Purification of laboratory chemicals:
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Oxford u.a.
Pergamon Pr.
1966
|
| Ausgabe: | 1. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Später u.d.T.: Armarego, Wilfred L. F.: Purification of laboratory chemicals |
| Beschreibung: | VIII, 362 S. |
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Datensatz im Suchindex
| _version_ | 1804128655102705664 |
|---|---|
| adam_text | PURIFICATION OF
LABORATORY CHEMICALS
BY
D D PERRIN, WLF ARMAREGO
A N D
DAWN R PERRIN
Department of Medical Chemistry,
Australian National University,
and
Division of Plant Industry,
Commonwealth Scientific and Industrial Research Organization, Canberra
PERGAMONPRESS
OXFORD • LONDON • EDINBURGH • NEWYORK
TORONTO • PARIS • BRAUNSCHWEIG
CONTENTS
PREFACE vii
CHAPTER 1 COMMON LABORATORY TECHNIQUES USED IN PI RIFICATION 1
General Remarks 1
Distillation 3
Technique 4
Distillation under Atmospheric Pressure 5
The Distilling Flask 5
Types of Columns and Packing 6
Condensers 8
Vacuum Distillation 9
Steam Distillation 10
Sublimation 11
Azeotropic Distillation 11
Recrystallization 12
Technique 12
Choice of Solvents 13
Mixed Solvents 14
Crystallization from the Melt 15
Drying 15
Removal of Solvents 15
Removal of Wpter 16
Intensity and Capacity of Common Desiccants 17
Chromatography and Ion-exchange 19
Ion-exchange Resins 21
Graded Adsorbents and Solvents 22
Preparation and Standardization of Alumina 23
Preparation of Other Adsorbents 24
Solvent Extraction and Distribution 25
Purification via Derivatives 26
Removal of Traces of Metals from Reagents 32
Tables 35
Bibliography 42
CHAPTER 2 RECENT AND MORE SPECIALIZED METHODS OF I LTRIFICATION 44
Metal Hydrides 44
Molecular Sieves 45
Ion-exchange Celluloses 47
Vapour-phase Chromatography 47
Zone Refining 50
Spinning-band Columns 51
Tables 52
Bibliography 53
v
yiCONTENTS
CHAPTER 3 PURIFICATION OF INDIVIDUAL ORGANIC CHEMICALS 54
CHAPTER 4 PURIFICATION OF INDIVIDUAL INORGANIC A ND METAL-ORGANIC CHEMICALS 286
CHAPTER 5 GENERAL METHODS FOR THE PURIFICATION OF CLASSES OF COMPOUNDS 347
Classes of Compounds 348
INDEX 359
I
|
| any_adam_object | 1 |
| author | Perrin, D. D. 1922-1998 Armarego, Wilfred L. F. Perrin, Dawn R. |
| author_GND | (DE-588)115382593 |
| author_facet | Perrin, D. D. 1922-1998 Armarego, Wilfred L. F. Perrin, Dawn R. |
| author_role | aut aut aut |
| author_sort | Perrin, D. D. 1922-1998 |
| author_variant | d d p dd ddp w l f a wlf wlfa d r p dr drp |
| building | Verbundindex |
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| callnumber-first | T - Technology |
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| callnumber-subject | TP - Chemical Technology |
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| ctrlnum | (OCoLC)362778 (DE-599)BVBBV013826009 |
| dewey-full | 660.2842 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.2842 |
| dewey-search | 660.2842 |
| dewey-sort | 3660.2842 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| edition | 1. ed. |
| format | Book |
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| spelling | Perrin, D. D. 1922-1998 Verfasser (DE-588)115382593 aut Purification of laboratory chemicals D. D. Perrin and W. L. F. Armarego and Dawn R. Perrin 1. ed. Oxford u.a. Pergamon Pr. 1966 VIII, 362 S. txt rdacontent n rdamedia nc rdacarrier Später u.d.T.: Armarego, Wilfred L. F.: Purification of laboratory chemicals Produits chimiques - Affinage Chemicals Purification Chromatographie (DE-588)4010153-8 gnd rswk-swf Chemikalie (DE-588)4009833-3 gnd rswk-swf Reinigung (DE-588)4049250-3 gnd rswk-swf Laboratorium (DE-588)4033927-0 gnd rswk-swf Reinigungsverfahren (DE-588)4391913-3 gnd rswk-swf Ionenaustausch (DE-588)4162300-9 gnd rswk-swf 1\p (DE-588)4014986-9 Enzyklopädie gnd-content Chemikalie (DE-588)4009833-3 s Reinigung (DE-588)4049250-3 s DE-604 Reinigungsverfahren (DE-588)4391913-3 s 2\p DE-604 3\p DE-604 4\p DE-604 Chromatographie (DE-588)4010153-8 s 5\p DE-604 Ionenaustausch (DE-588)4162300-9 s 6\p DE-604 Laboratorium (DE-588)4033927-0 s 7\p DE-604 Armarego, Wilfred L. F. Verfasser aut Perrin, Dawn R. Verfasser aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009455134&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 5\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 6\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 7\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Perrin, D. D. 1922-1998 Armarego, Wilfred L. F. Perrin, Dawn R. Purification of laboratory chemicals Produits chimiques - Affinage Chemicals Purification Chromatographie (DE-588)4010153-8 gnd Chemikalie (DE-588)4009833-3 gnd Reinigung (DE-588)4049250-3 gnd Laboratorium (DE-588)4033927-0 gnd Reinigungsverfahren (DE-588)4391913-3 gnd Ionenaustausch (DE-588)4162300-9 gnd |
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| title | Purification of laboratory chemicals |
| title_auth | Purification of laboratory chemicals |
| title_exact_search | Purification of laboratory chemicals |
| title_full | Purification of laboratory chemicals D. D. Perrin and W. L. F. Armarego and Dawn R. Perrin |
| title_fullStr | Purification of laboratory chemicals D. D. Perrin and W. L. F. Armarego and Dawn R. Perrin |
| title_full_unstemmed | Purification of laboratory chemicals D. D. Perrin and W. L. F. Armarego and Dawn R. Perrin |
| title_short | Purification of laboratory chemicals |
| title_sort | purification of laboratory chemicals |
| topic | Produits chimiques - Affinage Chemicals Purification Chromatographie (DE-588)4010153-8 gnd Chemikalie (DE-588)4009833-3 gnd Reinigung (DE-588)4049250-3 gnd Laboratorium (DE-588)4033927-0 gnd Reinigungsverfahren (DE-588)4391913-3 gnd Ionenaustausch (DE-588)4162300-9 gnd |
| topic_facet | Produits chimiques - Affinage Chemicals Purification Chromatographie Chemikalie Reinigung Laboratorium Reinigungsverfahren Ionenaustausch Enzyklopädie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009455134&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT perrindd purificationoflaboratorychemicals AT armaregowilfredlf purificationoflaboratorychemicals AT perrindawnr purificationoflaboratorychemicals |