New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Regensburg
2002
|
| Schlagworte: | |
| Online-Zugang: | Volltext Volltext Inhaltsverzeichnis |
| Beschreibung: | 181 S. graph. Darst. |
Internformat
MARC
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| 041 | 0 | |a eng | |
| 049 | |a DE-355 |a DE-12 |a DE-384 |a DE-473 |a DE-703 |a DE-1051 |a DE-824 |a DE-29 |a DE-91 |a DE-19 |a DE-1049 |a DE-92 |a DE-739 |a DE-20 | ||
| 084 | |a VK 5075 |0 (DE-625)147396: |2 rvk | ||
| 100 | 1 | |a Ye, Mao |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines |c vorgelegt von Mao Ye |
| 264 | 1 | |a Regensburg |c 2002 | |
| 300 | |a 181 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Universität Regensburg |d 2002 | ||
| 650 | 0 | 7 | |a Stereoselektive Reaktion |0 (DE-588)4132164-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Piperidonderivate |0 (DE-588)4386556-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Nucleophile Addition |0 (DE-588)4337149-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Piperidin |0 (DE-588)4174747-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Carbamate |0 (DE-588)4147270-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Enolate |0 (DE-588)4345140-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kohlenstoff-Kohlenstoff-Bindung |0 (DE-588)4164549-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Asymmetrische Synthese |0 (DE-588)4135603-2 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Piperidonderivate |0 (DE-588)4386556-2 |D s |
| 689 | 0 | 1 | |a Carbamate |0 (DE-588)4147270-6 |D s |
| 689 | 0 | 2 | |a Asymmetrische Synthese |0 (DE-588)4135603-2 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Piperidin |0 (DE-588)4174747-1 |D s |
| 689 | 1 | 1 | |a Enolate |0 (DE-588)4345140-8 |D s |
| 689 | 1 | 2 | |a Kohlenstoff-Kohlenstoff-Bindung |0 (DE-588)4164549-2 |D s |
| 689 | 1 | 3 | |a Nucleophile Addition |0 (DE-588)4337149-8 |D s |
| 689 | 1 | 4 | |a Stereoselektive Reaktion |0 (DE-588)4132164-9 |D s |
| 689 | 1 | |5 DE-604 | |
| 776 | 1 | 8 | |i Erscheint auch als |n Online-Ausgabe |o urn:nbn:de:bvb:355-opus-2110 |
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| 856 | 4 | 1 | |u https://epub.uni-regensburg.de/10125/ |x Verlag |z kostenfrei |3 Volltext |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010036626&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
