Stirring: theory and practice
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English German |
| Veröffentlicht: |
Weinheim u.a.
Wiley-VCH
2001
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIX, 362 S. Ill., graph. Darst. |
| ISBN: | 3527299963 |
Internformat
MARC
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| 100 | 1 | |a Zlokarnik, Marko |d 1931- |e Verfasser |0 (DE-588)106004298 |4 aut | |
| 240 | 1 | 0 | |a Rührtechnik |
| 245 | 1 | 0 | |a Stirring |b theory and practice |c Marko Zlokarnik |
| 264 | 1 | |a Weinheim u.a. |b Wiley-VCH |c 2001 | |
| 300 | |a XIX, 362 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Mixing | |
| 650 | 4 | |a Mixing machinery | |
| 650 | 0 | 7 | |a Dispergierung |0 (DE-588)4150199-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Suspension |0 (DE-588)4058671-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Mischen |0 (DE-588)4120742-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Rühren |0 (DE-588)4130232-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Homogenisieren |0 (DE-588)4138007-1 |2 gnd |9 rswk-swf |
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| 856 | 4 | 2 | |m Digitalisierung UB Bayreuth |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009517575&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-009517575 | ||
Datensatz im Suchindex
| _version_ | 1804128752838377472 |
|---|---|
| adam_text | Contents
Preface
xii
Symbols xv
1
Stirring, general
1
1.1
Stirring operations
1
1.2
Mixing equipment
2
1.2.1
Mixing tanks and their fittings
2
1.2.2
Stirrer types and their operating characteristics
6
1.2.3
Nozzles and spargers
11
1.2.4
Sealing of stirrer shafts
12
1.3
Mechanical stress
14
1.3.1
Stress on baffles
14
1.3.2
Stress on stirrer heads
14
1.3.3
Tank vibrations
ÍS
1.3.4
Wear of stirrer heads
15
1.3.5
Shear stress on the particulate material beinig mixed
16
1.4
Flow and Turbulence
20
1.4.1
Introduction
20
1.4.2
Statistical theory of turbulence
21
1.4.2.1
Description of turbulent flow
23
1.4.2.2
Energy spectra
25
1.4.3
Experimental determination of state of flow flow and its mathematical
modeling
27
1.4.3.1
Homogeneous material systems
27
1.4.3.2
Heterogeneous G/L material systems
34
1.4.3.3
Heterogeneous I/I material systems
34
1.4.4
Pumping capacity of stirrers
34
1.4.5
Surface motion
36
1.4.5.1
Vortex formation. Definition of geometric parameters
36
1.4.5.2
Gas entrainment via vortex
39
1.4.6
Micro-mixing and reactions
40
1.4.6.1
Introduction
40
1.4.6.2
Theoretical prediction of micro-mixing
43
1.4.6.3
Chemical reactions for determining micro-mixing
45
vi I
Contents
1.4.6.4
Experimental determination of micro-mixing
48
1.5
Short introduction to rheology
50
1.5.1
Newtonian liquids
50
1.5.2
Non-Newtonian liquids
51
1.5.3
Dimensionless representation of material functions
57
1.6
Short introduction to dimensional analysis and scale-up
60
1.6.1
Introduction
60
1.6.2
Dimensional analysis
62
1.6.2.1
Fundamentals
62
1.6.2.2
Dimensions and physical quantities
62
1.6.2.3
Primary and secondary quantities; dimensional constants
62
1.6.2.4
Dimensional systems
63
1.6.2.5
Dimensional homogeneity of a physical relationship
63
1.6.2.6
The pi theorem
66
1.6.3
Construction of pi sets using matrix transformation
66
1.6.3.1
Drawing-up of a relevance list for a problem
66
1.6.3.2
Determination of the characteristic geometric parameter
67
1.6.3.3
Constructing and solving of the dimensional matrix
68
1.6.3.4
Determination of the process characteristics
69
1.6.4
Fundamentals of the model theory and scale-up
70
1.6.4.1
Model theory
70
1.6.4.2
Model experiments and scale-up
71
1.6.5
Remarks regarding the relevance list and experimental technique
72
1.6.5.1
Taking into consideration of the acceleration due to gravity
g
72
1.6.5.2
Introduction of intermediate quantities
72
1.6.5.3
Dealing with material systems with unknown physical properties
72
1.6.5.4
Experimental methods for scale-up
73
1.6.6
Conclusions
73
1.6.6.1
