Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
München
Hieronymus
2001
|
| Schriftenreihe: | Pharmazie
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zugl.: München, Univ., Diss., 2001 |
| Beschreibung: | V, 340 S. graph. Darst. : 21 cm |
| ISBN: | 3897912341 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
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| 001 | BV014614634 | ||
| 003 | DE-604 | ||
| 005 | 20060627 | ||
| 007 | t | ||
| 008 | 020806s2001 gw d||| m||| 00||| ger d | ||
| 016 | 7 | |a 963889508 |2 DE-101 | |
| 020 | |a 3897912341 |c kart. : EUR 26.00 (freier Pr.) |9 3-89791-234-1 | ||
| 035 | |a (OCoLC)53805022 | ||
| 035 | |a (DE-599)BVBBV014614634 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a ger | |
| 044 | |a gw |c DE | ||
| 049 | |a DE-19 |a DE-12 |a DE-29T | ||
| 100 | 1 | |a Renz, Manfred |d 1970- |e Verfasser |0 (DE-588)123592437 |4 aut | |
| 245 | 1 | 0 | |a Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen |c Manfred Renz |
| 264 | 1 | |a München |b Hieronymus |c 2001 | |
| 300 | |a V, 340 S. |b graph. Darst. : 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Pharmazie | |
| 500 | |a Zugl.: München, Univ., Diss., 2001 | ||
| 650 | 0 | 7 | |a Alkylierung |0 (DE-588)4217435-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Chemische Synthese |0 (DE-588)4133806-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Emetaminanaloga |0 (DE-588)4692717-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Reissert-Verbindungen |0 (DE-588)4550749-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Emetinanaloga |0 (DE-588)4692692-6 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Emetinanaloga |0 (DE-588)4692692-6 |D s |
| 689 | 0 | 1 | |a Chemische Synthese |0 (DE-588)4133806-6 |D s |
| 689 | 0 | 2 | |a Reissert-Verbindungen |0 (DE-588)4550749-1 |D s |
| 689 | 0 | 3 | |a Alkylierung |0 (DE-588)4217435-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Emetaminanaloga |0 (DE-588)4692717-7 |D s |
| 689 | 1 | 1 | |a Chemische Synthese |0 (DE-588)4133806-6 |D s |
| 689 | 1 | 2 | |a Reissert-Verbindungen |0 (DE-588)4550749-1 |D s |
| 689 | 1 | 3 | |a Alkylierung |0 (DE-588)4217435-1 |D s |
| 689 | 1 | |5 DE-604 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012766196&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-012766196 | |
Datensatz im Suchindex
| _version_ | 1808227215794503680 |
|---|---|
| adam_text |
INHALTSVERZEICHNIS
1
EINLEITUNG:
-----------------------------------------------------------------------------------------------------------------16
1.1
T
HEMENSTELLUNG
-----------------------------------------------------------------------------------------------------------------------------
25
2
ALLGEMEINER
TEIL:
----------------------------------------------------------------------------------------------------
28
2.1
S
YNTHESE
VON
1
,3-D
IBROMPROPANDERIVATEN
ALS
KOMBINIERTE
A
LKYLIERUNGS
-
UND
Z
YKLISIERUNGSREAGENZIEN
:
-----------------------------------------------------------------------------------------------------
28
2.1.1
SYNTHESEPLANUNG.
----------------------------------------------------------------------------------------------------------------------
28
2.1.2
SYNTHESE
DIVERSER
PHOSPHONSAEUREDIETHYLESTER
040
(ABB.
15):
----------------------------------------------------
29
2.1.2.1
SYNTHESE
DER
ALKYLHALOGENIDE
039
ALS
EDUKTE
DER
PHOSPHONSAEUREESTER
040
(VGL.
TABELLE
1,
SEITE
29)
-
31
2.1.2.1.1
SYNTHESE
DER
SAEUREAMIDE
047,048,049,050
(VGL.
TABELLE
1,
SEITE
30)
------------------------------------
31
2.1.2.1
2
SYNTHESE
DES
NITRILS
053
(ABB.
16)
------------------------------------------------------------------------------------
31
2
1
2.1
3
SYNTHESE
DES
ACETALS
055
(VGL.
TABELLE
1,
SEITE
30)
--------------------------------------------------------------
32
2
1
2.1
4
SYNTHESE
DES
ETHERS
059
(ABB.
17)
-------------------------------------------------------------------------------------
32
2.1
3
SYNTHESE
VON
2,2-DIMETHYL-L,3-DIOXAN-5-ON
041
(ABB.
18):
------------------------------------------------------
33
2.1.4
ESTER-REIHE:
DARSTELLUNGSVERSUCHE
VON
HALOGENIDEN
DES
TYPS
044
(ABB.
19)
--------------------------
34
2.1.4.1
SYNTHESE
VON
A,SS-UNGESAETTIGTEN
ESTERN
NACH
HOMER-WADSWORTH-EMMONS.
-------------------------------------
34
2
1.4.2
ACETALSPALTUNG
VON
064
(ABB.
25):
--------
-
-
*
------------------------
-
---------------------------------------
------
37
2.1.4.3
BROMIERUNG
VON
073
(ABB.
26):
--------------------------------------------------------------------
YY
---------------------------
38
2.1.4.4
KATALYTISCHE
HYDRIERUNG
VON
064
(ABB.
