Gas chromatographic techniques and applications:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Sheffield
Sheffield Acad. Press [u.a.]
2001
|
| Ausgabe: | 1. publ. |
| Schriftenreihe: | Sheffield analytical chemistry
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 337 S. Ill., graph. Darst. |
| ISBN: | 1841271187 |
Internformat
MARC
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| 245 | 1 | 0 | |a Gas chromatographic techniques and applications |c ed. by Alan J. Handley ... |
| 250 | |a 1. publ. | ||
| 264 | 1 | |a Sheffield |b Sheffield Acad. Press [u.a.] |c 2001 | |
| 300 | |a XIV, 337 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Sheffield analytical chemistry | |
| 650 | 4 | |a Chromatographie en phase gazeuse | |
| 650 | 4 | |a Chromatographie en phase gazeuse - Technique | |
| 650 | 4 | |a Gas chromatography | |
| 700 | 1 | |a Handley, Alan J. |e Sonstige |4 oth | |
| 856 | 4 | 2 | |m GBV Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010081822&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
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Datensatz im Suchindex
| _version_ | 1804129666430140416 |
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| adam_text | GAS CHROMATOGRAPHIE TECHNIQUES AND APPLICATIONS EDITED BY ALAN J.
HANDLEY SEPARATIONS SCIENCE AND SPECTROSCOPY LGC, RUNCORN, UK AND EDWARD
R. ADLARD SCIENTIFIC EDITORIAL CONSULTANT WIRRAL, UK SHEFFIELD ACADEMIC
PRESS CRC PRESS CONTENTS 1 DEVELOPMENTS IN SAMPLE PREPARATION FOR
CAPILLARY GC ANALYSIS 1 PAT SANDRA AND FRANK DAVID 1.1 INTRODUCTION 1
1.2 ENRICHMENT METHODS 2 1.2.1 INTRODUCTION 2 1.2.2 GASEOUS (AIR)
SAMPLES 3 1.2.3 LIQUID (AQUEOUS) SAMPLES 8 1.2.4 SOLID SAMPLES 17 1.3
FRACTIONATION AND CLEAN-UP 26 1.3.1 INTRODUCTION 26 1.3.2 CHEMICAL
METHODS 26 1.3.3 CHROMATOGRAPHIE METHODS 26 1.4 EVAPORATION 30 1.5
DERIVATISATION 31 1.5.1 INTRODUCTION 31 1.5.2 ANALYSIS OF PHENOLS IN
WATER SAMPLES 31 1.5.3 ANALYSIS OF RACEMIC AMINO ACIDS IN BIOLOGICAL
FLUIDS 33 1.6 SOME CASE STUDIES 35 1.6.1 FRACTIONATION OF NITRO-PAHS
FROM AIR PARTICULATES 35 1.6.2 VERSATILE ROBOTIC SYSTEM FOR STATIC
(SPME) AND DYNAMIC (GPE) SAMPLING 37 1.6.3 THE 1999 BELGIAN DIOXIN
CRISIS 41 REFERENCES 50 2 SAMPLE INJEETION SYSTEM S 52 TONY TAYLOR 2.1
INTRODUCTION 52 2.2.1 IMPORTANT CONEEPTS 52 2.2 SPLIT/SPLITLESS
INJEETORS 53 2.2.1 SPLIT/SPLITLESS INLET DESIGN 53 2.2.2 SEPTA 54 2.2.3
SPLIT INJEETION MODE 57 2.2.4 SPLITLESS INJEETION MODE 64 2.3
PACKED-COLUMN INLETS 70 2.3.1 INLET DESIGN 70 2.3.2 INLET PARAMETERS AND
SAMPLE CONSIDERATIONS 71 2.4 CAPILLARY DIRECT INTERFACES 72 2.4.1 INLET
DESIGN 73 2.5 COOL ON-COLUMN INLETS 74 2.5.1 INLET DESIGN 74 2.5.2 INLET
PARAMETERS AND SAMPLE CONSIDERATIONS 77 2.5.3 RETENTION GAP 77 CONTENTS
XI 2.5.4 TEMPERATURE 78 2.5.5 FLOW RATES 78 2.6 PROGRAMMED TEMPERATURE
VAPORISING (PTV) INLETS 78 2.6.1 INLET DESIGN 79 2.6.2 INLET PARAMETERS
