Electroanalytical methods: guide to experiments and applications ; with 31 tables
Gespeichert in:
Format: | Buch |
---|---|
Sprache: | English |
Veröffentlicht: |
Berlin [u.a.]
Springer
2002
|
Schlagworte: | |
Online-Zugang: | Inhaltsverzeichnis |
Beschreibung: | XXII, 331 S. Ill., graph. Darst. |
ISBN: | 3540422293 |
Internformat
MARC
LEADER | 00000nam a22000008c 4500 | ||
---|---|---|---|
001 | BV014072179 | ||
003 | DE-604 | ||
005 | 20181018 | ||
007 | t | ||
008 | 011218s2002 gw ad|| |||| 00||| eng d | ||
016 | 7 | |a 963084844 |2 DE-101 | |
020 | |a 3540422293 |9 3-540-42229-3 | ||
035 | |a (OCoLC)248330062 | ||
035 | |a (DE-599)BVBBV014072179 | ||
040 | |a DE-604 |b ger |e rakddb | ||
041 | 0 | |a eng | |
044 | |a gw |c DE | ||
049 | |a DE-703 |a DE-29T |a DE-19 |a DE-355 |a DE-M49 |a DE-526 |a DE-634 |a DE-83 |a DE-11 | ||
050 | 0 | |a QD115 | |
082 | 0 | |a 543.0871 | |
084 | |a VG 8000 |0 (DE-625)147212:253 |2 rvk | ||
084 | |a CHE 224f |2 stub | ||
245 | 1 | 0 | |a Electroanalytical methods |b guide to experiments and applications ; with 31 tables |c F. Scholz (ed.). With contributions by A. M. Bond ... |
264 | 1 | |a Berlin [u.a.] |b Springer |c 2002 | |
300 | |a XXII, 331 S. |b Ill., graph. Darst. | ||
336 | |b txt |2 rdacontent | ||
337 | |b n |2 rdamedia | ||
338 | |b nc |2 rdacarrier | ||
650 | 4 | |a Elektroanalyse - Aufsatzsammlung | |
650 | 4 | |a Electrochemical analysis | |
650 | 0 | 7 | |a Elektroanalyse |0 (DE-588)4014237-1 |2 gnd |9 rswk-swf |
655 | 7 | |0 (DE-588)4143413-4 |a Aufsatzsammlung |2 gnd-content | |
689 | 0 | 0 | |a Elektroanalyse |0 (DE-588)4014237-1 |D s |
689 | 0 | |5 DE-604 | |
700 | 1 | |a Scholz, Fritz |d 1955- |e Sonstige |0 (DE-588)143718231 |4 oth | |
700 | 1 | |a Bond, Alan M. |d 1946- |e Sonstige |0 (DE-588)105306201X |4 oth | |
856 | 4 | 2 | |m SWB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009638370&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-009638370 |
Datensatz im Suchindex
_version_ | 1807228929788870656 |
---|---|
adam_text |
CONTENTS PART I BASIC ELECTROCHEMISTRY . . . . . . . . . . . . . . . . .
. . . . . . 1 I.1 THE ELECTRICAL DOUBLE LAYER AND ITS STRUCTURE . . . .
. . . . . . 3 Z. STOJEK I.1.1 INTRODUCTION . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . 3 I.1.2 DOUBLE-LAYER MODELS . . . . . . . .
. . . . . . . . . . . . . . . . 5 I.1.3 THICKNESS OF THE ELECTRIC DOUBLE
LAYER . . . . . . . . . . . . . . 7 I.1.4 RECENT DEVELOPMENTS . . . . .
. . . . . . . . . . . . . . . . . . . 8 REFERENCES . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . 8 I.2 THERMODYNAMICS OF
ELECTROCHEMICAL REACTIONS . . . . . . . . . 9 F. SCHOLZ I.2.1
INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 9
I.2.2 THE STANDARD POTENTIAL . . . . . . . . . . . . . . . . . . . . . .
. 9 I.2.3 THE FORMAL POTENTIAL . . . . . . . . . . . . . . . . . . . . .