28,
SEITE
40).
------------------------------------------------------------------
39
2.1.4.5
KATALYTISCHE
HYDRIERUNG
VON
073
(ABB.
29,
SEITE
41).
---------
-
------------------------------------------------
40
2.1.4.6
ACETALSPALTUNG
VON
075
(ABB.
28,
SEITE
40):
------------------------------------------------------------------------------
41
2.1
4
7
BROMIERUNG
VON
078
(ABB.
30):
------------------------
-
--------------------------------------------------------------------
41
2.
1
.4.8
TERT.-BUTYLESTER-GRUPPE:
-----------------------------------------------------------------------------------------------------------
43
2.1.5
SAEUREAMID-REIHE:
DARSTELLUNGSVERSUCHE
VON
HALOGENIDEN
DES
TYPS
044
(ABB.
37)
------------------
46
271.5
1
SYNTHESE
VON
SAEUREAMID-SUBSTITUIERTEN
OLEFINEN
NACH
HOMER-WADSWORTH-EMMONS:
------------------------
46
2.1.5.2
ACETALSPALTUNG
VON
085
UND
087
(ABB.
41):
--------------------------------------------------------------------------------
48
2.1.5.3
BROMIERUNG
-----------------------------------
-
-
-------------------------------
------------------------------
-----------------
48
2.1.6
ETHER-REIHE'
DARSTELLUNGSVERSUCHE
VON
HALOGENIDEN
DES
TYPS
044
(ABB.
42)
--------------------------
50
2.1.7
ACETAL-REIHE:
THEORETISCHE
UEBERLEGUNGEN
-------------------------------------------------------------------------------
51
2.1.8
NITRIL-REIHE:
DARSTELLUNGSVERSUCHE
VON
HALOGENIDEN
DES
TYPS
044
(ABB
45)
--------------------------
51
2
1.8.1
SYNTHESE
DESNITRIL-SUBSTITUIERTENOLEFINS091
(ABB.
46)
NACH
HOMER-WADSWORTH-EMMONS
-
--------------
52
2
1.8.2
ACETALSPALTUNG
VON
091
(ABB.
47):
-----------------------------------------------------------------------------------------------
52
2.1.8.3
BROMIERUNG
VON
092
(ABB
48)
---------------------------------------------------------------------------------------------------
52
2.1.8.4
HYDRIERUNG
VON
091
(ABB.
50):
---------------------------------------------------------------------------------------------------
53
2.1.8.5
ACETALSPALTUNG
VON
095
(ABB
51,
SEITE
54):
----------------------------------------------------------------------------------
53
2.1.8.6
BROMIERUNG
VON
096
(ABB.
55)
---------------------------------------------------------------------------------------------------
55
2.1.8.7
SYNTHESE
DESNITRIL-SUBSTITUIERTEN
OLEFINS
100(ABB.
56,
SEITE
56)
NACHHOMER-WADSWORTH-EMMONS.
-
55
2.1.8.8
VERSUCHE
ZUR
ACETALSPALTUNG
VON
100 (ABB.
57):
---------
-
-
-------------------------------------------------------
56
2.1.9
ABSCHLIESSENDE
BETRACHTUNGEN:
--------------------------------------------------------------------------------------------------
57
2.2
S
YNTHESE
VON
R
EISSERT
-V
ERBINDUNGEN
:
-----------------------------------------------------------------------------------------
58
2.2.1
SYNTHESE
DER
A
USGANGSSTOFFE:
-----------------------------------------------------------------------------------------------------
58
2.2
1.1
SYNTHESE
VON
6,7-DIMETHOXYISOCHINOHN
108
(ABB.
60,
SEITE
59)
--------------------------------------------------
58
2.2.1
2
SYNTHESE
VON
6,7-DIMETHOXY-3,4-DIHYDRO-ISOCHINOLIN
114
(ABB.
61,
SEITE
60)
-------------------------------
59
2.2.2
REISSERT
VERBINDUNGEN:
--------------------------------------------------------------------------------------------------------------
60
2.3
U
NTERSUCHUNGEN
ZUR
S
IMULTAN
-D
OPPELALKYLIERUNG
VON
R
EISSERT
-V
ERBIN
-
DUNGEN
:
-------------
63
2.3.1
SYNTHESEPLANUNG:
-----------------------------------------------------------------------------------------------------------------------
63
2.3.2
SIMULTANE
DOPPELALKYLIERUNG
MIT
1,
3-DIBROMPROPAN
YY
---------------------------------------------------------------
63
INHALTSVERZEICHNIS
2
3.3
SIMULTANE
DOPPELALKYLIERUNG
MIT
4-BROM-3-BROMMETHYL~BUT-2ENNITRIL
093
(ABB
66).
-------------
65
2.3.4
SIMULTANE
DOPPELALKYLIERUNGSVERSUCHE
MIT
DIBROMID
098
BZW
DITOSYLAT
097
(ABB.
67,
SEITE
67):
------------------------------------------------------------------------------------------------------------------------------------
66
2.3.5
HYDROLYSE
DER
REISSERT-VERBINDUNG
118
(ABB.
68,
SEITE
68)
-------------------------------------------------------
67
2.3.6
REDUKTIONSVERSUCHE
--------------------------------------------------------------------------------------------------------------------
69
2.3.6.1
REDUKTIONSVERSUCH
DER
VERBINDUNG
119
(ABB.
