Purification process and characterization of ultra high purity metals: application of basic science to metallurgical processing
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2002
|
| Schriftenreihe: | Springer series in materials processing
Physics and astronomy online library |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 411 S. graph. Darst. |
| ISBN: | 3540413227 |
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| 245 | 1 | 0 | |a Purification process and characterization of ultra high purity metals |b application of basic science to metallurgical processing |c Yoshio Waseda ... (eds.) |
| 264 | 1 | |a Berlin [u.a.] |b Springer |c 2002 | |
| 300 | |a XIV, 411 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Springer series in materials processing | |
| 490 | 0 | |a Physics and astronomy online library | |
| 650 | 4 | |a Metals |x Refining | |
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| 700 | 1 | |a Waseda, Yoshio |e Sonstige |4 oth | |
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CONTENTS
PART
I
FUNDAMENTALS
AND
THE
PRESENT
STATUS
OF
PURIFICATION
OF
METALS
1
THE
THERMODYNAMICS
OF
OXYGEN
IN
REACTIVE
METALS
T.H.
OKABE,
K.T.
JACOB
AND
Y.
WASEDA
.
3
1.1
INTRODUCTION
.
3
1.2
VARIOUS
TECHNIQUES
FOR
REMOVING
OXYGEN
FROM
REACTIVE
METALS
.
4
1.2.1
SOLID
STATE
ELECTROTRANSPORT
.
4
1.2.2
DEOXIDATION
USING
METAL/METAL
OXIDE
EQUILIBRIUM
.
5
1.2.3
CALCIUM
HALIDE
FLUX
DEOXIDATION
.
6
1.2.4
ELECTROCHEMICAL
DEOXIDATION
.
7
1.2.5
DEOXIDATION
BY
OXY
HALIDE
FORMATION
.
7
1.3
THE
THERMODYNAMICS
OF
OXYGEN
IN
REACTIVE
METALS
.
8
1.3.1
THE
PRINCIPLE
OF
MEASUREMENT
OF
ULTRA-LOW-OXYGEN
POTENTIALS
.
9
1.3.2
GIBBS
ENERGIES
OF
SOLUTION
OF
OXYGEN
IN
REACTIVE
METALS
.
10
1.4
THE
REMOVAL
OF
OXYGEN
FROM
REACTIVE
METALS
.
13
1.4.1
THE
THERMODYNAMIC
PROPERTIES
OF
OXYGEN
IN
RARE
EARTH
METALS
.
13
1.4.2
THE
REMOVAL
OF
OXYGEN
FROM
RARE
EARTH
METALS
.
21
1.4.3
COMPARISON
WITH
OTHER
DIRECT
OXYGEN
REMOVAL
TECHNIQUES
25
1.5
PURITY
EVALUATION
OF
DEOXIDIZED
REACTIVE
METALS
.
29
1.5.1
THE
REMOVAL
OF
OXYGEN
FROM
TITANIUM
.
29
1.5.2
PURITY
EVALUATION
OF
DEOXIDIZED
TITANIUM
.
31
1.6
SUMMARY
.
34
REFERENCES
.
35
2
PRINCIPLES
OF
METAL
PURIFICATION
AND
PURITY
EVALUATION
T.
KEKESI
AND
M.
ISSHIKI
.
39
2.1
METHODS
OF
PURIFICATION
.
39
2.1.1
PYROMETALLURGICAL
REFINING
.
41
2.1.2
HYDROMETALLURGICAL
PURIFICATION
.
42
2.1.3
ELECTROCHEMICAL
PURIFICATION
.
51
2.1.4
PURIFICATION
METHODS
BASED
ON
SOLID-LIQUID
EQUILIBRIA
.
54
VIII
CONTENTS
2.1.5
PURIFICATION
BY
SELECTIVE
VOLATILIZATION
.
56
2.1.6
PURIFICATION
BY
ELECTROTRANSPORT
.
60
2.2
PURITY
EVALUATION
.
61
2.2.1
DIRECT
INDICATION
OF
PURITY
.
61
2.2.2
INDIRECT
INDICATION
OF
PURITY
.
62
2.2.3
COMPARISON
OF
ACHIEVED
PURITY
LEVELS
.
65
REFERENCES
.
67
3
THE
PURIFICATION
OF
BASE
TRANSITION
METALS
T.
KEKESI
AND
M.
ISSHIKI
.
71
3.1
THE
PURIFICATION
OF
TITANIUM
.
71
3.2
THE
PURIFICATION
OF
VANADIUM
.
74
3.3
THE
PURIFICATION
OF
CHROMIUM
.
77
3.4
THE
PURIFICATION
OF
MANGANESE
.
78
3.5
THE
PURIFICATION
OF
IRON
.
80
3.6
THE
PURIFICATION
OF
COBALT
.
83
3.7
THE
PURIFICATION
OF
NICKEL
.
85
3.8
THE
PURIFICATION
OF
COPPER
.
89
3.9
THE
PURIFICATION
OF
ZINC
.
97
REFERENCES
.
100
4
REFRACTORY
METALS
A.
KOETHE
.
103
4.1
INTRODUCTION
.
103
4.2
GROUP
IVA
METALS
.
105
4.2.1
TITANIUM
.
105
4.2.2
ZIRCONIUM
AND
HAFNIUM
.
109
4.3
GROUP
VA
METALS
.
114
4.3.1
VANADIUM
.