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Datensatz im Suchindex
| _version_ | 1807504010210443264 |
|---|---|
| adam_text |
INDEX
CHAPTER
1:
INTRODUCTION
1
1.1
PIPERIDINES:
INTEGRAL
COMPONENTS
OF
COUNTLESS
ALKALOIDS
1
1.2
RECENT
DEVELOPMENT
OF
THE
REACTIONS
OF
N-PROTECTED-PIPERIDONES
2
1.2.1
N-PROTECTED-2-PIPERIDONES
2
1.2.2
N-PROTECTED-3-PIPERIDONES
7
1.2.3
N-PROTECTED-4-PIPERIDONES
14
1.3
AIM
OF
THIS
WORK
18
1.4
REFERENCES
20
CHAPTER
2:
SYNTHESES
OF
N-CARBAMATE-2-METHOXY-3-PIPERIDONES
DERIVATIVES
23
2.1
INTRODUCTION
23
2.2
BACKGROUND
AND
THE
DESIGN
OF
THE
SYNTHESIS
OF
N-PROTECTED-3-PIPERIDONES
26
2.3
SYNTHESIS
OF
N-CARBAMATE-2-METHOXY-3-PIPERIDONES
27
2.3.1
PROTECTION
OF
N-H
BOND
OF
PIPERIDINE
RING
27
2.3.2
PROTECTION
OF
HYDROXY
GROUP
AND
THE
SWEM-WITTIG
REACTION
28
2.3.3
THE
ANODIC
OXIDATIONS
29
2.3.4
ELIMINATION
AND
EPOXIDATION
FOLLOWED
BY
RING-OPENING
REACTION
32
2.3.5
SWEM
OXIDATION
OF
ALCOHOL
TO
CARBONYLS
33
2.4
THE
'H-NMR
STUDIES
OF
SOME
PIPERIDINE
DERIVATIVES
36
2.4.1
'H-NMR
OF
PIPERIDINE
AND
METHYLPIPERIDINES
37
2.4.2
'
H-NMR
ANALYSIS
OF
N-CARBAMATE-PIPERIDINES
38
2.5
REFERENCES
42
CHAPTER
3:
REACTIONS
OF
PIPERIDINE-3-ONES
ON
THE
CARBONYL
GROUP
45
3.1
NUCLEOPHILIC
ADDITION
ON
THE
CARBONYL
GROUP
46
3.1.1
THE
ADDITION
REACTION
WITH
2-FURYLLITHIUM
46
3.1.2
THE
ALDOL
REACTION
OF
N-CARBAMATE-2-METHOXY-3-PIPERIDONES
48
3.1.3
THE
ADDITION
REACTION
WITH
POTASIUM
CYANIDE
52
3.2
WITTIG
AND
HWE
REACTIONS
57
3.3
SOME
INTERESTING
REACTIONS
BASED
ON
NUCLEOPHILIC
ADDITION
PRODUCTS
55
3.3.1
THE
OXIDATION-REARRANGEMENT
OF
COMPOUND
134
55
3.3.2
STUDY
OF
THE
CSIC
REACTION
63
3.4
REFERENCES
66
CHAPTER
4:
REGIOSELECTIVE
FORMATION
OF
ENOL
ACETATES
AND
THE
ALDOL
REACTION
69
4.1
INTRODUCTION
8)
4.2
FORMATION
OF
SILYL
ENOL
ETHERS
1
4.3
FORMATION
OF
ENOL
ACETATES
TL
4.4
ATTEMPTS
OF
ALDOL
REACTIONS
OF
127
WITH
LITHIUM
ENOLATES,
SILYL
ENOL
ETHERS
AND
TITANIUM
ENOLATES
71
4.5
ALDOL
REACTION
WITH
ENOL
ACETATE
172
71
4.6
REFERENCES
7
CHAPTER
5:
REACTIONS
ON
6-SIDE
CHAIN
OF
N-CARBAMATE
PIPERIDINES
DERIVATIVES
1
5.1
STEREOSELECTIVITIES
OF
WITTIG
AND
HWE
REACTIONS
IN
6-SIDE
CHAIN
5.2.
SYNTHESIS
OF
L,2-DIHYDROXYHEXAHYDROINDOLIZIDINE-3-ON
I
5.2.1
INTRODUCTION
I
5.2.2
SYNTHESIS
OF
RACEMIC
L,2-DIHYDROXYHEXAHYDROINDOLIZIDINE-3-ON
184
I
5.3
SYNTHESIS
OF
5-METHOXY-TETRAHYDRO-OXAZOLO[3,4-A]PYRIDIN-3,6-DIONE
188
I
5.4
EXPLORATION
OF
EPOXIDATION
REACTIONS
!
5.5
REFERENCES
!