AND SAMPLE CONSIDERATIONS 80 2.6.3 TEMPERATURE 82 2.6.4 CARRIER FLOW 82
2.7 AUXILIARY SAMPLING DEVICES 83 2.7.1 GAS AND LIQUID SAMPLING VALVES
83 2.7.2 HEADSPACE AUTOSAMPLERS 85 2.8 CONCLUSIONS 90 REFERENCES 90 3
ADVANCES IN COLUMN TECHNOLOGY 91 ALLEN K. VICKERS AND DEAN ROOD 3.1
INTRODUCTION 91 3.2 MODERN CAPILLARY COLUMNS 92 3.2.1 CAPILLARY COLUMN
MATERIALS 92 3.2.2 COLUMN DIMENSIONS 93 3.2.3 STATIONARY PHASES 93 3.3
EXAMPLES OF SEPARATIONS OF DIFFERENT TYPES OF SAMPLES ON A VARIETY OF
COLUMNS 95 3.3.1 PETROLEUM ANALYSIS 95 3.3.2 ENVIRONMENTAL ANALYSIS 97
3.3.3 LIFE SCIENCES 113 3.3.4 FORENSIC ANALYSIS 121 3.4 CONCLUSION 121
REFERENCES 121 4 DETECTORS FOR QUANTITATIVE GAS CHROMATOGRAPHY 122 PAUL
LARSON 4.1 INTRODUCTION 122 4.2 PNEUMATIC CONTROL 122 4.2.1 FLAME
IONIZATION DETECTOR (FID) 125 4.2.2 NITROGEN PHOSPHORUS DETECTOR (NPD)
131 4.2.3 FLAME PHOTOMETRIE DETECTOR (FPD) 132 4.2.4 OTHER SULFUR
SELECTIVE DETECTORS 134 4.3 GAS PURIFIERS 135 4.4 MINIATURIZATION 136
4.5 DATA PATH CONSIDERATIONS 137 4.6 SUMMARY 138 REFERENCES 139 5
DETECTORS FOR COMPOUND IDENTIFICATION 140 MARK POWELL 5.1 INTRODUCTION
140 5.2 GAS CHROMATOGRAPHY-MASS SPECTROMETRY 140 5.2.1 INTERFACE TYPES
141 5.2.2 IONISATION TECHNIQUES 145 CONTENTS 5.2.3 ANALYSER TYPES 154
5.2.4 SELECTED ION MONITORING 167 5.2.5 GC-MS-MS 168 5.2.6 ISOTOPICALLY
LABELLED SURROGATE STANDARDS 170 5.2.7 APPLICATIONS 171 5.3 GAS
CHROMATOGRAPHY-ATOMIC EMISSION DETECTION 175 5.3.1 THEORY AND
INSTRUMENTATION 175 5.3.2 APPLICATIONS 179 5.4 GAS
CHROMATOGRAPHY-FOURIER TRANSFORM INFRARED SPECTROMETRY 181 5.4.1 THEORY
AND INSTRUMENTATION 181 5.4.2 APPLICATIONS 184 5.5 APPLICATIONS OF
COMBINED TECHNIQUES 186 5.5.1 GC-MS AND GC-AED 186 5.5.2 GC-MS AND
GC-FTIR 187 5.6 FUTURE DIRECTIONS AND DEVELOPMENTS 188 REFERENCES 189
METHOD VALIDATION IN GAS CHROMATOGRAPHY 192 R. D. MCDOWALL 6.1
INTRODUCTION 192 6.2 DEFINITION OF KEY TERMS 192 6.3 EQUIPMENT
QUALIFICATION AND METHOD VALIDATION 193 6.4 EQUIPMENT QUALIFICATION (EQ)
193 6.4.1 THE OVERALL EQ PROCESS 193 6.4.2 EQUIPMENT QUALIFICATION TO
ENSURE EFFICIENT METHOD TRANSFER 194 6.4.3 DESIGN QUALIFICATION (DQ) 194
6.4.4 INSTALLATION QUALIFICATION (IQ) 196 6.4.5 OPERATIONAL
QUALIFICATION (OQ) 196 6.4.6 MODULAR AND HOLISTIC QUALIFICATION 196
6.4.7 PERFORMANCE QUALIFICATION (PQ) 197 6.5 METHOD VALIDATION 197 6.5.1
DOCUMENTING THE METHOD 197 6.5.2 DEFINING THE VALIDATION PARAMETERS TO
MEASURE 197 6.5.3 ANALYTICAL REFERENCE SUBSTANCES 198 6.5.4 SCOPE OF
VALIDATION 198 6.5.5 SPECIFICITY VS SELECTIVITY 198 6.5.6 ACCURACY 200
6.5.7 LIMIT OF DETECTION (LOD) 201 6.5.8 LIMIT OF QUANTIFICATION (LOQ)
201 6.5.9 LINEARITY 202 6.5.10 RANGE 202 6.5.11 ROBUSTNESS 203 6.5.12
ANALYTE STABILITY 203 6.5.13 REVALIDATION OF A METHOD 203 6.5.14
INTERNAL OR EXTERNAL STANDARD METHOD? 204 6.5.15 CALIBRATION METHODS 205
REFERENCES CONTENTS XM 7 FASTER GAS CHROMATOGRAPHY 20 7 CAREL A.