70):
--------------------------------------------------------------------
69
2.3.6.2
SYNTHESE
DER
MODELLVERBINDUNG
123
(ABB.
72):
----------------------------------------------------
-
------------------
70
2.3.6.3
REDUKTIONS-ZUMSETZUNGSVERSUCHE
DER
VERBINDUNG
123
(ABB
72,
SEITE
70)
-------------------------------------
71
2.4
U
NTERSUCHUNGEN
ZUR
SUKZESSIVEN
D
OPPELALKYLIERUNG
VON
R
EISSERT
-V
ERBINDUNGEN
:
------------
72
2.4.1
SYNTHESEPLANUNG'
----------------------------------------------------------------------------------------------------------------------
72
2.4.2
ISOCHINOLIN-REIHE
---------------------------------------------------------------------------------------------------------------------
73
2.4.2.1
ALKYLIERUNG
DER
REISSERT-VERBINDUNG
102
(ABB.
76)
MIT
4-BROMMETHYL-3-ETHYL-5H-FURAN-2-ON
074
(ABB.
76):
-----------------------------------------------------------------------------------------------------------------------------------------
73
2.4.2.2
HYDROLYSE
DER
ALKYLIERTEN
REISSERT-VERBINDUNG
130 (ABB.
77):
--------------------------------------------------------
74
2.4.2.3
UMSETZUNGSVERSUCHE
ZU
VERBINDUNGEN
DES
TYPS
128
(ABB.
75,
SEITE
72,
R
=
H):
-----------------------------
75
2.4.2.4
ALKYLIERUNG
DER
REISSERT-VERBINDUNG
102
MIT
4-BROMMETHYL-3-ETHYL-DIHYDRO-FURAN-2-ON
079A
(ABB
80):
----------------------------------------------------------------------------------------------------------------------------------------------
76
2.4.2.5
HYDROLYSE
DER
ALKYLIERTEN REISSERT-VERBINDUNG
138
(ABB.
81,
SEITE
78):
------------------------------------------
77
2.4.2.OE
UMSETZUNGEN
VON
141
(ABB.
82)
ZU
VERBINDUNGEN
DES
TYPS
143
(ABB.
82):
--------------------------------------
79
2.4.2.7
BROMIERUNG
VON
143
(ABB.
84)
--------------------------------------------------------------------------------------------------
81
2.4.2
8
ALKYLIERUNG
DER
REISSERT-VERBINDUNG
102
MIT
ALKYLHALOGENID
147A
(ABB.
85):
---------------------------------
82
2.4.2.9
HYDROLYSE
DER
ALKYLIERTEN
REISSERT-VERBINDUNG
148
ZU
149 (ABB.
86)
UND
DEREN
REDUKTION
----------------
82
2.4.3
DIMETHOXYISOCHINOLIN-REIHE:
-----------------------------------------------------------------------------------------------------
85
2
4.3
1
ALKYLIERUNG
DER
REISSERT-VERBINDUNG
109
MIT 4-BROMMETHYL-3-ETHYL-DIHYDRO-FIIRAN-2-ON
079A
ZU
152
(ABB.
90):
-------------------------------------------------------------------------------------------------------------------------------
85
2.4.3
2
HYDROLYSE
DER
ALKYLIERTEN
REISSERT-VERBINDUNG
152
ZU
145
(ABB.
92)'
----------------------------------------------
86
2.4.3.3
UMSETZUNGEN
ZU
VERBINDUNGEN
DES
TYPS
146
(ABB.
93):
-----------------------------------------------------------------
87
2.4.3.3.1
HYDRIERUNGEN
VON
MODELLVERBINDUNGEN
-----------------------------------------------------------------------------
89
2.4.3
3
2
HYDRIERUNG
DER
VERBINDUNG
145
(ABB.
93,
SEITE
87):
-
------------------
-
-------------------------
90
2.4.34
AUFKLAERUNG
DER
STEREOCHEMIE
DER
VERBINDUNGEN
146
(146A/146B)
(ABB.
98,
SEITE
92):
---------------------
91
24.3.5
BROMIERUNG
DER
VERBINDUNGEN
146A
UND
146B
(ABB.
101):
-----------
-
---------------------------------------
95
24.3.6
ALKYLIERUNG
DER
REISSERT-VERBINDUNG
109
MIT
DEN
ALKYLHALOGENIDEN
162A
UND
162B
(ABB
103,
SEITE
97):
--------------------------------------------------------------------------------------------------------------------------
96
24.3.7
HYDROLYSE
DER
ALKYLIERTEN REISSERT-VERBINDUNGEN
163A
UND
163B
(ABB.
105,
SEITE
99):
----------------
98
24.3.8
UMSETZUNGEN
VON
164A
UND
1
64B
ZU
EMETAMIN
(165A/165B,
ABB.
108,
SEITE
101)
UND
EMETIN
(166A/166B,
ABB.
