New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Göttingen
Cuvillier
2002
|
| Ausgabe: | 1. Aufl. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zugl.: Göttingen, Univ., Diss., 2002 |
| Beschreibung: | VI, 132 S. |
| ISBN: | 3898733629 |
Internformat
MARC
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| 001 | BV014257309 | ||
| 003 | DE-604 | ||
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| 016 | 7 | |a 964183153 |2 DE-101 | |
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| 035 | |a (DE-599)BVBBV014257309 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a eng | |
| 044 | |a gw |c DE | ||
| 049 | |a DE-703 | ||
| 100 | 1 | |a Bai, Guangcai |d 1962- |e Verfasser |0 (DE-588)123706963 |4 aut | |
| 245 | 1 | 0 | |a New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides |c vorgelegt von Guangcai Bai |
| 250 | |a 1. Aufl. | ||
| 264 | 1 | |a Göttingen |b Cuvillier |c 2002 | |
| 300 | |a VI, 132 S. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Zugl.: Göttingen, Univ., Diss., 2002 | ||
| 650 | 7 | |a Hochschulschrift |2 gtt | |
| 650 | 0 | 7 | |a Chemische Synthese |0 (DE-588)4133806-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Stickstoffverbindungen |0 (DE-588)4183288-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Übergangsmetallkomplexe |0 (DE-588)4131837-7 |2 gnd |9 rswk-swf |
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| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Vierte Nebengruppe |0 (DE-588)4344825-2 |D s |
| 689 | 0 | 1 | |a Übergangsmetallkomplexe |0 (DE-588)4131837-7 |D s |
| 689 | 0 | 2 | |a Stickstoffverbindungen |0 (DE-588)4183288-7 |D s |
| 689 | 0 | 3 | |a Chemische Synthese |0 (DE-588)4133806-6 |D s |
| 689 | 0 | |5 DE-604 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009777220&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-009777220 | |
Datensatz im Suchindex
| _version_ | 1808045645106249728 |
|---|---|
| adam_text |
TABLE
OF
CONTENTS
I
1.
INTRODUCTION
.
1
1.1.
REACTIONS
OF
ALKALI
METAL
AMMONIA
SOLUTIONS
WITH
METAL
COMPOUNDS
.
1
1.2.
AMIDO
(NH
2
~),
IMIDO
(NH
2
"
),
AND
NITRIDO
(N
3
TRANSITION
METAL
COMPOUNDS
.
3
1.3.
GROUP
4
ORGANOMETALLIC
IMIDO
(RN
2
)
COMPLEXES
.
6
1.4.
HYDROLYSIS
OF
GROUP
4
ORGANOMETALLIC
COMPOUNDS
.
7
1.5.
REACTIONS
OF
DIAZOMETHANE
DERIVATIVES
WITH
GROUP
4
ORGANOMETALLIC
COMPOUNDS
.
8
1.6.
SCOPE
AND
AIM
OF
THE
PRESENT
WORK
.
9
2.
RESULTS
AND
DISCUSSION
.
11
2.1.
SYNTHESES
OF
AMIDO
(NH
2
"
),
IMIDO
(NH
2
),
AND
NITRIDO
(N
3
*)
GROUP
4
METAL
COMPOUNDS
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
SYSTEM
.
11
2.1.1.
SYNTHESES
AND
CHARACTERIZATION
OF
THE
POLYAMIDOIMIDONITRIDO
SQUARE
PYRAMIDAL
ZIRCONIUM
CLUSTER
[{(MEC5H
4
)ZR}
5
(
(
U5-N)(
I
U3-NH)4(/Z-NH2)4]
(3)
AND
THE
ORGANOPOTASSIUM
POLYMER
[(MEC
5
H
4
)K]
N
(4)
.
13
2.1.2.
SYNTHESIS
AND
CHARACTERIZATION
OF
AN
IMIDO
(NH
"
)
BRIDGED
DINUCLEAR
ZIRCONIUM
COMPLEX
[(R/-L)ZR(^-NH)]
2
(9,
L
=
(PNRBU)
2
(TBUN)
2
)
.