CRAMERS, J. G. M. JANSSEN, M. M. VAN DEURSEN AND J. BEENS 7.1
INTRODUCTION AND SCOPE 207 7.2 OPTIONS FOR INCREASED SPEED OF SEPARATION
207 7.2.1 RESOLUTION NORMALISED CONDITIONS 208 7.2.2 GUIDELINES FOR
RETENTION TIME REDUCTION 212 7.3 PRACTICAL CONSEQUENCES OF FAST GC 227
7.3.1 PRESSURE DROP 228 7.3.2 COLUMN LOADABILITY 228 7.3.3 DETECTION
LIMITS 228 7.3.4 INJECTION BAND WIDTH 229 7.3.5 EXTRACOLUMN BAND
BROADENING 229 7.3.6 TIME CONSTANT FOR DETECTION 229 7.3.7 ELUTION
TEMPERATURE/MAXIMUM COLUMN TEMPERATURE 230 7.3.8 COUPLING TO MASS
SPECTROMETRY 230 7.4 PRACTICAL IMPLEMENTATIONS OF SELECTED OPTIONS FOR
FAST GC 231 7.4.1 NARROW-BORE COLUMNS 231 7.4.2 MULTICAPILLARY COLUMNS
237 7.4.3 FAST TEMPERATURE PROGRAMMING 240 7.4.4 VACUUM OUTLET OPERATION
242 7.4.5 COMPREHENSIVE TWO-DIMENSIONAL GAS CHROMATOGRAPHY 249
REFERENCES 256 8 MULTIDIMENSIONAL AND COMPREHENSIVE MULTIDIMENSIONAL GAS
CHROMATOGRAPHY 260 PHILIP J. MARRIOTT AND RUSSELL M. KINGHORN 8.1
INTRODUCTION 260 8.2 GAS CHROMATOGRAPHY AS ONE DIMENSION IN
MULTIDIMENSIONAL ANALYTICAL METHODS 261 8.3 MULTIDIMENSIONAL SEPARATION
METHODS 261 8.3.1 SCOPE OF CONVENTIONAL CAPILLARY GAS CHROMATOGRAPHY:
RATIONALE FOR HIGHER- RESOLUTION METHODS 262 8.3.2 APPROACHES TO COUPLED
COLUMN METHODS FOR IMPROVED SEPARATION IN GAS CHROMATOGRAPHY 264 8.3.3
CONVENTIONAL MULTIDIMENSIONAL GAS CHROMATOGRAPHY 268 8.4 COMPREHENSIVE
TWO-DIMENSIONAL GAS CHROMATOGRAPHY 278 8.4.1 GENERAL BENEFITS OF GC X GC
281 8.4.2 UNDERSTANDING THE COMPREHENSIVE GAS CHROMATOGRAPHY EXPERIMENT
281 8.4.3 METHODS FOR MODULATION OF PEAK SIGNALS BETWEEN TWO DIMENSIONS
283 8.4.4 ORFHOGONALITY OF SEPARATION 285 8.4.5 PRESENTATION OF GC X GC
DATA 287 8.4.6 APPLICATIONS OFGCXGC 288 8.4.7 STANDARDS AND MASS
SPECTROMETRY STUDIES WITH GC X GC 293 ACKNOWLEDGEMENTS 294 REFERENCES
295 XIV CONTENTS ON-LINE AND AT-LINE GAS CHROMATOGRAPHY 298 TOM LYNCH
9.1 INTRODUCTION 298 9.2 WHY DO WE NEED PROCESS ANALYSIS? 299 9.2.1
ON-LINE, AT-LINE OR CENTRAL LABORATORY? 299 9.3 TRENDS AND RECENT
DEVELOPMENTS IN PROCESS GAS CHROMATOGRAPHY 301 9.4 RECENT DEVELOPMENTS
IN CONVENTIONAL ON-LINE PROCESS GAS CHROMATOGRAPHY INSTRUMENTATION 303
9.4.1 THE APPLICATION OF LIVE SWITCHING TECHNIQUES 304 9.4.2 THE
DEVELOPMENT OF PLUG-AND-PLAY GAS CHROMATOGRAPHY HARDWARE 307 9.4.3
PARALLEL CHROMATOGRAPHY 309 9.5 THE DEVELOPMENT OF GAS
CHROMATOGRAPH-BASED TRANSMITTER INSTRUMENTATION 316 9.6 THE APPLICATION
OF LABORATORY GAS CHROMATOGRAPH INSTRUMENTS AS ON-LINE PROCESS ANALYSIS