Advantages of use of dimensional analysis
73
1.6.6.2
Range of applicability of dimensional analysis
74
2
Stirrer power
76
2.1
Stirrer power in a homogeneous liquid
76
2.1.1
Newtonian liquids
76
2.1.2
Non-Newtonian liquids
82
2.2
Stirrer power in G/L systems
83
2.2.1
Newtonian liquids
83
2.2.2
Non-Newtonian liquids
90
2.3
Flooding point
94
3
Homogenization
97
3.1
Definition of macro- and micro-mixing
97
3.2
Definition of degree of mixing
98
3.3
Determination of the degree of mixing and the mixing time
100
3.3.1
Physical methods
101
Contents
vii
3.3.2 Chemical
measurement methods
102
3.3.3
Degree of mixing and molar excess
102
3.4
Homogenization characteristics
104
3.4.1
Material systems without density and viscosity differences
104
3.4.2
Material systems with density and viscosity differences
ПО
3.4.3
Non-Newtonian mixtures
112
3.5
Optimization to minimum mixing work
116
3.6
Scale-up of the homogenization process
118
3.7
Homogenization in storage tanks
122
3.7.1
Homogenization with propellers
122
3.7.2
Homogenization with liquid jets
123
3.7.3
Homogenization through rising up gas bubbles
123
4
Gas-liquid contacting
126
4.1
Introduction
126
4.2
Physical fundamentals of mass transfer
126
4.2.1
Determining the driving force
126
4.2.2
Temperature dependence of k _a
129
4.2.3
Saturation concentration cs of the gas in the liquid
130
4.2.4
Definition of the characteristic concentration difference Ac
130
4.2.5
Consideration of the absorption process from a physical and industrial
viewpoint
132
4.3
Determination of k .a
132
4.3.1
Unsteady-state measurement methods
132
4.3.1.1
Measurement with oxygen electrodes
133
4.3.1.2
Pressure gauge method
133
4.3.1.3
Dynamic response methods
134
4.3.2
Steady-state methods
134
4.3.2.1 Sulfite
methods
134
4.3.2.2
Hydrazine methods
136
4.3.2.3
Sodium
sulfite
feed technique
137
4.3.2.4
Hydrogen peroxide method
137
4.4
Mass transfer characteristics for the G/L system
138
4.4.1
Establishing mass transfer relationships
138
4.4.2
Mass transfer relationship: experimental data
139
4.4.3 Sorption
characteristics in the coalescing system water/air
141
4.4.4 Sorption
characteristics in coalescence-inhibited systems
143
4.4.5 Sorption
characteristics in rheological material systems
145
4.4.6 Sorption
characteristic in biological material systems
149
4.5
Interfacial
area per unit volume
α
151
4.5.1
Definition of
о
151
4.5.2
Determination of a
152
4.5.2.1
Physical methods
152
4.5.2.2
Chemical methods
152
4.5.3
Process relationships for a
152
viii
I Contents
4.6
Gas fraction (gas hold-up) in gassed liquids
153
4.6.1
Definition of
ε
354
4.6.2
Determination of
ε
154
4.6.3
Process relationships for
ε
155
4.7
Gas bubble diameter
db
an<ł
its effect upon ki
156
4.8
Gas-absorption in oil/water dispersions
361
4.9
Chemisorption
162
4.10
Bubble coalescence
365
4.11
Foam breaking
375
4.11.1
Methods and devices for foam breaking
376
4.11.2
Foam centrifuge and foam turbine
177
4.11.3
Minimum rotor tip speed
379
4.11.4
Process characteristic of the foam centrifuge and its scale-up
380
4.12
Special gas-liquid contacting techniques
183
4.12.1
Hollow stirrers
183
4.12.1.1
Application areas
383
4.12.1.2
Suction, power and efficiency characteristics
385
4.12.1.3
Comparison of hollow stirrer and turbine stirrer
387
4.12.1.4 Sorption
characteristics
190
4.12.2
Surface aerators
390
4.12.2.1
Centrifugal surface aerators
390
4.12.2.2
Power characteristic
393
4.12.2.3 Sorption
characteristic
392
4.12.2.4
Plunging water jet aerators
194
4.12.2.5
Horizontal blade-wheel reactor
197
4.12.3
Gas spargers
399
4.12.3.1
Sintered glass or ceramics plates, perforated metal plates and static
mixers
200
4.12.3.2
Injectors (G/I nozzles)
201
4.12.3.3
Funnel shaped nozzle as ejectors
205
5
Suspension of Solids in Liquids
(S/Ĺ
System)
206
5.1
Classification of the suspension condition
206
5.1.1
Complete suspension
206
5.1.2
Homogeneous suspension
207
5.2
Distribution of solids upon suspension
208
5.3