20
2.1.3.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
POLYIMIDONITRIDO
OCTAHEDRAL
TITANIUM
CLUSTER
[(L'TI)
6
(^3-NH)
6
(^3-N)2-6(C7H
8
)]
(10,
L'
=
^-MEC
6
H4C(NSIME3)2))
.
23
2.1.4.
SYNTHESIS
AND
CHARACTERIZATION
OF
CP*2TINH
2
(11)
.
27
2.2.
SYNTHESIS
OF
A
METAL
DINITROGEN
COMPLEX
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
SYSTEM
.
29
2.2.1.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
IMIDO
TITANIUM(II)/TITANIUM(III)
POTASSIUM
DINITROGEN
COMPLEX
[(CP*TI)4(U3-NH)
4
CU4-7
1
:
RI':
RF:
//-NJHKJ]
(12)
.
30
2.3.
SYNTHESES
OF
POLYOXO
METAL
ORGANIC
CLUSTERS
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
II
TABLE
OF
CONTENTS
SYSTEM
.
35
2.3.1.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
POLYOXOZIRCONIUM
CLUSTER
[{(ETME4C5)ZR}
6
(/Z
6
-O)(/I
3
-
O)
8
-(C
7
H
8
)]
(13)
.
35
2.3.2.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
POLYOXOZIRCONIUM
CLUSTER
[{(ETME^SJZRJSCUS-O)^
O)
8
-(C,H
12
)]
(16)
.
41
2.3.3.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
POLYOXOZIRCONIUM
HYDROXIDE
[(CP*ZR)S()U
6
-O)(P5
O)
4
(^
3
-OH)
8
-2(C
7
H
8
)]
(17)
.
44
2.3.4.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
VANADIUM(IV)/VANADIUM(V)
SODIUM
OXIDE
(CP'V)
6
(^-O)
8
(^3-O)2NA
(19)
.
50
2.4.
SYNTHESIS
OF
A
ZIRCONIUM
DIHYDRIDE
IN
A
LIQUID
AMMONIA/TOIUENE
TWO
PHASE
SYSTEM.
55
2.4.1.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
IMIDO-MTSA-ZIRCONOCENE
DIHYDRIDE
[
{HN(SIME
2
C
5
H4)2ZRH(A-H)}
2
C
7
H
8
]
(20)
.
55
2.5.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
TITANIUM(HI)
COMPOUND
L'JTI
(21,
L'
=
P
MEC
4
H
4
C(NSIME
3
)
2
)
.
58
2.6.
SYNTHESES
OF
NITROGEN
CONTAINING
TITANIUM
AND
ZIRCONIUM
COMPOUNDS
VIA
THE
REACTIONS
OF
CORRESPONDING
METAL
COMPOUNDS
WITH
DIAZO
DERIVATIVES
AND
ANILINE.
62
2.6.1.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
IMIDO
(NSIMEJ)
BRIDGED
DINUCLEAR
TITANIUM
COMPOUND
[(MEC
5
H4)TICL(/Z-NSIME
3
)]2
(22)
.
62
2.6.2.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
^-HYDRAZONATO
ZIRCONIUM
COMPLEX
CPJZRCKZ/
2
-
NHNCHSIME
3
)
C
7
H
8
(23)
.
65
2.6.3.
SYNTHESIS
AND
CHARACTERIZATION
OF
THE
IMIDO
(NPH)
BRIDGED
DINUCLEAR
ZIRCONIUM
COMPOUND
[CL
2
ZR(^-NPH)-2THF]2
(24)
.
67
2.7.
SYNTHESES
OF
BIS(TERT-BUTYIAMIDO)CYCLODIPHOSPH(HI)AZANE
ZIRCONIUM
COMPLEXES
.
69
2.7.1.
SYNTHESIS
AND
CHARACTERIZATION
OF
LZRCH
(25,
L
=
(PNTBU)
2
(/BUN)
2
))
.
70
2.7.2.
SYNTHESIS
AND
CHARACTERIZATION
OF
(7
3
-L)(7
1
-LH)ZRCL
(26,
L
=
(PNTBU)2(TBUN)
2
))
.
70
2.7.3.
SYNTHESIS
AND
CHARACTERIZATION
OF
[(?/-LH)ZR(NRBU){(NRBU)2PPNRBU}{K'(7
6
-
C
7
H
8
)}-0.5C
7
H
8
]
(27,
L
=
(PN/BU)
2
(/BUN)
2
))
.