. . . 16 I.2.4 CHARACTERISTIC POTENTIALS OF ELECTROANALYTICAL TECHNIQUES
. . . . 18 I.2.4.1 DIRECT CURRENT POLAROGRAPHY (EMPLOYING A
DROPPING-MERCURY ELECTRODE) . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . 18 I.2.4.2 CYCLIC VOLTAMMETRY . . . . . . . . . . . . .
. . . . . . . . . . . . 22 I.2.4.3 DIFFERENTIAL PULSE VOLTAMMETRY (DPV),
ALTERNATING CURRENT VOLTAMMETRY (ACV) AND SQUARE WAVE VOLTAMMETRY (SWV)
. . 23 I.2.5 THERMODYNAMICS OF THE TRANSFER OF IONS BETWEEN TWO PHASES
23 I.2.6 THERMODYNAMIC DATA DERIVED FROM STANDARD AND FORMAL POTENTIALS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26 I.2.6.1
DATA DERIVED FROM STANDARD POTENTIALS . . . . . . . . . . . . . . 26
I.2.6.2 DATA DERIVED FROM FORMAL POTENTIALS . . . . . . . . . . . . . .
. 27 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . 27 I.3 KINETICS OF ELECTROCHEMICAL REACTIONS . . . . . . . . . . . .
. . 29 G. INZELT I.3.1 INTRODUCTION . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . 29 I.3.2 RELATIONSHIP BETWEEN THE CURRENT DENSITY
AND POTENTIAL UNDER STEADY-STATE CONDITIONS . . . . . . . . . . . . . .
. . . . . 30 I.3.2.1 EQUILIBRIUM . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . 32 I.3.2.2 RATE CONTROLLED BY THE CHARGE TRANSFER STEP
. . . . . . . . . . . 32 I.3.2.3 EFFECT OF MASS TRANSPORT ON THE
KINETICS OF ELECTRODE PROCESSES . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . 33 I.3.2.4 REVERSIBILITY, QUASI-REVERSIBILITY,
IRREVERSIBILITY . . . . . . . . . 39 I.3.2.5 EFFECT OF THE DOUBLE-LAYER
STRUCTURE ON THE RATE OF THE CHARGE TRANSFER REACTION . . . . . . . . .
. . . . . . . . . . . . . 42 I.3.3 CURRENT-POTENTIAL TRANSIENTS . . . .
. . . . . . . . . . . . . . . . 44 I.3.3.1 CHARGING THE DOUBLE LAYER . .
. . . . . . . . . . . . . . . . . . . 44 I.3.3.2 FARADAIC CURRENT . . .
. . . . . . . . . . . . . . . . . . . . . . . . 45 REFERENCES . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . . 47 PART II
ELECTROANALYTICAL TECHNIQUES . . . . . . . . . . . . . . . . . . . 49
II.1 CYCLIC VOLTAMMETRY . . . . . . . . . . . . . . . . . . . . . . . .
. 51 F. MARKEN, A. NEUDECK, A. M. BOND II.1.1 INTRODUCTION . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . 51 II.1.1.1 SHAPE OF CYCLIC
VOLTAMMOGRAMS . . . . . . . . . . . . . . . . . . 55 II.1.2 BASIC
PRINCIPLES . . . . . . . . . . . . . . . . . . . . . . . . . . . 57
II.1.3 EFFECTS DUE TO CAPACITY AND RESISTANCE . . . . . . . . . . . . .
. 66 II.1.4 ELECTRODE GEOMETRY, SIZE, AND CONVECTION EFFECTS . . . . . .
. . 68 II.1.5 DETERMINATION OF REDOX STATE AND NUMBER OF TRANSFERRED
ELECTRONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
72 II.1.5.1 CHRONOAMPEREOMETRIC TEST PROCEDURE . . . . . . . . . . . . .
. 72 II.1.5.2 METHOD BASED ON CYCLIC VOLTAMMETRY . . . . . . . . . . . .
. . . 72 II.1.5.3 METHODS BASED ON STEADY-STATE TECHNIQUES . . . . . . .
. . . . . 72 II.1.6 HETEROGENEOUS KINETICS . . . . . . . . . . . . . . .