CHAPTER
6:
SUMMARY
5
CHAPTER
7:
EXPERIMENTAL
SECTION
10
7.1
INSTRUMENTS
AND
GENERAL
TECHNIQUES
IQ
7.2
SYNTHESIS
OF
THE
COMPOUNDS
10
7.2.1
SYNTHESIS
OF
N-CARBAMATE-2-METHOXY-3-PIPERIDONES
DERIVATIVES
10
7.2.2
REACTIONS
OF
3-PIPERIDONES
DERIVATIVES
13
7.2.3
FORMATION
OF
ENOL
ACETATES
AND
ALDOL
REACTION
14
7.2.4
REACTION
ON
6-SIDE
CHAIN
OF
N-CARBAMATE
PIPERIDINES
15|
CHAPTER8:
SPECTROSCOPY
163
ACKNOWLEDGEMENTS |
| any_adam_object | 1 |
| author | Ye, Mao |
| author_facet | Ye, Mao |
| author_role | aut |
| author_sort | Ye, Mao |
| author_variant | m y my |
| building | Verbundindex |
| bvnumber | BV014833091 |
| classification_rvk | VK 5075 |
| collection | ebook |
| ctrlnum | (OCoLC)643716417 (DE-599)BVBBV014833091 |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| indexdate | 2024-08-16T01:02:30Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-010036626 |
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| spelling | Ye, Mao Verfasser aut New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines vorgelegt von Mao Ye Regensburg 2002 181 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Dissertation Universität Regensburg 2002 Stereoselektive Reaktion (DE-588)4132164-9 gnd rswk-swf Piperidonderivate (DE-588)4386556-2 gnd rswk-swf Nucleophile Addition (DE-588)4337149-8 gnd rswk-swf Piperidin (DE-588)4174747-1 gnd rswk-swf Carbamate (DE-588)4147270-6 gnd rswk-swf Enolate (DE-588)4345140-8 gnd rswk-swf Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd rswk-swf Asymmetrische Synthese (DE-588)4135603-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Piperidonderivate (DE-588)4386556-2 s Carbamate (DE-588)4147270-6 s Asymmetrische Synthese (DE-588)4135603-2 s DE-604 Piperidin (DE-588)4174747-1 s Enolate (DE-588)4345140-8 s Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 s Nucleophile Addition (DE-588)4337149-8 s Stereoselektive Reaktion (DE-588)4132164-9 s Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:355-opus-2110 https://nbn-resolving.org/urn:nbn:de:bvb:355-opus-2110 Resolving-System kostenfrei Volltext https://epub.uni-regensburg.de/10125/ Verlag kostenfrei Volltext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010036626&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ye, Mao New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines Stereoselektive Reaktion (DE-588)4132164-9 gnd Piperidonderivate (DE-588)4386556-2 gnd Nucleophile Addition (DE-588)4337149-8 gnd Piperidin (DE-588)4174747-1 gnd Carbamate (DE-588)4147270-6 gnd Enolate (DE-588)4345140-8 gnd Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd Asymmetrische Synthese (DE-588)4135603-2 gnd |
| subject_GND | (DE-588)4132164-9 (DE-588)4386556-2 (DE-588)4337149-8 (DE-588)4174747-1 (DE-588)4147270-6 (DE-588)4345140-8 (DE-588)4164549-2 (DE-588)4135603-2 (DE-588)4113937-9 |
| title | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines |
| title_auth | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines |
| title_exact_search | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines |
| title_full | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines vorgelegt von Mao Ye |
| title_fullStr | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines vorgelegt von Mao Ye |
| title_full_unstemmed | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines vorgelegt von Mao Ye |
| title_short | New N-carbamate-2-methoxy-3-piperidones as precursors of highly functionalized piperidines |
| title_sort | new n carbamate 2 methoxy 3 piperidones as precursors of highly functionalized piperidines |
| topic | Stereoselektive Reaktion (DE-588)4132164-9 gnd Piperidonderivate (DE-588)4386556-2 gnd Nucleophile Addition (DE-588)4337149-8 gnd Piperidin (DE-588)4174747-1 gnd Carbamate (DE-588)4147270-6 gnd Enolate (DE-588)4345140-8 gnd Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd Asymmetrische Synthese (DE-588)4135603-2 gnd |
| topic_facet | Stereoselektive Reaktion Piperidonderivate Nucleophile Addition Piperidin Carbamate Enolate Kohlenstoff-Kohlenstoff-Bindung Asymmetrische Synthese Hochschulschrift |
| url | https://nbn-resolving.org/urn:nbn:de:bvb:355-opus-2110 https://epub.uni-regensburg.de/10125/ http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=010036626&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT yemao newncarbamate2methoxy3piperidonesasprecursorsofhighlyfunctionalizedpiperidines |