74
TABLE
OF
CONTENTS
III
3.
SUMMARY
AND
OUTLOOK
.
79
3.1.
SUMMARY
.
79
3.2.
OUTLOOK
.
86
4.
EXPERIMENTAL
SECTION
.
89
4.1.
GENERAL
PROCEDURES
.
89
4.2.
PHYSICAL
MEASUREMENTS
.
89
4.3.
STARTING
MATERIALS
.
90
4.4.
SYNTHESES
OF
AMIDO
(NHJ
-
),
IMIDO
(NH
2
),
AND
NITRIDO(N
3
3
GROUP
IV
METAL
COMPOUNDS
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
SYSTEM
.
90
4.4.1.
SYNTHESISS
OF
[{(MEC
5
H
4
)ZR}
5
(^5-N)GZ3-NH)4CU-NH2)4]
(3)
AND
(MECSHDQ,,
(4)
.
90
4.4.2.
SYNTHESIS
OF
[(Z/
3
-L)ZR(//-NH)]
2
(9)
.
92
4.4.3.
SYNTHESIS
OF
[(LTI)
6
CU
3
-NH)
6
(/Z3-N)2-6(C
7
H
8
)]
(10)
.
92
4.4.4.
SYNTHESIS
OF
CP
2
'TINH2
(11)
.
93
4.5.
SYNTHESIS
OF
((CP'TI^CZ^-NHHTUJ-T;'://:;;
2
:?;
2
-^):!^]
(12)
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
SYSTEM
.
94
4.6.
SYNTHESES
OF
ORGANOMETALLIC
OXIDES
AND
HYDROXIDES
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
SYSTEM
.
94
4.6.1.
SYNTHESIS
OF
[{(ETME4C
5
)ZR}
6
(/4
6
-O)(
1
U3-O)
8
-(C
7
H
8
)]
(13)
.
94
4.6.2.
SYNTHESIS
OF
[{(ETME
4
C5)ZR}
6
CU
6
-O)CU3-O)
8
-(C
9
HI2)]
(16)
.
95
4.6.3.
SYNTHESIS
OF
[(CP'ZR)
6
CU
6
-O)(A3-O)
4
(U3-OH)
8
-2(C
7
H
8
)]
(17)
.
95
4.6.4.
SYNTHESES
OF
[CP*VCL(^-O)]4-OC
4
H
8
(18)
AND
(CP
'
V)
6
G-O)
8
(U3-O)2NA
(19)
.
96
4.7.
SYNTHESIS
OF
[{HN(SIME
2
C
5
H4)2ZRH04-H)}2
C
7
H
8
]
(20)
IN
A
LIQUID
AMMONIA/TOLUENE
TWO
PHASE
SYSTEM
.
96
IV
TABLE
OF
CONTENTS
4.8.
SYNTHESIS
OF
L'
3
TI
(21)
BY
THE
REDUCTION
OF
L'JTICLJ
WITH
ALKALI
METAL
AMMONIA
SOLUTIONS
IN
TOLUENE
.
97
4.9.
SYNTHESES
OF
NITROGEN
CONTAINING
TITANIUM
AND
ZIRCONIUM
COMPOUNDS
VIA
THE
REACTIONS
OF
CORRESPONDING
METAL
COMPOUNDS
WITH
DIAZO
DERIVATIVES
AND
ANILINE.
.98
4.9.1.
SYNTHESIS
OF
[(MEC
5
H4)TICL(U-NSIME
3
)]
2
(22)
.
98
4.9.2.
SYNTHESIS
OF
CP
2
ZRCL(
7
/
2
-NHNCHSIME
3
)C
7
H
8
(23)
.
98
4.9.3.
SYNTHESIS
OF
[CL
2
ZR(/Z-NPH)-2THF]
2
(24)
.
99
4.10.
SYNTHESES
OF
BIS(TERT-BUTYLAMIDO)CYCLODIPHOSPH(III)AZANE
ZIRCONIUM
COMPLEXES
.
100
4.10.1.
SYNTHESIS
OF
LZRCL
2
(25)
.