. . . . . . . . 74 II.1.7 HOMOGENEOUS KINETICS . . . . . . . . . . . . .
. . . . . . . . . . 80 II.1.7.1 THE EC PROCESS . . . . . . . . . . . . .
. . . . . . . . . . . . . . 81 II.1.7.2 THE EC PROCESS . . . . . . . .
. . . . . . . . . . . . . . . . . . . 84 II.1.7.3 THE CE PROCESS . . . .
. . . . . . . . . . . . . . . . . . . . . . . 85 II.1.7.4 THE E * CE *
PROCESS . . . . . . . . . . . . . . . . . . . . . . . . . . . 87
II.1.7.5 THE E * CE * PROCESS . . . . . . . . . . . . . . . . . . . . .
. . . . . . 89 II.1.7.6 SQUARE SCHEMES AND MORE COMPLEX REACTION SCHEMES
. . . . . 90 II.1.8 MULTI-PHASE SYSTEMS . . . . . . . . . . . . . . . .
. . . . . . . . 91 REFERENCES . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . 93 II.2. PULSE VOLTAMMETRY . . . . . . . . . . . . . .
. . . . . . . . . . . 99 Z. STOJEK II.2.1 INTRODUCTION . . . . . . . . .
. . . . . . . . . . . . . . . . . . . . 99 II.2.2 STAIRCASE VOLTAMMETRY
. . . . . . . . . . . . . . . . . . . . . . . 102 II.2.2.1 EQUIVALENCE
OF STAIRCASE AND LINEAR SCAN VOLTAMMETRIES . . . . 102 II.2.3 NORMAL
PULSE VOLTAMMETRY . . . . . . . . . . . . . . . . . . . . . 103 II.2.3.1
INFLUENCE OF ADSORPTION . . . . . . . . . . . . . . . . . . . . . . .
106 II.2.4 REVERSE PULSE VOLTAMMETRY . . . . . . . . . . . . . . . . . .
. . . 106 II.2.5 DIFFERENTIAL PULSE VOLTAMMETRY . . . . . . . . . . . .
. . . . . . 109 REFERENCES . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . 110 XII CONTENTS II.3 SQUARE-WAVE VOLTAMMETRY . . . . . .
. . . . . . . . . . . . . . . 111 M. LOVRI´ C II.3.1 INTRODUCTION . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . 111 II.3.2 SIMPLE
REACTIONS ON STATIONARY PLANAR ELECTRODES . . . . . . . . 113 II.3.3
SIMPLE REACTIONS ON STATIONARY SPHERICAL ELECTRODES AND MICROELECTRODES
. . . . . . . . . . . . . . . . . . . . . . . . . . . 118 II.3.4
REACTIONS OF AMALGAM-FORMING METALS ON THIN MERCURY FILM ELECTRODES . .
. . . . . . . . . . . . . . . . . . . . . . . . . 119 II.3.5 ELECTRODE
REACTIONS COMPLICATED BY ADSORPTION OF THE REACTANT AND PRODUCT . . . .
. . . . . . . . . . . . . . . . . . . . 120 II.3.6 APPLICATIONS OF
SQUARE-WAVE VOLTAMMETRY . . . . . . . . . . . . 126 II.3.7 APPENDIX . .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 128 REFERENCES
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 133 II.4
CHRONOCOULOMETRY . . . . . . . . . . . . . . . . . . . . . . . . . 137
G. INZELT II.4.1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . 137 II.4.2 FUNDAMENTAL THEORETICAL CONSIDERATIONS . . .
. . . . . . . . . . 138 II.4.3 PRACTICAL PROBLEMS . . . . . . . . . . .
. . . . . . . . . . . . . . . 141 II.4.4 DOUBLE-STEP CHRONOCOULOMETRY .
. . . . . . . . . . . . . . . . . 142 II.4.5 EFFECT OF HETEROGENEOUS
KINETICS ON CHRONOCOULOMETRIC RESPONSES . . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . 145 REFERENCES . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . 148 II.5 ELECTROCHEMICAL IMPEDANCE
SPECTROSCOPY . . . . . . . . . . . . 149 U. RETTER, H. LOHSE II.5.1
INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
149 II.5.2 DEFINITIONS, BASIC RELATIONS, THE KRAMERS-KRONIG TRANSFORMS .
. 149 II.5.3 MEASURING TECHNIQUES . . . . . . . . . . . . . . . . . . .
