Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Stuttgart
Max-Planck-Inst. für Metallforschung
2002
|
| Schriftenreihe: | Bericht / Max-Planck-Institut für Metallforschung
Nr. 114 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zugl.: Stuttgart, Univ., Diss., 2002 |
| Beschreibung: | 128 S. Ill., graph. Darst. : 21 cm |
Internformat
MARC
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| 245 | 1 | 0 | |a Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics |c vorgelegt von Haihui Ye. Institut für Nichtmetallische Anorganische Materialien der Universität Stuttgart ... |
| 264 | 1 | |a Stuttgart |b Max-Planck-Inst. für Metallforschung |c 2002 | |
| 300 | |a 128 S. |b Ill., graph. Darst. : 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Bericht / Max-Planck-Institut für Metallforschung |v Nr. 114 | |
| 500 | |a Zugl.: Stuttgart, Univ., Diss., 2002 | ||
| 650 | 0 | 7 | |a Mikrostruktur |0 (DE-588)4131028-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Sintern |0 (DE-588)4140299-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Korngrenze |0 (DE-588)4137128-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Chemische Eigenschaft |0 (DE-588)4371174-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Flüssiger Zustand |0 (DE-588)4336025-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Siliciumcarbid |0 (DE-588)4055009-6 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Siliciumcarbid |0 (DE-588)4055009-6 |D s |
| 689 | 0 | 1 | |a Sintern |0 (DE-588)4140299-6 |D s |
| 689 | 0 | 2 | |a Flüssiger Zustand |0 (DE-588)4336025-7 |D s |
| 689 | 0 | 3 | |a Korngrenze |0 (DE-588)4137128-8 |D s |
| 689 | 0 | 4 | |a Mikrostruktur |0 (DE-588)4131028-7 |D s |
| 689 | 0 | 5 | |a Chemische Eigenschaft |0 (DE-588)4371174-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Ye, Haihui |d 1972- |e Sonstige |0 (DE-588)123750067 |4 oth | |
| 810 | 2 | |a Max-Planck-Institut für Metallforschung |t Bericht |v Nr. 114 |w (DE-604)BV010796017 |9 114 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009831798&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-009831798 | |
Datensatz im Suchindex
| _version_ | 1808136439358029824 |
|---|---|
| adam_text |
TABLE
OF
CONTENTS
ABSTRACT
.
2
ACKNOLEDGEMENTS
.
4
TABLE
OF CONTENTS
.
5
LIST
OF
SYMBOLS
AND ABBREVIATIONS
.
7
1
INTRODUCTION
.
9
2
REVIEW
OF
SINTERING
AND
MICROSTRUCTURES
OF
SIC-BASED
CERAMICS
.
11
2.1
STRUCTURAL
PROPERTIES
OF
SIC
.
11
2.2
SINTERING
OF
SIC
.
12
2.2.1
DIFFICULTIES
IN
SINTERING
.
12
2.2.2
SOLID-STATE
SINTERING
.
13
2.2.3
LIQUID-PHASE
SINTERING
.
13
2.3
MICROSTRUCTURE
FEATURES
OF
LIQUID-PHASE
SINTERED
SIC
.
16
2.3.1
PHASE
TRANSFORMATION
.
16
2.3.2
COARSENING
AND
SOLUTION-REPRECIPITATION
PROCESS
.
17
2.3.3
EFFECT
OF
SINTERING
ATMOSPHERE
ON
MICROSTRUCTURES
.
17
2.4
GRAIN-BOUNDARY
FILMS
AND
TRIPLE-JUNCTION
PHASES
OF
SIC
CERAMICS
.
18
2.4.1
STABILITY
OF
GRAIN-BOUNDARY
FILMS
IN
CERAMIC
MATERIALS
.
18
2.4.2
GRAIN-BOUNDARY
FILMS
IN
LIQUID-PHASE
SINTERED
SIC
.
19
2.4.3
TRIPLE-JUNCTION
PHASES
AND
THEIR
CRYSTALLIZATION
.