100
4.10.2.
SYNTHESIS
OF
(T;
3
-L)(7'-LH)ZRCL
(26)
.
100
4.10.3.
SYNTHESIS
OF
[(^'-LH)ZR(NTBU){(NTBU)
2
PPN/BU}
{K(Z7
6
-C
7
H
G
)}-0.5C
7
H
G
]
(27)
.
101
5.
HANDLING
AND
DISPOSAL
OF
SOLVENTS
AND
RESIDUAL
WASTE
.
102
6.
CRYSTAL
DATA
AND
REFINEMENT
DETAILS
.
103
7.
REFERENCES
.
120 |
| any_adam_object | 1 |
| author | Bai, Guangcai 1962- |
| author_GND | (DE-588)123706963 |
| author_facet | Bai, Guangcai 1962- |
| author_role | aut |
| author_sort | Bai, Guangcai 1962- |
| author_variant | g b gb |
| building | Verbundindex |
| bvnumber | BV014257309 |
| ctrlnum | (OCoLC)50459672 (DE-599)BVBBV014257309 |
| edition | 1. Aufl. |
| format | Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV014257309 |
| illustrated | Not Illustrated |
| indexdate | 2024-08-22T00:31:32Z |
| institution | BVB |
| isbn | 3898733629 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009777220 |
| oclc_num | 50459672 |
| open_access_boolean | |
| owner | DE-703 |
| owner_facet | DE-703 |
| physical | VI, 132 S. |
| publishDate | 2002 |
| publishDateSearch | 2002 |
| publishDateSort | 2002 |
| publisher | Cuvillier |
| record_format | marc |
| spelling | Bai, Guangcai 1962- Verfasser (DE-588)123706963 aut New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides vorgelegt von Guangcai Bai 1. Aufl. Göttingen Cuvillier 2002 VI, 132 S. txt rdacontent n rdamedia nc rdacarrier Zugl.: Göttingen, Univ., Diss., 2002 Hochschulschrift gtt Chemische Synthese (DE-588)4133806-6 gnd rswk-swf Stickstoffverbindungen (DE-588)4183288-7 gnd rswk-swf Übergangsmetallkomplexe (DE-588)4131837-7 gnd rswk-swf Vierte Nebengruppe (DE-588)4344825-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Vierte Nebengruppe (DE-588)4344825-2 s Übergangsmetallkomplexe (DE-588)4131837-7 s Stickstoffverbindungen (DE-588)4183288-7 s Chemische Synthese (DE-588)4133806-6 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009777220&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Bai, Guangcai 1962- New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides Hochschulschrift gtt Chemische Synthese (DE-588)4133806-6 gnd Stickstoffverbindungen (DE-588)4183288-7 gnd Übergangsmetallkomplexe (DE-588)4131837-7 gnd Vierte Nebengruppe (DE-588)4344825-2 gnd |
| subject_GND | (DE-588)4133806-6 (DE-588)4183288-7 (DE-588)4131837-7 (DE-588)4344825-2 (DE-588)4113937-9 |
| title | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides |
| title_auth | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides |
| title_exact_search | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides |
| title_full | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides vorgelegt von Guangcai Bai |
| title_fullStr | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides vorgelegt von Guangcai Bai |
| title_full_unstemmed | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides vorgelegt von Guangcai Bai |
| title_short | New methods for the syntheses of amido, imido, nitrido and dinitrogen metal complexes and organometallic hydrides and oxides |
| title_sort | new methods for the syntheses of amido imido nitrido and dinitrogen metal complexes and organometallic hydrides and oxides |
| topic | Hochschulschrift gtt Chemische Synthese (DE-588)4133806-6 gnd Stickstoffverbindungen (DE-588)4183288-7 gnd Übergangsmetallkomplexe (DE-588)4131837-7 gnd Vierte Nebengruppe (DE-588)4344825-2 gnd |
| topic_facet | Hochschulschrift Chemische Synthese Stickstoffverbindungen Übergangsmetallkomplexe Vierte Nebengruppe |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009777220&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT baiguangcai newmethodsforthesynthesesofamidoimidonitridoanddinitrogenmetalcomplexesandorganometallichydridesandoxides |