. . . . 151 II.5.4 REPRESENTATION OF THE IMPEDANCE DATA . . . . . . . .
. . . . . . 153 II.5.5 EQUIVALENT CIRCUITS . . . . . . . . . . . . . . .
. . . . . . . . . . 154 II.5.6 THE CONSTANT PHASE ELEMENT . . . . . . .
. . . . . . . . . . . . . 154 II.5.7 COMPLEX NON-LINEAR REGRESSION
LEAST-SQUARES (CNRLS) FOR THE ANALYSIS OF IMPEDANCE DATA . . . . . . . .
. . . . . . . . 155 II.5.8 COMMERCIAL COMPUTER PROGRAMS FOR MODELLING OF
IMPEDANCE DATA . . . . . . . . . . . . . . . . . . . . . . . . . 156
II.5.9 CHARGE TRANSFER AT THE ELECTRODE * THE RANDLES MODEL . . . . . .
156 II.5.10 SEMIINFINITE HEMISPHERICAL DIFFUSION FOR FARADAIC PROCESSES
. . 159 II.5.11 DIFFUSION OF PARTICLES IN FINITE-LENGTH REGIONS * THE
FINITE WARBURG IMPEDANCE . . . . . . . . . . . . . . . . . . . 160
II.5.12 HOMOGENEOUS OR HETEROGENEOUS CHEMICAL REACTION AS
RATE-DETERMINING STEP . . . . . . . . . . . . . . . . . . . . . . . 162
II.5.13 POROUS ELECTRODES . . . . . . . . . . . . . . . . . . . . . . .
. . . 162 II.5.14 SEMICONDUCTOR ELECTRODES . . . . . . . . . . . . . . .
. . . . . . 162 II.5.15 KINETICS OF NON-FARADAIC PROCESSES . . . . . . .
. . . . . . . . . 163 II.5.16 REFERENCES TO RELEVANT FIELDS OF
APPLICATIONS OF EIS . . . . . . . 165 REFERENCES . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . . 165 CONTENTS XIII II.6 UV/VIS/NIR
SPECTROELECTROCHEMISTRY A. NEUDECK, F. MARKEN, R. G. COMPTON . . . . . .
. . . . . . . . . 167 II.6.1 INTRODUCTION * WHY COUPLE TECHNIQUES? . . .
. . . . . . . . . . 167 II.6.2 FLOWING VERSUS STAGNANT SYSTEMS *
ACHIEVING SPATIAL, TEMPORAL, AND MECHANISTIC RESOLUTION . . . . . . . .
. . . . . . 169 II.6.2.1 STEADY-STATE OR TRANSIENT TECHNIQUES . . . . .
. . . . . . . . . . 169 II.6.2.2 CELL GEOMETRY AND EXPERIMENTAL DESIGN
CONSIDERATIONS . . . . 172 II.6.2.3 TIME-SCALE CONSIDERATIONS . . . . .
. . . . . . . . . . . . . . . . 173 II.6.2.4 SPATIAL AND MECHANISTIC
RESOLUTION . . . . . . . . . . . . . . . . 174 II.6.3 UV/VIS/NIR
SPECTROELECTROCHEMICAL TECHNIQUES . . . . . . . . . 175 II.6.3.1
SPECTROELECTROCHEMISTRY IN TRANSMISSION MODE . . . . . . . . . 175
II.6.3.2 SPECTROELECTROCHEMISTRY IN REFLECTION MODE . . . . . . . . . .
. 186 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . 187 II.7 STRIPPING VOLTAMMETRY . . . . . . . . . . . . . . . . . . .
. . . . 191 M. LOVRI´ C II.7.1 INTRODUCTION . . . . . . . . . . . . . .