111,
SEITE
104)
ANALOGA:
-----------------------------------------------------------------------------
99
24.3.9
SYNTHESEVERSUCHE
ZU
2,3-TRANS
KONFIGURIERTEN
EMETAMIN
UND
EMETIN-ANALOGA:
-------------------
---------
106
2.5
A
BSCHLIEBENDE
B
ETRACHTUNGEN
:
---------------------------------------------------------------------------------------------------
108
3
ZUSAMMENFASSUNG:
-------------------------------------------------------------------------------------------------
109
3.1
I
SOCHINOLIN
-R
EIHE
(A
BB
.
117,
S
EITE
HO):
---------------------------------------------------------------------------------------
109
3.2
6
,7-D
IMETHOXYISOCHINOLIN
-R
EIHE
:
------------------------------------------------------------------------------------------------
111
4
EXPERIMENTELLER
TEIL
-------------------------------------------------------------------------------------------
115
4.1
(5-A
MINO
-2,2
DIMETHYL
-[1,3]
DIOXAN
-5
YL
)
METHANOL
(062)
---------------------------------------------------------
117
4.2
2,2-D
IMETHYL
-[1,3]DIOXAN-5
ON
(041)
--------------------------------------------------------------------------------------------
118
4.3
2-(D
IETHOXY
-
PHOSPHORYL
)
BUTTERSAEUREETHYLESTER
(063)
---------------------------------------------------------
119
4.4
2-C
YCLOHEXYLIDENBUTTERSAEUREETHYLESTER
(071)
-----------------------------------------------------------------------
120
4.5
2-(2,2-DLMETHYL-[L,3]DIOXAN-5-YL!DEN)BUTTERSAEUREETHYLESTER
(064)
---------------------------------------
121
II
INHALTSVERZEICHNIS
4.6
3-E
THYL
-4
HYDROXYMETHYL
-5Z/
FURAN
-2
ON
(073)
------------------------------------------------------------------------
123
4.7
4-BROMMETHYL-3-ETHYL-5//-FURAN-2-ON
(074)
------------------------------------------------------------------------------
125
4.8
2-(L-PHENYL-METHANOYL)-L,2-DIHYDRO-ISOCHINOLIN-L-CARBONLTRIL(102)
-----------------------------------
126
4.9
(D
IETHOXY
-
PHOSPHORYL
)
ESSIOS
A
UREETHYLESTER
(069)
-----------------------------------------------------------------
128
4.10
(2,2-DLMETHYL-[L,3]D10XAN-5-YLIDEN)-ESSLGSAEUREETHYLESTER
(070)
--------------------------------------
128
4.11
2(S)/(R)-(2,2-D
IMETHYL
-[1,3]
DIOXAN
-5
YL
)
BUTTERS
A
UREETHYLESTER
(075)
---------------------------
130
4.12
3-E
THYL
-4
HYDROXYMETHYL
-
DIHYDRO
-
FURAN
-2
ON
(078)
(D
IASTEREOMERENGEMISCH
)
------------
132
4.13
1
-(4-ETHYL-5-OXO-2,5-DIHYDRO-FURAN-3-YLMETHYL)-2-(
1
-PHENYL-METHANOYL)-1,2-DIHYDRO
ISOCHINOLIN
-
I
-
CARBONITRIL
(130)
-----------------------------------------------------------------------------------------------
134
4.14
3-E
THYL
-4
ISOCHINOLIN
-
I
-
YLMETHYL
-5H
FURAN
-2
ON
(131)
-------------------------------------------------------
136
4.15
(3R,4R)/(3S,4S)-4-BROMMETHYL-3-ETHYL-DIHYDRO-FURAN-2-ON(079A)
----------------------------------
138
4.16
C
YANOMETHYL
-
PHOSPHONSAEUREDIETHYLESTER
(090)
------------------------------------------------------------------
140
4.17
(2,2-DLMETHYL-[
1
,3]DIOXAN-5-YLIDEN)-ACETONITRIL
(091)
---------------------------------------------------------
140
4.18
4-HYDROXY-3-HYDROXYMETHYL-BUT-2-ENNITRIL(092)
-------------------------------------------------------------
142
4.19
4-BROM-3-BROMMETHYL-BUT-2-ENNITRIL
(093)
-------------------------------------------------------------------------
144
4.20
B
ENZOESAEURE
(Z)-2
BENZOYLOXYMETHYL
-3
CYANO
-
ALLYLESTER
(094)
-------------------------------------
145
4.21
(2,2-D
IMETHYL
-[1,3]
DIOXAN
-5
YL
)
ACETONITRIL
(095)
---------------------------------------------------------------
147
4.22
4-H
YDROXY
-3
HYDROXYMETHYL
-
BUTYRONITRIL
(096)
-----------------------------------------------------------------
149
4.23
TOLUOL-4-SULFONSAURE-2-TOSYLOXYMETHYL-3-CYANO-PROPYLESTER(097)
---------------------------
151
4.24
4-BROM-3-BROMMETHYL-BUTYRONITRIL(098)
----------------------------------------------------------------------------