INSTRUMENTS 318 9.7 THE MICRO GAS CHROMATOGRAPH 322 9.8 RECENT
DEVELOPMENTS IN AT-LINE GAS CHROMATOGRAPHY 324 9.8.1 WHY DO WE NEED
AT-LINE GAS CHROMATOGRAPHY? 324 9.8.2 WHAT ARE AT-LINE GAS
CHROMATOGRAPHS? 325 9.8.3 AT-LINE GAS CHROMATOGRAPHY DEVELOPMENT IN BP
AMOCO 325 9.8.4 THE BENEFITS OF AT-PLANT CHROMATOGRAPHY 326 9.8.5 THE
CURRENT STATUS OF AT-LINE GAS CHROMATOGRAPHY 327 9.9 FUTURE DEVELOPMENTS
IN PROCESS GAS CHROMATOGRAPHY 329 9.9.1 WHAT WILL DRIVE NEW
DEVELOPMENTS? 329 9.9.2 THE FUTURE FOR ON-LINE GAS CHROMATOGRAPHY 330
9.9.3 THE FUTURE FOR AT-LINE GAS CHROMATOGRAPHY 332 ACKNOWLEDGEMENTS 333
REFERENCES 333 INDEX 334
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| illustrated | Illustrated |
| indexdate | 2024-07-09T19:08:46Z |
| institution | BVB |
| isbn | 1841271187 |
| language | English |
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| publisher | Sheffield Acad. Press [u.a.] |
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| spelling | Gas chromatographic techniques and applications ed. by Alan J. Handley ... 1. publ. Sheffield Sheffield Acad. Press [u.a.] 2001 XIV, 337 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Sheffield analytical chemistry Chromatographie en phase gazeuse Chromatographie en phase gazeuse - Technique Gas chromatography Handley, Alan J. Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010081822&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Gas chromatographic techniques and applications Chromatographie en phase gazeuse Chromatographie en phase gazeuse - Technique Gas chromatography |
| title | Gas chromatographic techniques and applications |
| title_auth | Gas chromatographic techniques and applications |
| title_exact_search | Gas chromatographic techniques and applications |
| title_full | Gas chromatographic techniques and applications ed. by Alan J. Handley ... |
| title_fullStr | Gas chromatographic techniques and applications ed. by Alan J. Handley ... |
| title_full_unstemmed | Gas chromatographic techniques and applications ed. by Alan J. Handley ... |
| title_short | Gas chromatographic techniques and applications |
| title_sort | gas chromatographic techniques and applications |
| topic | Chromatographie en phase gazeuse Chromatographie en phase gazeuse - Technique Gas chromatography |
| topic_facet | Chromatographie en phase gazeuse Chromatographie en phase gazeuse - Technique Gas chromatography |
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