The HPLC solvent guide:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York
Wiley-Interscience
2002
|
| Ausgabe: | 2. ed. |
| Schlagworte: | |
| Online-Zugang: | Table of contents Inhaltsverzeichnis |
| Beschreibung: | XVIII, 643 S. graph. Darst. |
| ISBN: | 0471411388 |
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| 245 | 1 | 0 | |a The HPLC solvent guide |c Paul C. Sadek |
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| 300 | |a XVIII, 643 S. |b graph. Darst. | ||
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Datensatz im Suchindex
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| adam_text | CONTENTS
Preface xiü
Introduction xv
Abbreviations, Acronvms, and Symbols xvii
Chapter 1 Physical and Chemical Solvent Properties 1
1.1 UV Cutoff, 2
1.2 Absorbance Versus Wavelength Curves, 3
1.3 Reversed-Phase Solvents, 5
1.3.1 Mobile Phases and Mobile Phase Modifiers, 9
1.4 Normal-Phase Solvents, 11
1.5 System Peaks, 14
1.6 Lot-to-lot Solvent Variability, 16
1.7 Viscosity, 19
1.8 Miscibility and Solubility, 22
1.9 Buffers and Other Mobile Phase Additives, 25
1.10 Volatility, 29
1.11 Solvents: Instability, Reactivity, and Denaturants, 31
1.11.1 Ethers, 32
1.11.2 Chlorinated Alkanes, 34
1.11.3 Ethanol, 36
1.11.4 Water, 36
1.11.5 Acetone, 38
1.12 Sample Stability in Solvents, 39
1.13 Mobile Phase Interaction with Stationary Phase, 40
1.14 Inherent Contaminants, 41
1.15 Solvent Effects on Fluorescence, 42
1.16 Particulates and Solvent Filtering, 43
1.17 Manufacturers and Testing Protocols, 44
v
vi CONTENTS
Chapter 2 Method Optimization 45
2.1 Eluotropic Series and Solvent Strength Parameters, 46
2.1.1 Eluotropic Series, 46
2.1.2 Solvent Strength Parameters, 49
2.1.3 Mathematical Representation of Solvent Strength, 52
2.2 Triangulation and Other Algonthmic Methods, 53
2.3 Scout Gradients, 58
2.4 Window Diagrams, 60
2.5 Brute-force Method, 60
2.6 Other Optimization Techniques and Retention Parameters, 61
Chapter 3 Method Validation and Ongoing Performance Evaluation 63
3.1 Qualification Process, 64
3.1.1 Instrument Qualification, 64
3.1.2 Design Qualification, 65
3.1.3 Installation Qualification, 65
3.1.4 Operational Qualification, 66
3.1.5 Performance Qualification, 66
3.2 Method Validation, 67
3.2.1 Accuracy, 68
3.2.2 Precision, 68
3.2.3 Linearity, 69
3.2.4 Linear and Working Ranges, 71
3.2.5 Specificity, 72
3.2.6 Detection and Quantitation Limit, 72
3.2.7 Robustness, 73
3.2.8 Ruggedness, 73
3.3 System Suitability, 74
Chapter 4 Alcohols 75
4.1 Impurities, 81
4.2 General Analytes, 82
4.2.1 Simple Substituted Benzene Analytes, 82
4.2.2 Other Organic Compounds, 89
4.2.3 Organometallic Compounds and Metal-Ligand Complexes, 93
4.2.4 Summary, 96
4.3 Environmentally Important Analytes, 96
4.3.1 PAHs, Substituted PAHs, and Related Analytes, 96
4.3.2 Nitrated and Chlorinated Nonpesticide/Herbicide Pollutant
Analytes, 100
4.3.3 Pesticides, Herbicide, and Fungicides, 103
4.3.3.1 Pesticides, 103
4.3.3.2 Herbicides, 108
4.3.3.3 Fungicides, 111
4.3.4 Summary, 113
CONTENTS vii
4.4 Industrial and Polymer Analytes, 113