152
4.25
(3,4-DLMETHOXY-BENZYLIDEN)-(2,2-DIMETHOXY-ETHYL)-AMIN(105)
------------------------------------------
154
4.26
(3,4-DLMETHOXY-BENZYL)-(2,2-DLMETHOXY-ETHYL)-AMIN(106)
--------------------------------------------------
155
4.27
N-(3,4-DLMETHOXY-BENZYL)-N-(2,2-DIMETHOXY-ETHYL)-4-METHYL-BENZOLSULFONAMID(107)156
4.28
6,7-DLMETHOXYISOCHINOLIN
(108)
------------------------------------------------------------------------------------------------
157
4.29
6,7-DLMETHOXY-2-(
1
-PHENYL-METHANOYL)
1
,2-DIHYDRO-ISOCHINOLIN
1
-CARBONITRIL
(109)
-
158
4.30
4-[
1
-CYANO-6,7-DIMETHOXY-2-(L
-PHENYL-METHANOYL)
1
,2-DIHYDRO-ISOCHINOLIN
1
-YL]-3-[
1
-
CYANO-6,7-DIMETHOXY-2-(L-PHENYL-METHANOYL)-L,2-DLHYDRO-ISOCHINOLIN-L-YLMETHYL]-BUT
2
ENNITRIL
(118)
---------------------------------------------------------------------------------------------------------------------------
160
4.31
2-B
ROM
-1,1
DIMETHOXY
-
BUTAN
(055)
----------------------------------------------------------------------------------------
163
4.32
2-(6,7-DLMETHOXY-ISOCHINOLIN
1
-YLMETHYL)-9,
1
0-DIMETHOXY-BENZO[A]CHINOUZIN-4
YUDENAMIN
(119)
------------------------------------------------------------------------------------------------------------------------
164
4.33
2-B
ROMMETHYL
-
BENZONITRIL
(121)
----------------------------------------------------------------------------------------------
165
4.34
1
-(2-C
YANO-BENZYL)-6,7-DIMETHOXY-2-(
1
-PHEN
YL
-
MBTHANOYL
)
1
,2
DIHYDRO
-
ISOCHINOLIN
-
1
-
CARBONITRIL
(122)
-----------------------------------------------------------------------------------------------------------------------
166
4.35
2,3-D
IMETHOXY
-
DIBENZO
[
A
,
G
]
CHINOLIZIN
-8
YLIDENAMIN
(123)
---------------------------------------------------
169
4.36
(D
IETHOXY
-
PHOSPHORYL
)
ESSIGSAEURE
-
TERT
.
BUTYLESTER
(080)
--------------------------------------------------
171
4.37
(2,2-D
IMETHYL
-[1,3]
DIOXAN
-5
YLIDEN
)
ESSICS
A
URE
-
TERT
-
BUTYLESTER
(081)
-----------------------------
172
4.38
4-HYDROXYMETHYL-5W-FURAN-2-ON
(082)
---------------------------------------------------------------------------------
174
4.39
2-B
ROM
-N,N
DIMETHYL
-
BUTTERSAEUREAMID
(047)
-----------------------------------------------------------------------
174
4.40
2-B
ROM
-N,N
DIETHYLBUTTERSAEUREAMID
(049)
---------------------------------------------------------------------------
176
4.41
(1
-D
IMETHYLCARBAMOYL
-
PROPYL
)
PHOSPHONSAEUREDIETHYLESTBR
(083)
----------------------------------
178
4.42
2-BROM-N,N-DIMETHYL-ACETAMID(048)
------------------------------------------------------------------------------------
179
4.43
DIMETHYLCARBAMOYLMETHYL-PHOSPHONSAEUREDIETHYLESTER(084)----------------------------------------
181
4.44
2-(2,2-D
IMETHYL
-[1,3]
DIOXAN
-5
YLIDEN
)-N,N
DIMETHYL
-
ACETAMID
(085)
-------------------------------
182
4.45
2-BROM-N,N-DIETHYL-ACETAMID(050)
--------------------------------------------------------------------------------------
184
III
INHALTSVERZEICHNIS
4.46
DIETHYLCARBAMOYLMETHYL-PHOSPHONSAUREDIETHYLESTER(086)------------------------------------------
185
4.47
2-(2,2-D
IMETHYL
-[1,3]
DIOXAN
-5
YLIDEN
)-N,N
DIETHYL
-
ACETAMID
(087)
---------------------------------
186
4.48
4-H
YDROXY
-3
HYDROXYMETHYL
-
BUT
-2
ENS
A
UREDIETHYLAMID
(088)
---------------------------------------
188
4.49
2-B
ENZYLOXY
-
ETHANOL
(058)
----------------------------------------------------------------------------------------------------
189
4.50
(2-BROM-ETHOXYMETHYL)-BENZOL
(059)
-----------------------------------------------------------------------------------
191
4.51
(2-B
ENZYLOXY
-
ETHYL
)
PHOSPHONS
A
UREDIETHYLESTER
(089)
----------------------------------------------------
192
4.52
2-BROM-BUTTERSA
UE
REAMID
(052)
----------------------------------------------------------------------------------------------
193
4.53
