
6.2 Thermodilatometry........................................... 106
6.3 Thermomechanical Analysis (TMA)............................. 112
6.4 Dynamic Mechanical Analysis (DMA)........................... 120
References ........................................................ 127
7. COMBINATION OF THERMAL ANALYSIS TECHNIQUES
7.1 Principles.................................................. 129
7.2 Equipment ................................................. 130
References ........................................................ 137
Vil
8. EVOLVED GAS ANALYSIS (EGA)
8.1 Basic Principles............................................. 139
8.2 Evolved Gas Detection (EGD) ................................. 139
8.3 Mass Spectrometry (MS)...................................... 141
8.4 Fourier Transform Infrared (FTIR) Spectroscopy................... 143
8.5 Gas Chromatography (GC) .................................... 144
8.6 Special-purpose Detectors..................................... 147
8.7 Applications of EGA......................................... 148
8.8 Pulsed Gas Thermal Analysis .................................. 152
References........................................................ 154
9. LESS-COMMON TECHNIQUES
9.1 Introduction................................................ 157
9.2 Emanation Thermal Analysis (ETA)............................. 157
9.3 Thermosonimetry (TS) and Thermoacoustimetry ................... 164
9.4 Thermoelectrometry (or Thermoelectrical Analysis, TEA)............ 172
9.5 Miscellaneous Techniques..................................... 177
References ........................................................ 178
10. REACTION KINETICS FTtOM THERMAL ANALYSIS
10.1 Introduction................................................ 181
10.2 Heterogeneous reactions ...................................... 182
10.3 Formulation of the problem.................................... 183
10.4 Kinetic Analysis of Isothermal Data............................. 194
10.5 Kinetic Analysis of Nonisothermal Data.......................... 195
10.6 The influences of various parameters on the shapes of theoretical thermal
analysis Curves............................................. 200
10.7 The Compensation Effect ..................................... 204
10.8 Complex reactions........................................... 205
10.9 Prediction of Kinetic Behaviour................................ 206
10.10 Kinetic Standards............................................ 206
10.11 Kinetic Test Data............................................ 207
10.12 Publication of Kinetic Results.................................. 209
10.13 Conclusions................................................ 209
References........................................................ 211
11. PURITY DETERMINATION USING DSC
11.1 Introduction................................................ 215
11.2 Phase equilibria............................................. 217
11.3 The DSC melting curve....................................... 219
Ð.4 Corrections................................................. 221
11.5 Step methods............................................... 224
Ð.6 Conclusions................................................ 224
References........................................................ 226
Vill
12. CONCLUSIONS
12.1 The Range of Thermal Analysis ................................ 229
12.2 The Future of Thermal Analysis ................................ 229
References ........................................................ 230
APPENDICES
A. LITERATURE............................................. 231
A.I Books..................................................... 231
A.2 Conference Proceedings ...................................... 235
A.3 Journals................................................... 236
A.4 Nomenclature............................................... 237
A.5 Manufacturer s Literature ..................................... 237
B. MAJOR SUPPLIERS OF THERMAL ANALYSIS EQUIPMENT . 238
B.I Choosing Thermal Analysis Equipment .......................... 238
B.2 Major Suppliers of Thermal Analysis Equipment................... 238
C. DATA PROCESSING IN THERMAL ANALYSIS .............. 241
C.I Introduction................................................ 241
C.2 Data processing............................................. 241
C.3 Spreadsheets and database packages............................. 242
C.4 Algorithms................................................. 242
References ........................................................ 244
D. INTRODUCTORY EXPERIMENTS.......................... 245
D.I Differential Scanning Calorimetry (DSC)......................... 245
D.2 Thermogravimetry (TG)....................................... 246
E. EXAMPLE EXAMINATION QUESTIONS .................... 247
EXPLANATION OF THE SYMBOLS USED IN THE TEXT ............ 251
INDEX.......................................................... 255
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| language | English |
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| series | Hot topics in thermal analysis and calorimetry |
| series2 | Hot topics in thermal analysis and calorimetry |
| spelling | Introduction to thermal analysis techniques and applications ed. by Michael E. Brown 2. ed. Dordrecht [u.a.] Kluwer Acad. Publ. 2001 XI, 264 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Hot topics in thermal analysis and calorimetry 1 Analyse thermique Thermal analysis Thermoanalyse (DE-588)4135675-5 gnd rswk-swf Thermoanalyse (DE-588)4135675-5 s DE-604 Brown, Michael E. 1938- Sonstige (DE-588)129944629 oth Hot topics in thermal analysis and calorimetry 1 (DE-604)BV015009425 1 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010088526&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Introduction to thermal analysis techniques and applications Hot topics in thermal analysis and calorimetry Analyse thermique Thermal analysis Thermoanalyse (DE-588)4135675-5 gnd |
| subject_GND | (DE-588)4135675-5 |
| title | Introduction to thermal analysis techniques and applications |
| title_auth | Introduction to thermal analysis techniques and applications |
| title_exact_search | Introduction to thermal analysis techniques and applications |
| title_full | Introduction to thermal analysis techniques and applications ed. by Michael E. Brown |
| title_fullStr | Introduction to thermal analysis techniques and applications ed. by Michael E. Brown |
| title_full_unstemmed | Introduction to thermal analysis techniques and applications ed. by Michael E. Brown |
| title_short | Introduction to thermal analysis |
| title_sort | introduction to thermal analysis techniques and applications |
| title_sub | techniques and applications |
| topic | Analyse thermique Thermal analysis Thermoanalyse (DE-588)4135675-5 gnd |
| topic_facet | Analyse thermique Thermal analysis Thermoanalyse |
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