4.4.1 Surfactant and Additive Analytes, 113
4.4.2 Polymers and Polymer Additives, 115
4.4.3 Sunscreen Agents, 118
4.4.4 Dyes, 120
4.4.5 Other Industrial Analytes, 123
4.4.6 Summary, 124
4.5 Biological Analytes, 124
4.5.1 Carboxylic Acid Analytes, 124
4.5.2 Basic Amine Analytes, 130
4.5.3 Aflatoxins, Mycotoxms, and Other Toxic Analytes, 133
4.5.4 Vitamins and Related Analytes, 139
4.5.4.1 Water-soluble Vitamins and Related
Compounds, 139
4.5.4.2 Fat-soluble Vitamins and Related
Compounds, 140
4.5.5 Terpenoids, Flavonoids, and Related Compounds, 148
4.5.5.1 Terpenoids, 148
4.5.5.2 Flavanoids, 151
4.5.5.3 Caffeine and Related Compounds, 153
4.5.5.4 Other Compounds, 155
4.5.6 Analytes Derived from Oils and Fats, 169
4.5.7 Nucleotides, Nucleosides, and Related Analytes, 171
4.5.8 Other Analytes, 174
4.5.9 Summary, 178
4.6 Amino Acid, Peptide, and Protein Analytes, 178
4.6.1 Amino Acid Analytes, 178
4.6.2 Peptide Analytes, 180
4.6.3 Protein Analytes, 181
4.6.4 Summary, 184
4.7 Pharmaceutical Analytes, 184
4.7.1 Drug Surveys and Screening Procedures, 184
4.7.2 Retention Mechanisms for Drug Compounds, 186
4.7.3 NSAIDs and Analgesic Drugs, 187
4.7.4 Antibiotic Drugs, 189
4.7.5 Anticancer Drugs, 192
4.7.6 Antiepileptic Drugs, 195
4.7.7 Steroidal Drugs, 196
4.7.8 Anthelmintics, 198
4.7.9 Illicit Drugs, 199
4.7.10 Antihistamines, 201
4.7.11 Anti-HIV Drugs, 202
4.7.12 Antianxiety and Antipsychotic Drugs, 202
4.7.13 Other Drug Analytes, 204
4.7.14 Summary, 213
viii CONTENTS
Chapter 5 Alkanes and Alkyl Aromatics 214
5.1 Impurities, 216
5.2 General Analytes, 221
5.2.1 Simple Substituted Aromatic Analytes, 221
5.2.2 Organometallics and Metal-Ligand Complexes, 226
5.2.3 Summary, 227
5.3 Environmentally Important Analytes, 227
5.3.1 PAHs, Substituted PAHs, and Related Analytes, 227
5.3.2 Nitrated and Chlorinated Nonpesticide/herbicide Pollutant
Analytes, 230
5.3.3 Pesticide, Herbicide, and Fungicide Analytes, 231
5.3.4 Summary, 233
5.4 Industnal and Polymer Analytes, 233
5.4.1 Surfactant and Additive Analytes, 233
5.4.2 Other Polymeric Analytes, 235
5.4.3 Fullerenes, 236
5.4.4 Summary, 237
5.5 Biological Analytes, 238
5.5.1 Carboxylic Acid Analytes, 238
5.5.2 Vitamins and Related Analytes, 239
5.5.3 Terpenoids, Flavonoids, Steroids, and Related Compounds, 242
5.5.4 Analytes Derived from Oils and Fats, 244
5.5.5 Other Analytes, 248
5.5.6 Summary, 250
5.6 Amino Acid and Peptide Analytes, 250
5.6.1 Summary, 250
5.7 Pharmaceutical Analytes, 252
5.7.1 Cardiac Glycosides, 252
5.7.2 NSAIDs and Analgesic Drugs, 253
5.7.3 Benzodiazepines, 253
5.7.4 Other Analytes, 254
5.7.5 Summary, 257
Chapter 6 Chlorinated Alkanes and Chlorinated Benzenes 258
6.1 Impurities, 260
6.2 General Analytes, 266
6.2.1 Simple Substituted Benzene Analytes, 266
6.2.2 Organometallics and Metal-Ligand Complexes, 269
6.2.3 Summary, 269
6.3 Environmentally Important Analytes, 269
6.3.1 PAHs, Substituted PAHs, and Related Analytes, 269
6.3.2 Nitrated and Chlorinated Nonpesticide/herbicide Analytes, 271
6.3.3 Pesticide and Herbicide Analytes, 271
6.3.4 Summary, 272
CONTENTS ix