. . . . . . . . . . . . . . . 191 II.7.2 OVERVIEW OF PRECONCENTRATION
METHODS . . . . . . . . . . . . . . 192 II.7.2.1 METAL DEPOSITION ON
SOLID ELECTRODES . . . . . . . . . . . . . . . 193 II.7.2.2 METAL
DEPOSITION ON MERCURY ELECTRODES . . . . . . . . . . . . . 196 II.7.2.3
DEPOSITION OF SPARINGLY SOLUBLE SALTS ON ELECTRODES . . . . . . . 199
II.7.2.4 ADSORPTIVE PRECONCENTRATION . . . . . . . . . . . . . . . . . .
. . 200 II.7.2.5 PRECONCENTRATION BY SURFACE COMPLEXATION . . . . . . .
. . . . . 204 II.7.3 STRIPPING VOLTAMMETRY AT TWO IMMISCIBLE LIQUID
ELECTROLYTE SOLUTIONS . . . . . . . . . . . . . . . . . . . . . . . .
205 II.7.4 GENERAL FEATURES OF STRIPPING VOLTAMMETRY . . . . . . . . . .
. . 205 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . 208 II.8 ELECTROCHEMICAL STUDIES OF SOLID COMPOUNDS AND MATERIALS
. . 211 D. A. FIEDLER, F. SCHOLZ II.8.1 INTRODUCTION . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . 211 II.8.2 EXPERIMENTAL . . . . .
. . . . . . . . . . . . . . . . . . . . . . . . 211 II.8.2.1 ELECTRODES
AND ELECTRODE PREPARATION . . . . . . . . . . . . . . . 211 II.8.2.2
SAMPLE PREPARATION . . . . . . . . . . . . . . . . . . . . . . . . . 214
II.8.2.3 EXPERIMENTAL SETUP . . . . . . . . . . . . . . . . . . . . . .
. . . 215 II.8.2.4 STRATEGY . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . 215 II.8.2.5 WHAT COMPOUNDS AND MATERIALS CAN BE
STUDIED? . . . . . . . . 216 II.8.3 ELECTROCHEMICAL METHODS . . . . . .
. . . . . . . . . . . . . . . . 216 II.8.3.1 PHASE IDENTIFICATIONS AND
QUANTITATIVE ANALYSIS OF SOLIDS . . . . 216 II.8.3.2 STUDIES OF THE
ELECTROCHEMICAL BEHAVIOR OF SOLID MATERIALS . . . 218 II.8.4 COMBINED
METHODS . . . . . . . . . . . . . . . . . . . . . . . . . 220 II.8.4.1
EX SITU METHODS . . . . . . . . . . . . . . . . . . . . . . . . . . .
220 II.8.4.2 IN SITU METHODS . . . . . . . . . . . . . . . . . . . . . .
. . . . . 221 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . .
. . . . . . 221 XIV CONTENTS II.9 POTENTIOMETRY . . . . . . . . . . . .
. . . . . . . . . . . . . . . . 223 H. KAHLERT II.9.1 INTRODUCTION . . .
. . . . . . . . . . . . . . . . . . . . . . . . . . 223 II.9.2 CELL
VOLTAGE . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 223
II.9.3 INDICATOR ELECTRODES AND THEIR POTENTIALS . . . . . . . . . . . .
. 224 II.9.3.1 REDOX ELECTRODES . . . . . . . . . . . . . . . . . . . .
. . . . . . 224 II.9.3.2 METAL ELECTRODES OR ELECTRODES OF THE FIRST
KIND . . . . . . . . . 227 II.9.3.3 ELECTRODES OF THE SECOND KIND . . .
. . . . . . . . . . . . . . . . 229 II.9.3.4 MEMBRANE ELECTRODES . . . .
. . . . . . . . . . . . . . . . . . . . 229 II.9.4 INTERFERENCES AND
DETECTION LIMITS IN POTENTIOMETRIC MEASUREMENTS . . . . . . . . . . . .
. . . . . . . . . . . . . . . . 236 REFERENCES . . . . . . . . . . . . .
. . . . . . . . . . . . . . . . . 240 PART III ELECTRODES AND
ELECTROLYTES . . . . . . . . . . . . . . . . . . . . 243 III.1 WORKING
ELECTRODES . . . . . . . . . . . . . . . . . . . . . . . . . 245 S *.