Suspension characteristics
233
5.3.1
Relevance lists and pi spaces
233
5.3.1.1
Specification according to the nature of the target quantity nx
233
5.3.1.2
Specification according to particle property dp and/or wss
231
5.3.2
Suspension characteristics with dp as the characteristic particle
dimension
212
5.3.2.1
Relevance list and pi space
212
5.3.2.2
The process relationship
213
5.3.2.3
Power requirements upon suspension
236
Contents
І
ix
5.3.2.4 Power
requirement for the critical stirrer speed nx
217
5.3.2.5
Scaling up in suspension according to the criterion nx
217
5.3.3
Suspension characteristic with wss as the characteristic particle
property
217
5.3.3.1
Determination of the particle sinking velocity in the swarm wss
217
5.3.3.2
The relevance list and the pi space
220
5.3.3.3
The process relationship
220
5.3.3.4
Final discussion from the viewpoint of the dimensional analysis
229
5.3.3.5
Establishing of scale-up criteria
230
5.3.4
Suspension characteristic with the energy dissipation number E*
231
5.3.5
Effect of geometric and device-related factors on the suspension
characteristic
233
5.4
Homogenization of the liquid in the S/L system
235
5.5
Mass transfer in the S/L system
236
5.5.1
Physical basis of mass transfer in the S/L system
236
5.5.2
Process characteristics of mass transfer in the S/L system
237
5.6
Suspension in the S/L/G-system: hydrodynamics and power
requirement
241
5.7
Mass transfer in the S/L/G system
241
6
Dispersion in L/L Systems
244
6.1
Lowest stirrer speed for dispersion
244
6.2
Dispersion characteristics
246
6.2.1
The target quantity
¿32 246
6.2.2
Coalescence in the L/L system
247
6.2.3
Determination method for
¿¿32 247
6.2.4
Dimensional-analytical description
248
6.2.5
The process characteristics
249
6.2.6
Effect of coalescence and of
φν
on
àyi
250
6.2.7
Effect of viscosity
251
6.2.8
Effect of stirring duration
252
6.3
Droplet size distribution
253
6.3.1
Fundamentals
253
6.3.2
Effect of stirrer speed
254
6.3.3
Effect of stirrer type and material system
255
6.3.4
Effect of the mixing time
262
6.4
Stirrer power for dispersion
263
6.5
Scaling up of dispersion processes
263
6.6
Mass and heat transfer upon dispersion
264
6.7
Mathematical modeling of the dispersion process
267
7
Intensification of heat transfer by stirring
272
7.1
Physical fundamentals of heat transfer
272
7.1.1
Determination of
a¡
273
7.1.2
Dimensional-analytical description
273
χ Ι
Contents
7.2
Heat transfer between a homogeneous liquid and a heat transfer
surface
275
7.2.1
Flow range Re
=
102-106
275
7.2.2
Flow range Re
<
102
278
7.3
Generalized representation of the heat transfer characteristic by
including the stirrer power per unit volume
282
7.4
Effect of the Vis-term
284
7.4.1
Taking non-Newtonian viscosity into consideration
286
7.5
Optimization of stirrers for a maximum removal of reaction heat
288
7.6
Heat transfer for G/L material systems
291
7.6.1
Dimensionally analytical description
291
7.7
Heat transfer in S/L systems
293
7.7.1
Direct heat exchange ice cubes/water
293
7.7.2
Indirect heat exchange for Ap
> 0 294
7.7.3
Indirect heat exchange at Ap
ä
0 295
7.8
Heat transfer in L/L material systems
298
7.8.1
Direct heat exchange
298
7.8.2
Indirect heat exchange
298
7.9
Heat transfer in
G/L/ S
material systems
299
8
Mixing and stirring in pipes
300
8.1
Mixing and homogenization
300
8.1.1
Straight, smooth or rough pipe without fittings
300
8.1.2
Pipe with a jet mixer or with a Tee piece
302
8.1.2.1
Jet mixers
302
8.1.2.2
Tee pieces
304
8.1.3
Flow deflecting fittings ( motionless or static mixers )
305
Kenics mixer
307
Sulzer mixers SMV and SMX
[533] 308
Ross-ISG mixer
309
8.2
G/L-mass transfer
309
8.2.1
Mass transfer in pipe flow
309
8.2.2
Mass transfer in pipe with static mixer
310
8.3
Heat transfer
311
8.3.1
Heat transfer in pipe flow
311
8.3.2
Heat transfer in pipe with static mixer
311
8.4
Dispersion in L/L system
314
8.4.1
Dispersion in pipe flow
314
8.4.2
Dispersion in pipe with static mixer
335