21
3
CHARACTERIZATION
METHOD
-
ELECTRON
MICROSCOPY
.
27
3.1
INTERACTIONS
BETWEEN
ELECTRONS
AND
MATTER
.
27
3.2
SCANNING
ELECTRON
MICROSCOPY
AND
X-RAY
MICROANALYSIS
.
28
3.3
TRANSMISSION
ELECTRON
MICROSCOPY
.
29
3.4
HIGH
RESOLUTION
TRANSMISSION
ELECTRON
MICROSCOPY
.
30
3.5
ELECTRON
ENERGY-LOSS
SPECTROMETRY
.
32
3.6
SPECIMEN
PREPARATION
FOR
TEM
.
34
4
THE
MODEL
SYSTEM
SIC-SIOJ
.
41
4.1
INTRODUCTION
.
41
4.2
EXPERIMENTAL
PROCEDURE
.
41
4.3
DENSIFICATION
.
42
4.3.1
EFFECT
OF
SINTERING
TEMPERATURE
.
42
6
4.3.2
EFFECT
OF
THE
SIO
2
CONTENT
.
43
4.4
GRAIN-BOUNDARY
FILMS
.
44
4.4.1
HRTEM
OBSERVATIONS
AND
EELS
COMPOSITIONAL
ANALYSES
.
44
4.4.2
CALCULATIONS
BASED
ON
CLARKE
'
S
MODEL
.
44
4.5
SI
2
N
2
O
CRYSTALLIZATION
IN
TRIPLE
JUNCTIONS
.
46
4.6
CRACK
DEFLECTION
.
47
5
THE
"
COARSE
SIC
"
MODEL
SYSTEM
.
62
5.1
INTRODUCTION
.
62
5.2
EXPERIMENTAL
PROCEDURE
.
62
5.3
OVERALL
MICROSTRUCTURE
AND
COMPOSITION
.
63
5.4
CHEMICAL
COMPOSITION
OF
INTERGRANULAR
PHASES
.
65
5.5
CRYSTALLINE
INTERGRANULAR
PHASES
.
66
5.6
EFFECT
OF
NITROGEN
INCORPORATION
.
67
6
LPS-SIC
WITH
Y
2
O
3
-A1N
ADDITIVES
.
77
6.1
INTRODUCTION
.
77
6.2
EXPERIMENTAL
PROCEDURE
.
77
6.3
DENSIFICATION
.
78
6.4
EFFECT
OF
SINTERING
ATMOSPHERE
ON
GRAIN
GROWTH
AND
DENSIFICATION
.
79
6.5
SIC
GRAIN
MORPHOLOGY
AND
PHASE
TRANSFORMATION
.
80
6.6
GRAIN-BOUNDARY
FILMS
.
81
6.6.1
HRTEM
OBSERVATION
.
81
6.6.2
EELS
ANALYSES
AND
ELEMENT
EXCESS
.
82
6.6.3
ELNES
ANALYSES
AND
BONDING
INFORMATION
.
83
6.7
TRIPLE-JUNCTION
PHASES
.
83
6.7.1
TRIPLE
JUNCTIONS
AND
LARGE
POCKETS
.
83
6.7.2
CRYSTALLIZATION
OF
PHASES
AT
TRIPLE
JUNCTIONS
AND
LARGE
POCKETS
.
84
6.7.3
IDENTIFICATION
OF
THE
SECONDARY
CRYSTALLINE
PHASES
.
84
6.7.4
EELS
ANALYSES
AND
CONFIRMATION
OF
N-RICH
TRIPLE-JUNCTION
PHASES
.
85
6.7.5
DISTRIBUTION
OF
ELEMENTS
ACROSS
TRIPLE-JUNCTION
PHASES
.
86
7
SUMMARY
AND
CONCLUSIONS
.
109
ZUSAMMENFASSUNG
.
111
REFERENCES
.
121
CURRICULUM
VITAE
(LEBENSLAUF)
.