KOMORSKY-LOVRI´ C III.1.1 INTRODUCTION . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . 245 III.1.2 ELECTRODE MATERIALS . . . . . . . .
. . . . . . . . . . . . . . . . . 247 III.1.3 ELECTRODE GEOMETRY . . . .
. . . . . . . . . . . . . . . . . . . . . 251 III.1.4 HYDRODYNAMIC
CONDITIONS . . . . . . . . . . . . . . . . . . . . . 253 III.1.5
CHEMICALLY MODIFIED ELECTRODES . . . . . . . . . . . . . . . . . . 257
REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
259 III.2 REFERENCE ELECTRODES . . . . . . . . . . . . . . . . . . . . .
. . . 261 H. KAHLERT III.2.1 INTRODUCTION . . . . . . . . . . . . . . .
. . . . . . . . . . . . . . 261 III.2.2 THE STANDARD HYDROGEN ELECTRODE
. . . . . . . . . . . . . . . . . 263 III.2.3 ELECTRODES OF THE SECOND
KIND AS REFERENCE ELECTRODES . . . . . 264 III.2.3.1 MERCURY-BASED
REFERENCE ELECTRODES . . . . . . . . . . . . . . . 264 III.2.3.2 THE
SILVER/SILVER CHLORIDE ELECTRODE . . . . . . . . . . . . . . . . 268
III.2.4 PH-BASED REFERENCE ELECTRODES . . . . . . . . . . . . . . . . .
. 269 III.2.5 INNER POTENTIAL STANDARDS . . . . . . . . . . . . . . . .
. . . . . . 270 III.2.6. SOLID-STATE REFERENCE ELECTRODES . . . . . . .
. . . . . . . . . . . 271 III.2.7 PSEUDO REFERENCE ELECTRODES . . . . .
. . . . . . . . . . . . . . . 271 III.2.8 PRACTICAL PROBLEMS . . . . . .
. . . . . . . . . . . . . . . . . . . . 272 III.2.8.1 THE ELECTROLYTE OF
REFERENCE ELECTRODES . . . . . . . . . . . . . . 272 III.2.8.2 THE
DIAPHRAGM . . . . . . . . . . . . . . . . . . . . . . . . . . . 275
III.2.8.3 REFILLING OF THE REFERENCE SOLUTION . . . . . . . . . . . . .
. . . . 276 III.2.8.4 MAINTENANCE OF REFERENCE ELECTRODES . . . . . . .
. . . . . . . . 276 REFERENCES . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . 277 CONTENTS XV III.3 ELECTROLYTES . . . . . . . . . .
. . . . . . . . . . . . . . . . . . . 279 S *. KOMORSKY-LOVRI´ C III.3.1
INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
279 III.3.2 IONIC TRANSPORT . . . . . . . . . . . . . . . . . . . . . .
. . . . . 280 III.3.3 IONIC SOLUTIONS . . . . . . . . . . . . . . . . .
. . . . . . . . . . . 287 III.3.3.1 AQUEOUS ELECTROLYTE SOLUTIONS . . .
. . . . . . . . . . . . . . . . 293 III.3.3.2 NONAQUEOUS ELECTROLYTE
SOLUTIONS . . . . . . . . . . . . . . . . . 296 REFERENCES . . . . . . .
. . . . . . . . . . . . . . . . . . . . . . . 299 III.4 EXPERIMENTAL
SETUP . . . . . . . . . . . . . . . . . . . . . . . . . 301 Z. STOJEK
III.4.1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . 301 III.4.2 THE WORKING ELECTRODE . . . . . . . . . . . . . . . .
. . . . . . . 301 III.4.3 THE REFERENCE ELECTRODE . . . . . . . . . . .
. . . . . . . . . . . 302 III.4.4 THE COUNTER ELECTRODE . . . . . . . .
. . . . . . . . . . . . . . . 303 III.4.5 INSTRUMENTAL PARAMETERS AND
WIRING . . . . . . . . . . . . . . . 303 III.4.6 NONAQUEOUS MEDIA . . .