8.5
Micro-mixing and chemical reaction
316
8.5.1
Pipe reactor
317
8.5.2
Pipe reactor with a jet mixer
ЗІ9
8.5.3
Pipe reactor with static mixer
320
8.6
Modeling of mixing processes in pipes
322
8.6.1
Pipe flow
322
Contents
І
xi
8.6.2
Pipe with Tee mixer
323
8.6.3
Pipe with static mixer
323
8.7
Stirring in pipes and mixing columns
324
Literature
328
Subject Index
360
|
| any_adam_object | 1 |
| author | Zlokarnik, Marko 1931- |
| author_GND | (DE-588)106004298 |
| author_facet | Zlokarnik, Marko 1931- |
| author_role | aut |
| author_sort | Zlokarnik, Marko 1931- |
| author_variant | m z mz |
| building | Verbundindex |
| bvnumber | BV013910029 |
| callnumber-first | T - Technology |
| callnumber-label | TA357 |
| callnumber-raw | TA357.5.M59 TP156.M5 |
| callnumber-search | TA357.5.M59 TP156.M5 |
| callnumber-sort | TA 3357.5 M59 |
| callnumber-subject | TA - General and Civil Engineering |
| classification_rvk | VN 7160 VN 7161 |
| classification_tum | CIT 170f |
| ctrlnum | (OCoLC)46693210 (DE-599)BVBBV013910029 |
| dewey-full | 660.284292 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.284292 |
| dewey-search | 660.284292 |
| dewey-sort | 3660.284292 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie Chemie-Ingenieurwesen |
| format | Book |
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| id | DE-604.BV013910029 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:54:15Z |
| institution | BVB |
| isbn | 3527299963 |
| language | English German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009517575 |
| oclc_num | 46693210 |
| open_access_boolean | |
| owner | DE-M49 DE-BY-TUM DE-1046 DE-526 DE-703 |
| owner_facet | DE-M49 DE-BY-TUM DE-1046 DE-526 DE-703 |
| physical | XIX, 362 S. Ill., graph. Darst. |
| publishDate | 2001 |
| publishDateSearch | 2001 |
| publishDateSort | 2001 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Zlokarnik, Marko 1931- Verfasser (DE-588)106004298 aut Rührtechnik Stirring theory and practice Marko Zlokarnik Weinheim u.a. Wiley-VCH 2001 XIX, 362 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Mixing Mixing machinery Dispergierung (DE-588)4150199-8 gnd rswk-swf Suspension (DE-588)4058671-6 gnd rswk-swf Mischen (DE-588)4120742-7 gnd rswk-swf Rühren (DE-588)4130232-1 gnd rswk-swf Homogenisieren (DE-588)4138007-1 gnd rswk-swf Mischen (DE-588)4120742-7 s DE-604 Homogenisieren (DE-588)4138007-1 s Dispergierung (DE-588)4150199-8 s Suspension (DE-588)4058671-6 s Rühren (DE-588)4130232-1 s Digitalisierung UB Bayreuth application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009517575&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zlokarnik, Marko 1931- Stirring theory and practice Mixing Mixing machinery Dispergierung (DE-588)4150199-8 gnd Suspension (DE-588)4058671-6 gnd Mischen (DE-588)4120742-7 gnd Rühren (DE-588)4130232-1 gnd Homogenisieren (DE-588)4138007-1 gnd |
| subject_GND | (DE-588)4150199-8 (DE-588)4058671-6 (DE-588)4120742-7 (DE-588)4130232-1 (DE-588)4138007-1 |
| title | Stirring theory and practice |
| title_alt | Rührtechnik |
| title_auth | Stirring theory and practice |
| title_exact_search | Stirring theory and practice |
| title_full | Stirring theory and practice Marko Zlokarnik |
| title_fullStr | Stirring theory and practice Marko Zlokarnik |
| title_full_unstemmed | Stirring theory and practice Marko Zlokarnik |
| title_short | Stirring |
| title_sort | stirring theory and practice |
| title_sub | theory and practice |
| topic | Mixing Mixing machinery Dispergierung (DE-588)4150199-8 gnd Suspension (DE-588)4058671-6 gnd Mischen (DE-588)4120742-7 gnd Rühren (DE-588)4130232-1 gnd Homogenisieren (DE-588)4138007-1 gnd |
| topic_facet | Mixing Mixing machinery Dispergierung Suspension Mischen Rühren Homogenisieren |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009517575&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT zlokarnikmarko ruhrtechnik AT zlokarnikmarko stirringtheoryandpractice |