128 |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV014331561 |
| illustrated | Illustrated |
| indexdate | 2024-08-23T00:34:42Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009831798 |
| open_access_boolean | |
| physical | 128 S. Ill., graph. Darst. : 21 cm |
| publishDate | 2002 |
| publishDateSearch | 2002 |
| publishDateSort | 2002 |
| publisher | Max-Planck-Inst. für Metallforschung |
| record_format | marc |
| series2 | Bericht / Max-Planck-Institut für Metallforschung |
| spelling | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics vorgelegt von Haihui Ye. Institut für Nichtmetallische Anorganische Materialien der Universität Stuttgart ... Stuttgart Max-Planck-Inst. für Metallforschung 2002 128 S. Ill., graph. Darst. : 21 cm txt rdacontent n rdamedia nc rdacarrier Bericht / Max-Planck-Institut für Metallforschung Nr. 114 Zugl.: Stuttgart, Univ., Diss., 2002 Mikrostruktur (DE-588)4131028-7 gnd rswk-swf Sintern (DE-588)4140299-6 gnd rswk-swf Korngrenze (DE-588)4137128-8 gnd rswk-swf Chemische Eigenschaft (DE-588)4371174-1 gnd rswk-swf Flüssiger Zustand (DE-588)4336025-7 gnd rswk-swf Siliciumcarbid (DE-588)4055009-6 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Siliciumcarbid (DE-588)4055009-6 s Sintern (DE-588)4140299-6 s Flüssiger Zustand (DE-588)4336025-7 s Korngrenze (DE-588)4137128-8 s Mikrostruktur (DE-588)4131028-7 s Chemische Eigenschaft (DE-588)4371174-1 s DE-604 Ye, Haihui 1972- Sonstige (DE-588)123750067 oth Max-Planck-Institut für Metallforschung Bericht Nr. 114 (DE-604)BV010796017 114 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009831798&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics Mikrostruktur (DE-588)4131028-7 gnd Sintern (DE-588)4140299-6 gnd Korngrenze (DE-588)4137128-8 gnd Chemische Eigenschaft (DE-588)4371174-1 gnd Flüssiger Zustand (DE-588)4336025-7 gnd Siliciumcarbid (DE-588)4055009-6 gnd |
| subject_GND | (DE-588)4131028-7 (DE-588)4140299-6 (DE-588)4137128-8 (DE-588)4371174-1 (DE-588)4336025-7 (DE-588)4055009-6 (DE-588)4113937-9 |
| title | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics |
| title_auth | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics |
| title_exact_search | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics |
| title_full | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics vorgelegt von Haihui Ye. Institut für Nichtmetallische Anorganische Materialien der Universität Stuttgart ... |
| title_fullStr | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics vorgelegt von Haihui Ye. Institut für Nichtmetallische Anorganische Materialien der Universität Stuttgart ... |
| title_full_unstemmed | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics vorgelegt von Haihui Ye. Institut für Nichtmetallische Anorganische Materialien der Universität Stuttgart ... |
| title_short | Microstructure and chemistry of grain-boundary films and triple-junction phases in liquid-phase sintered SiC ceramics |
| title_sort | microstructure and chemistry of grain boundary films and triple junction phases in liquid phase sintered sic ceramics |
| topic | Mikrostruktur (DE-588)4131028-7 gnd Sintern (DE-588)4140299-6 gnd Korngrenze (DE-588)4137128-8 gnd Chemische Eigenschaft (DE-588)4371174-1 gnd Flüssiger Zustand (DE-588)4336025-7 gnd Siliciumcarbid (DE-588)4055009-6 gnd |
| topic_facet | Mikrostruktur Sintern Korngrenze Chemische Eigenschaft Flüssiger Zustand Siliciumcarbid Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009831798&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV010796017 |
| work_keys_str_mv | AT yehaihui microstructureandchemistryofgrainboundaryfilmsandtriplejunctionphasesinliquidphasesinteredsicceramics |