. . . . . . . . . . . . . . . . . . . . . . 304 III.4.7 ELIMINATION OF
ELECTRICAL NOISE . . . . . . . . . . . . . . . . . . . 304 REFERENCES .
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 305 PART IV
PUBLICATIONS IN ELECTROCHEMISTRY . . . . . . . . . . . . . . . . . 307
IV.1 SEMINAL PUBLICATIONS IN ELECTROCHEMISTRY AND ELECTROANALYSIS . . .
. . . . . . . . . . . . . . . . . . . . . . 309 F. SCHOLZ, G. INZELT, Z.
STOJEK IV.2 TEXTBOOKS ON FUNDAMENTAL ELECTROCHEMISTRY AND
ELECTROANALYTICAL TECHNIQUES . . . . . . . . . . . . . . . . . . . 315
F. SCHOLZ IV.2.1 GENERAL TEXTBOOKS . . . . . . . . . . . . . . . . . . .
. . . . . . . 315 IV.2.2 MONOGRAPHS ON SPECIAL TECHNIQUES AND SUBJECTS .
. . . . . . . 315 IV.2.3 SERIES EDITIONS OF ADVANCES IN ELECTROCHEMISTRY
. . . . . . . . . 316 IV.2.4 REFERENCE BOOKS FOR ELECTROCHEMICAL DATA .
. . . . . . . . . . . 316 IV.2.5 JOURNALS ON ELECTROCHEMISTRY . . . . .
. . . . . . . . . . . . . . 316 IV.2.6 JOURNALS THAT REGULARLY PUBLISH
PAPERS ON ELECTROCHEMISTRY AND/OR ELECTROANALYSIS . . . . . . . . . . .
. . 317 IV.2.7 WWW SOURCES . . . . . . . . . . . . . . . . . . . . . . .
. . . . . 317 SUBJECT INDEX . . . . . . . . . . . . . . . . . . . . . .
. . . . . . . . . . . . 319 XVI CONTENTS |
any_adam_object | 1 |
author_GND | (DE-588)143718231 (DE-588)105306201X |
building | Verbundindex |
bvnumber | BV014072179 |
callnumber-first | Q - Science |
callnumber-label | QD115 |
callnumber-raw | QD115 |
callnumber-search | QD115 |
callnumber-sort | QD 3115 |
callnumber-subject | QD - Chemistry |
classification_rvk | VG 8000 |
classification_tum | CHE 224f |
ctrlnum | (OCoLC)248330062 (DE-599)BVBBV014072179 |
dewey-full | 543.0871 |
dewey-hundreds | 500 - Natural sciences and mathematics |
dewey-ones | 543 - Analytical chemistry |
dewey-raw | 543.0871 |
dewey-search | 543.0871 |
dewey-sort | 3543.0871 |
dewey-tens | 540 - Chemistry and allied sciences |
discipline | Chemie / Pharmazie Chemie |
format | Book |
fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>00000nam a22000008c 4500</leader><controlfield tag="001">BV014072179</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20181018</controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">011218s2002 gw ad|| |||| 00||| eng d</controlfield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">963084844</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">3540422293</subfield><subfield code="9">3-540-42229-3</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)248330062</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV014072179</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="044" ind1=" " ind2=" "><subfield code="a">gw</subfield><subfield code="c">DE</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-703</subfield><subfield code="a">DE-29T</subfield><subfield code="a">DE-19</subfield><subfield code="a">DE-355</subfield><subfield code="a">DE-M49</subfield><subfield code="a">DE-526</subfield><subfield code="a">DE-634</subfield><subfield code="a">DE-83</subfield><subfield code="a">DE-11</subfield></datafield><datafield tag="050" ind1=" " ind2="0"><subfield code="a">QD115</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">543.0871</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VG 8000</subfield><subfield code="0">(DE-625)147212:253</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">CHE 224f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Electroanalytical methods</subfield><subfield code="b">guide to experiments and applications ; with 31 tables</subfield><subfield code="c">F. Scholz (ed.). With contributions by A. M. Bond ...</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Berlin [u.a.]</subfield><subfield code="b">Springer</subfield><subfield code="c">2002</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XXII, 331 S.