2-BROM-BUTYRONITRIL
(053)
------------------------------------------------------------------------------------------------------
194
4.54
(1-C
YANO
-
PROPYL
)
PHOSPHONSAEUREDIETHYLESTER
(099)
------------------------------------------------------------
195
4.55
2-(2,2-D
IMETHYL
-[1,3]
DIOXAN
-5
YLIDEN
)
BUTYRONITRIL
(100)
---------------------------------------------------
196
4.56
1-(4-E
THYL
-5
OXO
-
TETRAHYDRO
-
FURAN
-3
YLMETHYL
)-6,7
DIMETHOXY
-2-(1
PHENYL
-
METHANOYL)-1,2-DIHYDRO-ISOCHINOLIN-1-CARBONITRIL
(152)
----------------------------------------------------
198
4.57
4-(6,7-D
IMETHOXY
-
ISOCHINOLIN
-1
YLMETHYL
)-3
ETHYL
-
DIHYDRO
-
FURAN
-2
ON
(145)
---------------
202
4.58
1-(4-E
THYL
-5
OXO
-2,5
DIHYDRO
-
FURAN
-3
YLMETHYL
)-6,7
DIMETHOXY
-2-(1
PHENYL
-
METHANOYL
)
1,2-DIHYDRO-ISOCHINOLIN-L-CARBONITRIL
(174)
------------------------------------------------------------------------
204
4.59
1
-(4-ETH
YL-5-OXO-TETRAHYDRO-FURAN-3-YLMETHYL)-2-(
1
-PHEN
YL-METHANOYL)
1,2
-DIHYDRO
ISOCHINOLIN
1
-CARBONITRIL
(DIASTEREOMERENGEMISCH)
(138)
-----------------------------------
207
4.60
3-ETHYL-4-ISOCHINOLIN
1
-YLMETHYL-DIH
YDRO-FURAN-2-ON
(141)
-------------------------------------------
210
4.61
3-ETHYL-4-(5,6,7,8-TETRAHYDRO-ISOCHINOLIN-1-YLMETHYL)-DIHYDRO-FURAN-2-ON
(144)
--------
213
4.62
3-E
THYL
-2
HYDROXYMETHYL
-1,2,3,6,7,1
1
B
-
HEXAHYDRO
-
BENZO
[
A
]
CHINOLIZIN
-4
ON
(D
IASTEREOMERENGEMISCH
)
(143)
-----------------------------------------------------------------------------------------------
215
4.63
2-BR0MMETHYL-3-ETHYL
1,2,3,6,7,11
B-HEXAHYDRO-BENZO[
A
]CHINOLIZIN-4-ON
(1
47A/147SS)
-
219
4.64
1
-(3-ETHYL-4-0X0
1,3,4,6,7,11
B-HEXAHYDR0-2W-BENZ0[
A]CHINOLIZIN-2-YLMETHYL)-2-(
1
-
PHEN
YL-METHANOYL)
1
,2-DIHYDRO-ISOCHINOLIN
1
-CARBONITRIL
(148)
(DIASTEREOMERENGEMISCH)
-------------------------------------------------------------------------------------------------------
223
4.65
3-ETHYL-2-LSOCHINOLIN-L-YLMETHYL-L,2,3,6,7,LLB-HEXAHYDRO-BENZO[A]CHLNOLLZIN-4-ON(149)
----------------------------------------------------------------------------------------------------------------------------------------------------
227
4.66
3-ETHYL-2-(L,2,3,4-TETRAHYDRO-ISOCHINOLIN-L-YLMETHYL)-L,2,3,6,7,LLB-HEXAHYDRO
BENZO
[
A
]
CHINOLIZIN
-4
ON
(150)
-------------------------------------------------------------------------------------------------
229
4.67
3-ETHYL-2-(
1
,2,3,4-TETRAHYDRO-ISOCHINOLIN
1
-YLMETHYL)
1,3,4,6,7,11
B-HEXAHYDRO-277
BENZO[A]CHINOLIZIN
(151)
----------------------------------------------------------------------------------------------------------
233
4.68
6,
7-D1METHOXY-2-0-P-TOLYL-METHANOYL)-1,2-DIHYDRO-ISOCHINOLIN-L-CARBONITRIL
(110)
236
4.69
2-BENZYL-L-(4-ETHYL-5-OXO-TETRAHYDRO-FURAN-3-YLMETHYL)-6,7-DIMETHOXY
ISOCHINOLINIUMBROMID
(158)
-----------------------------------------------------------------------------------------------------
238
4.70
N-[2-(3,4-D
IMETHOXY
-
PHENYL
)
ETHYL
]
FORMAMID
(113)
-----------------------------------------------------------
240
4.71
6,7-DIMETHOXY-3,4-DIHYDRO-ISOCHINOLIN
(114)
------------------------------------------------------------------------
242
4.72
6,7-DLMETH0XY-2-(
1
-PHENYL-METHANOYL)
1
,2,3,4-TETRAHYDRO-ISOCHINOLIN
1
-CARBONITRIL
(115)
--------------------------------------------------------------------------------------------------------------------------------------------
243
4.73
L-(4-ETHYL-5-OXO-TETRAHYDRO-FURAN-3-YLMETHYL)-6,7-DIMETHOXY-2-(L-PHENYL
METHANOYL
)-1,2,3,4
TETRAHYDRO
-
ISOCHINOLIN
-1
CARBONITRIL
(D
IASTEREOMER
)
(157)
----------
244
4.74
6,7-D
IMETHOXY
-1,2,3,4
TETRAHYDRO
-
ISOCHINOLIN
(159)
-----------------------------------------------------------
247
4.75
(2R.3R.1
IBS)
(BZW.
2S,3S,1
I
B
R)
-3-ETHYL-2-HYDROXYMETHYL-9,10-DIMETHOXY-L,2,3,6,7,LLB
HEXAHYDRO
-
BENZO
[
A
]
CHINOLIZIN
-4
ON
(146
A
)
UND
(2R,3R,1
I
B
R)
(BZW.