6.4 Industrial and Polymer Analytes, 272
6.4.1 Surfactant and Additive Analytes, 272
6.4.2 Polymeric Analytes, 273
6.4.3 Fullerenes, 274
6.4.4 Summary, 275
6.5 Biological Analytes, 275
6.5.1 Carboxylic Acid Analytes, 275
6.5.2 Vitamins and Related Analytes, 275
6.5.3 Analytes from Fats and Oils^ 277
6.5.4 Other Analytes, 278
6.5.5 Summary, 280
6.6 Amino Acid and Peptide Analytes, 280
6.7 Pharmaceutical Analytes, 281
Chapter 7 Ethers 285
7.1 Impurities, 287
7.2 General Analytes, 288
7.2.1 Simple Substituted Benzenes and Related Analytes, 288
7.3 Environmentally Important Analytes, 291
7.3.1 PAHs, Substituted PAHs, and Related Analytes, 291
7.3.2 Pesticide and Herbicide Residue Analytes, 292
7.4 Industrial and Polymer Analytes, 294
7.4.1 Surfactant and Additive Analytes, 294
7.4.2 Polymeric Analytes, 294
7.4.3 Fullerenes and Other Industrial Analytes, 296
7.5 Biological Analytes, 297
7.5.1 Carboxylic Acid Analytes, 297
7.5.2 Vitamins and Related Analytes, 298
7.5.3 Terpenoids, Flavonoids, Steroids, and Related Analytes, 300
7.5.4 Analytes Derived from Oils and Fats, 302
7.5.5 Other Analytes, 303
7.6 Amino Acid and Peptide Analytes, 305
7.7 Pharmaceutical Analytes, 305
7.7.1 Summary, 311
Chapter 8 Ketones and Esters 312
8.1 Impurities, 314
8.2 General Analytes, 316
8.3 Environmentally Important Analytes, 318
8.4 Industrial and Polymer Analytes, 319
8.5 Biological Analytes, 320
8.6 Pharmaceutical Analytes, 325
x CONTENTS
Chapter 9 Nitriles and Nitrogenous Solvents 327
9.1 Impurities, 328
9.2 General Analytes, 329
9.2.1 General Sample Solvent Considerations, 329
9.2.2 Simple Substiruted Hydrocarbons and Benzene Analyte Retention
Studies, 332
9.2.3 Other Compounds, 337
9.2.4 Organometallic and Metal-Ligand Complexes, 341
9.2.5 Summary, 343
9.3 Environmentally Important Analytes, 343
9.3.1 Substitutes Benzenes and Related Analytes, 343
9.3.2 PAHs, Substituted PAHs, and Related Analytes, 344
9.3.3 Nitro-, Nitroso-, and Chlorinated Nonpesticide/herbicide
Pollutant Analytes, 348
9.3.4 Pesticide, Herbicide, and Fungicide Analytes, 350
9.3.4.1 Pesticides, 350
9.3.4.2 Herbicides, 363
9.3.4.3 Fungicides, 368
9.3.4 Summary, 369
9.4 Industrial and Polymer Analytes, 370
9.4.1 Surfactant and Additive Analytes, 370
9.4.2 Polymeric Analytes, 373
9.4.3 Dyes and Related Analytes, 375
9.4.4 Other Industrial Analytes, 378
9.4.5 Personal Care and Cosmetic Analytes, 379
9.4.6 Summary, 380
9.5 Biological Analytes, 381
9.5.1 Carboxylic Acid Analytes, 381
9.5.2 Basic Amine Analytes, 387
9.5.3 Aflatoxins, Mycotoxins, and Other Toxic Analytes, 395
9.5.4 Vitamins and Related Analytes, 401
9.5.4.1 Water-soluble Vitamins and Related Compounds, 401
9.5.4.2 Fat-Soluble Vitamins and Related Compounds, 402
9.5.5 Terpenoids, Flavonoids, and Other Naturally Occurring
Analytes, 405
9.5.5.1 Terpenoids, 405
9.5.5.2 Flavanoids and Related Compounds, 408
9.5.5.3 Alkaloids and Related Compounds, 418
9.5.5.4 Fats, Oils, and Related Analytes, 425
9.5.6 Nucleotides, Nucleosides, and Related Analytes, 428
9.5.7 Sugars and Related Analytes, 430
9.5.8 Other Analytes, 433
9.5.9 Summary, 450