</subfield><subfield code="b">Ill., graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Elektroanalyse - Aufsatzsammlung</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Electrochemical analysis</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Elektroanalyse</subfield><subfield code="0">(DE-588)4014237-1</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)4143413-4</subfield><subfield code="a">Aufsatzsammlung</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Elektroanalyse</subfield><subfield code="0">(DE-588)4014237-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Scholz, Fritz</subfield><subfield code="d">1955-</subfield><subfield code="e">Sonstige</subfield><subfield code="0">(DE-588)143718231</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Bond, Alan M.</subfield><subfield code="d">1946-</subfield><subfield code="e">Sonstige</subfield><subfield code="0">(DE-588)105306201X</subfield><subfield code="4">oth</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">SWB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009638370&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-009638370</subfield></datafield></record></collection> |
genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
genre_facet | Aufsatzsammlung |
id | DE-604.BV014072179 |
illustrated | Illustrated |
indexdate | 2024-08-13T00:10:14Z |
institution | BVB |
isbn | 3540422293 |
language | English |
oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009638370 |
oclc_num | 248330062 |
open_access_boolean | |
owner | DE-703 DE-29T DE-19 DE-BY-UBM DE-355 DE-BY-UBR DE-M49 DE-BY-TUM DE-526 DE-634 DE-83 DE-11 |
owner_facet | DE-703 DE-29T DE-19 DE-BY-UBM DE-355 DE-BY-UBR DE-M49 DE-BY-TUM DE-526 DE-634 DE-83 DE-11 |
physical | XXII, 331 S. Ill., graph. Darst. |
publishDate | 2002 |
publishDateSearch | 2002 |
publishDateSort | 2002 |
publisher | Springer |
record_format | marc |
spelling | Electroanalytical methods guide to experiments and applications ; with 31 tables F. Scholz (ed.). With contributions by A. M. Bond ... Berlin [u.a.] Springer 2002 XXII, 331 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Elektroanalyse - Aufsatzsammlung Electrochemical analysis Elektroanalyse (DE-588)4014237-1 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Elektroanalyse (DE-588)4014237-1 s DE-604 Scholz, Fritz 1955- Sonstige (DE-588)143718231 oth Bond, Alan M. 1946- Sonstige (DE-588)105306201X oth SWB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009638370&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
spellingShingle | Electroanalytical methods guide to experiments and applications ; with 31 tables Elektroanalyse - Aufsatzsammlung Electrochemical analysis Elektroanalyse (DE-588)4014237-1 gnd |
subject_GND | (DE-588)4014237-1 (DE-588)4143413-4 |
title | Electroanalytical methods guide to experiments and applications ; with 31 tables |
title_auth | Electroanalytical methods guide to experiments and applications ; with 31 tables |
title_exact_search | Electroanalytical methods guide to experiments and applications ; with 31 tables |
title_full | Electroanalytical methods guide to experiments and applications ; with 31 tables F. Scholz (ed.). With contributions by A. M. Bond ... |
title_fullStr | Electroanalytical methods guide to experiments and applications ; with 31 tables F. Scholz (ed.). With contributions by A. M. Bond ... |
title_full_unstemmed | Electroanalytical methods guide to experiments and applications ; with 31 tables F. Scholz (ed.). With contributions by A. M. Bond ... |
title_short | Electroanalytical methods |
title_sort | electroanalytical methods guide to experiments and applications with 31 tables |
title_sub | guide to experiments and applications ; with 31 tables |
topic | Elektroanalyse - Aufsatzsammlung Electrochemical analysis Elektroanalyse (DE-588)4014237-1 gnd |
topic_facet | Elektroanalyse - Aufsatzsammlung Electrochemical analysis Elektroanalyse Aufsatzsammlung |
url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009638370&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
work_keys_str_mv | AT scholzfritz electroanalyticalmethodsguidetoexperimentsandapplicationswith31tables AT bondalanm electroanalyticalmethodsguidetoexperimentsandapplicationswith31tables |