2S,3S,1
1
B
S)-3-E
THYL
-2
HYDROXYMETHYL
-9,
1
0-DIMETHOXY
1,2,3,6,7,11
B
-
HEXAHYDRO
-
BENZO
[
A
]
CHINOLIZIN
-4
ON
(146
B
)
--------------------------------------------------------------------------------------------------------------------------------------------------
248
IV
INHALTSVERZEICHNIS
4.76
(2R,3R,1
IBS)
(BZW.
2S,3S,1
LBR)-2-BROMMETHYL-3-ETHYL-9,10-DIMETHOXY-L,2,3,6,7,L
1B
HEXAHYDRO
-
BENZO
[
A
]
CHINOLIZIN
-4
ON
(162
A
)
--------------------------------------------------------------------------
258
4.77
(2R,3R,1
LBR)-2-BROMMETHYL-3-ETHYL-9,10-DIMETHOXY-L,2,3,6,7,L
1B-HEXAHYDR0
BENZO[A]CHLNOLIZIN-4-ON
(162
B
)
(BZW.
2S,3S,1
IBS)
----------------------------------------------------------------
261
4.78
1
-((2S.3R,
11
BR)
(BZW.
2R.3S,
11
BS)-3-ETHYL-9,
10-DIMETHOXY-4-OXO
1,3,4,6,7,11
B-HEXAHYDRO
2//-BENZO[A]CHINOLIZIN-2-YLMETHYL)-6,7-DIMETHOXY-2-(L-PHENYL-METHANOYL)-L,2-DIHYDRO
ISOCHINOLIN
1
-CARBONITRIL
(DIASTEREOMERENGEMISCH)
(163B)
----------------------------------------------
264
4.79
1-((2S,3R,1
IBS)
(BZW.
2R,3S,11BR)
-3-ETHYL-9,10-DIMETHOXY-4-OXO-L,3,4,6,7,L
1B-HEXAHYDRO
2H-BENZO[A]CHINOLIZIN-2-YLMETHYL)-6,7-DIMETHOXY-2-(L-PHENYL-METHANOYL L,2-DIHYDRO
ISOCHINOLIN-1-CARBONITRIL
(DIASTEREOMERENGEMISCH)
(163A)
----------------------------------------------
269
4.80
(2S,3R,11BR)
(BZW.
2R.3S.1
LBS)-2-(6,7-DLMETHOXY-ISOCHINOLIN-L-YLMETHYL)-3-ETHYL-9,10
DIMETHOXY
-1,2,3,6,7,1
1
B
-
HEXAHYDRO
-
BENZO
[
A
]
CHINOLIZIN
-4
ON
(164
B
)
---------------------------------
274
4.81
(2S.3R.1
IBS)
(BZW.
2R,3S,LLBR)-2-(6,7-DLMETHOXY-ISOCHINOLIN-L-YLMETHYL)-3-ETHYL-9,10
DIMETHOXY
-1,2,3,6,7,1
1
B
-
HEXAHYDRO
-
BENZO
[
A
]
CHINOLIZIN
-4
ON
(164
A
)
---------------------------------
277
4.82
1-(3,4-D
IMETHOXY
-
BENZYL
)-6,7
DIMETHOXY
-1,2,3
4
TETRAHYDRO
-
ISOCHINOLIN
(161)
--------------
280
4.83
(2S,3R,11BR)
(BZW.
2R,3S,1
LBS)-2-(6,7-DLMETHOXY-ISOCHINOLIN-L-YLMETHYL)-3-ETHYL-9,10
DIMETHOXY
-1,3,4,6,7,1
1
B
-
HEXAHYDRO
-2//
BENZO
[
A
]
CHINOLIZIN
(165
B
)
------------------------------------
281
4.84
(2S.3R.1
IBS)
(BZW.
2R,3S,1
LBR 2-(6,7-DLMETHOXY-ISOCHINOLIN-L-YLMETHYL)-3-ETHYL-9,10
DIMETHOXY-1,3,4,6,7,1
1B-HEXAHYDRO-2/7-BENZO[A]CHINOLIZIN
(165
A
)
UND
(2S,1
IBS)
(BZW.
2R,
11
BR)-2-(6,7-DLMETHOXY-ISOCHINOLIN
1
-YLMETHYL)-3-ETHYL-9,
1
0-DIMETHOXY
1,6,7,11
B
-
TETRAHYDRO
-2H
BENZO
[
A
]
CHINOLIZIN
(170)
(VGL.
4.85).
---------------------------------------------------------
284
4.85
(2S,1
IBS)
(BZW.
2R,1
1
B
R)-2-(6,7-D
IMETHOXY
-
ISOCHINOLIN
-1
YLMETHYL
)-3
ETHYL
-9,10
DIMETHOXY
1,6,7,11
B-TETRAHYDRO-2/F-0ENZO[A]CHINOLIZIN
(170)
-----------------------------------------
288
4.86
(2R,3R,1
IBS)
(BZW.
2S,3S,1
LBR)-2-(6,7-DLMETHOXY-L,2,3,4-TETRAHYDRO-ISOCHINOL-IN-L
YLMETHYL)-3-ETHYL-9,10-DIMETHOXY-L,3,4,6,7,L
1B-HEXAHYDRO-2/ABENZO[A]
CHINOLIZIN
(166
A
)
---------------------------------------------------------------------------------------------------------------------------------------------------
290
4.87
(2R.3R.1
1
B
R
(BZW.