9.6 Amino Acid, Peptide, and Protein Analytes, 450
CONTENTS xi
9.6.1 Amino Acid Analytes, 450
9.6.2 Peptide Analytes, 452
9.6.3 Protein Analytes, 457
9.6.4 Summary, 459
9.7 Pharmaceutical Analytes, 459
9.7.1 Drug Surveys and Screening Procedures, 459
9.7.2 NSAIDs and Analgesic Drugs, 460
9.7.3 Antibiotic Drugs, 464
9.7.4 Anticancer Drugs, 476
9.7.5 Antiepüeptic Drugs, 482
9.7.6 Anthelmintics, 485
9.7.7 Illicit and Related Drugs, 487
9.7.8 Antihistammes, 490
9.7.9 Antiretroviral Drugs, 492
9.7.10 Antidepressants, 496
9.7.11 Antibacterial Drugs, 499
9.7.12 Anesthetics, 503
9.7.13 Immunosuppressants, 504
9.7.14 Analgesics, 505
9.7.15 Antihypercholesterolemic and Antihyperlipidemic Drugs, 506
9.7.16 Antihypertension Drugs, 507
9.7.17 Antimalarials, 511
9.7.18 Steroids, 512
9.7.19 Antipsychotics, 515
9.7.20 Other Drug Analytes, 518
9.8 Summary, 527
Chapter 10 Water, Dimethyl Sulfoxide, and Common Acidic Modifiers 531
10.1 General Considerations and Impurities, 531
10.1.2 Solvent Preparation, 532
10.2 Industrial Analytes, 535
10.3 Biological Analytes, 538
10.3.1 Carboxylic Acid Analytes, 539
10.3.2 Basic Amine Analytes, 540
10.3.3 Toxins, 541
10.3.4 Vitamins, 542
10.3.5 Nucleotides, Nucleosides, Amino Acids, and Peptides, 543
10.3.6 Terpenoids, Flavonoids, and Related Analytes, 545
10.4 Pharmaceutical Analytes, 546
10.5 Summary, 547
10.6 Dimethyl Sulfoxide, 549
References 552
Index 607
|
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| isbn | 0471411388 |
| language | English |
| lccn | 2002275754 |
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| spelling | Sadek, Paul C. Verfasser aut The HPLC solvent guide Paul C. Sadek 2. ed. New York Wiley-Interscience 2002 XVIII, 643 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier High-performance liquid chromatography Equipment and supplies Solvents HPLC (DE-588)4072641-1 gnd rswk-swf Mobile Phase (DE-588)4245386-0 gnd rswk-swf HPLC (DE-588)4072641-1 s Mobile Phase (DE-588)4245386-0 s DE-604 http://www.loc.gov/catdir/toc/wiley022/2002275754.html Table of contents HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009869469&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Sadek, Paul C. The HPLC solvent guide High-performance liquid chromatography Equipment and supplies Solvents HPLC (DE-588)4072641-1 gnd Mobile Phase (DE-588)4245386-0 gnd |
| subject_GND | (DE-588)4072641-1 (DE-588)4245386-0 |
| title | The HPLC solvent guide |
| title_auth | The HPLC solvent guide |
| title_exact_search | The HPLC solvent guide |
| title_full | The HPLC solvent guide Paul C. Sadek |
| title_fullStr | The HPLC solvent guide Paul C. Sadek |
| title_full_unstemmed | The HPLC solvent guide Paul C. Sadek |
| title_short | The HPLC solvent guide |
| title_sort | the hplc solvent guide |
| topic | High-performance liquid chromatography Equipment and supplies Solvents HPLC (DE-588)4072641-1 gnd Mobile Phase (DE-588)4245386-0 gnd |
| topic_facet | High-performance liquid chromatography Equipment and supplies Solvents HPLC Mobile Phase |
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