2S,3R,1
LBS)2-(6,7-DLMETHOXY-L,2,3,4-TETRAHYDRO-LSOCHLNO-LLN-L
YLMETHYL)-3-ETHYL-9,
1
0-DIMETHOXY
1,3,4,6,7,11
B-HEXAHYDRO-2//-BENZO[A]CHINOLIZIN
(1
66B)
---------------------------------------------------------------------------------------------------------------------------------------------------
294
4.88
2-(6,7-DLMETHOXY-ISOCHINOLIN-L-YLMETHYL)-3-ETHYL-9,10-DIMETHOXY-L,3,4,6,7,L
1
B
-
HEXAHYDRO
-2H
BENZO
[
A
]
CHINOLIZIN
(172)
------------------------------------------------------------------
299
4.89
(2S.3R,
11
BS)-2-((R)-6,7-DLMETHOXY
1
,2,3,4-TETRAHYDRO-ISOCHINOLIN
1
-YLMETHYL)-3-ETHYL
9,10-DIMERHOXY-L,3,4,6,7,L
1
B
-
HEXAHYDRO
-2/7
BENZO
[
A
]
CHINOLIZIN
(176)
F
LUKA
------------------
302
5
SPEKTRENANHANG
-----------------------------------------------------------------------------------------------------
306
6
LITERATURVERZEICHNIS
-------------------------------------------------------------------------------------------
334
7
LEBENSLAUF
----------------------------------------------------------------------------------------------------------------
340
V |
| any_adam_object | 1 |
| author | Renz, Manfred 1970- |
| author_GND | (DE-588)123592437 |
| author_facet | Renz, Manfred 1970- |
| author_role | aut |
| author_sort | Renz, Manfred 1970- |
| author_variant | m r mr |
| building | Verbundindex |
| bvnumber | BV014614634 |
| ctrlnum | (OCoLC)53805022 (DE-599)BVBBV014614634 |
| format | Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV014614634 |
| illustrated | Illustrated |
| indexdate | 2024-08-24T00:37:31Z |
| institution | BVB |
| isbn | 3897912341 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-012766196 |
| oclc_num | 53805022 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-12 DE-29T |
| owner_facet | DE-19 DE-BY-UBM DE-12 DE-29T |
| physical | V, 340 S. graph. Darst. : 21 cm |
| publishDate | 2001 |
| publishDateSearch | 2001 |
| publishDateSort | 2001 |
| publisher | Hieronymus |
| record_format | marc |
| series2 | Pharmazie |
| spelling | Renz, Manfred 1970- Verfasser (DE-588)123592437 aut Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen Manfred Renz München Hieronymus 2001 V, 340 S. graph. Darst. : 21 cm txt rdacontent n rdamedia nc rdacarrier Pharmazie Zugl.: München, Univ., Diss., 2001 Alkylierung (DE-588)4217435-1 gnd rswk-swf Chemische Synthese (DE-588)4133806-6 gnd rswk-swf Emetaminanaloga (DE-588)4692717-7 gnd rswk-swf Reissert-Verbindungen (DE-588)4550749-1 gnd rswk-swf Emetinanaloga (DE-588)4692692-6 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Emetinanaloga (DE-588)4692692-6 s Chemische Synthese (DE-588)4133806-6 s Reissert-Verbindungen (DE-588)4550749-1 s Alkylierung (DE-588)4217435-1 s DE-604 Emetaminanaloga (DE-588)4692717-7 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012766196&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Renz, Manfred 1970- Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen Alkylierung (DE-588)4217435-1 gnd Chemische Synthese (DE-588)4133806-6 gnd Emetaminanaloga (DE-588)4692717-7 gnd Reissert-Verbindungen (DE-588)4550749-1 gnd Emetinanaloga (DE-588)4692692-6 gnd |
| subject_GND | (DE-588)4217435-1 (DE-588)4133806-6 (DE-588)4692717-7 (DE-588)4550749-1 (DE-588)4692692-6 (DE-588)4113937-9 |
| title | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen |
| title_auth | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen |
| title_exact_search | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen |
| title_full | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen Manfred Renz |
| title_fullStr | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen Manfred Renz |
| title_full_unstemmed | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen Manfred Renz |
| title_short | Synthese 2,3-cis-konfigurierter Emetamin- und Emetin-Analoga durch doppelte Alkylierung von Reissert-Verbindungen |
| title_sort | synthese 2 3 cis konfigurierter emetamin und emetin analoga durch doppelte alkylierung von reissert verbindungen |
| topic | Alkylierung (DE-588)4217435-1 gnd Chemische Synthese (DE-588)4133806-6 gnd Emetaminanaloga (DE-588)4692717-7 gnd Reissert-Verbindungen (DE-588)4550749-1 gnd Emetinanaloga (DE-588)4692692-6 gnd |
| topic_facet | Alkylierung Chemische Synthese Emetaminanaloga Reissert-Verbindungen Emetinanaloga Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=012766196&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT renzmanfred synthese23ciskonfigurierteremetaminundemetinanalogadurchdoppeltealkylierungvonreissertverbindungen |