114
4.3.2
NIOBIUM
.
114
4.3.3
TANTALUM
.
121
4.4
GROUP
VIA
METALS
.
121
4.4.1
CHROMIUM
.
121
4.4.2
MOLYBDENUM
.
122
4.4.3
TUNGSTEN
.
125
4.5
GROUP
VILA
METALS
.
125
4.5.1
RHENIUM
.
125
4.6
INTERSTITIAL
IMPURITIES
.
126
4.6.1
GENERAL
REMARKS
.
126
4.6.2
NITROGEN
AND
HYDROGEN
.
129
4.6.3
OXYGEN
.
133
4.6.4
CARBON
.
136
4.6.5
PURIFICATION
BY
GETTERING
WITH
A
MORE
REACTIVE
METAL
.
137
4.7
PURIFICATION
BY
ELECTROTRANSPORT
.
138
CONTENTS
IX
4.8
DETERIORATION
OF
THE
PURITY
OF
UHP
REFRACTORY
METALS
DURING
PREPARATION
OR
APPLICATION
.
139
REFERENCES
.
140
5
PURIFICATION
OF
THE
RARE
EARTH
METALS
D.
FORT
.
145
5.1
INTRODUCTION
.
145
5.2
BACKGROUND
INFORMATION
.
145
5.2.1
IMPURITIES
IN
RARE
EARTH
METALS
.
145
5.2.2
THE
BASIC
PROPERTIES
OF
THE
RARE
EARTHS
.
147
5.3
PURIFICATION
TECHNIQUES
FOR
RARE
EARTH
METALS
.
149
5.3.1
VACUUM
MELTING
AND
VACUUM
DEGASSING
.
150
5.3.2
ZONE
REFINING
.
151
5.3.3
VAPOR
TECHNIQUES
.
154
5.3.4
SOLID
STATE
ELECTROTRANSPORT
(SSE)
.
158
5.4
RETAINING
PURITY
DURING
SAMPLE
PREPARATION
AND
CRYSTAL
GROWTH
164
5.4.1
COMBINING
PURIFICATION
AND
CRYSTAL
GROWTH
.
164
5.4.2
CRYSTAL
GROWTH
AFTER
PURIFICATION
.
165
5.5
PURIFICATION
ROUTES
FOR
RARE
EARTH
METALS
.
166
5.6
INDIVIDUAL
ELEMENTS
.
167
REFERENCES
.
174
PART
II
NEW
METHODS
FOR
PURIFICATION
6
HYDROGEN
PLASMA
ARC
MELTING
K.
MIMURA
AND
M.
ISSHIKI
.
181
6.1
INTRODUCTION
.
181
6.2
THE
REMOVAL
OF
NONMETALLIC
IMPURITIES
BY
HYDROGEN
PLASMA
ARC
MELTING
.
182
6.2.1
THE
REMOVAL
OF
OXYGEN,
NITROGEN
AND
CARBON
FROM
IRON
.
184
6.2.2
THE
REMOVAL
OF
OXYGEN
AND
NITROGEN
FROM
COBALT
.
188
6.2.3
THE
REMOVAL
OF
OXYGEN
AND
NITROGEN
FROM
REFRACTORY
METALS
.
190
6.3
THE
REMOVAL
OF
METALLIC
IMPURITY
ELEMENTS
BY
HYDROGEN
PLASMA
ARC
MELTING
.
192
6.3.1
THE
PURIFICATION
OF
COMMERCIALLY
PURE
REFRACTORY
METALS.
193
6.3.2
THE
REMOVAL
OF
ALLOYING
ELEMENTS
FROM
REFRACTORY
METAL
BASED
ALLOYS
.
195
6.3.3
THE
MECHANISM
FOR
REMOVING
METALLIC
IMPURITY
ELEMENTS
FROM
THE
MELT
BY
HPAM
.
198
6.4
SUMMARY
.
200
REFERENCES
.
201
X
CONTENTS
7
ION-BEAM
DEPOSITION
K.
MIYAKE
.
203
7.1
INTRODUCTION
.
203
7.2
THE
BASIC
PRINCIPLE
OF
THE
ION-BEAM
DEPOSITION
METHOD
.
204
7.3
THE
DESIGN
CONCEPTS
OF
ION-BEAM
DEPOSITION
SYSTEMS
.
206
7.3.1
THE
ION
ENERGY
RANGE
.
207
7.3.2
ION
CURRENT
DENSITY
AND
VACUUM
REQUIREMENTS
.
208
7.3.3
DEPOSITION
TIME
AND
DOSE
CALCULATION
.
209
7.3.4
THE
VACUUM
PUMPING
SYSTEM
.
210
7.3.5
THE
PRODUCTION
OF
A
HIGH-INTENSITY,
LOW-ENERGY
METAL
ION
BEAM
.
210
7.3.6
ION
BEAM
TRANSPORT
AND
DECELERATION
.
212
7.3.7
SAMPLE
MANIPULATION
AND
FILM
DEPOSITION
.
215
7.4
HIGH-PURITY
AND
HIGH-CORROSION-RESISTANCE
FE
FILM
FORMATION
.
215
7.5
SUMMARY
.
221
REFERENCES
.
221
8
PURIFICATION
AND
ISOTOPE
SEPARATION
BY
LASER
TECHNIQUES
S.
SATO
.
223
8.1
INTRODUCTION
.
223
8.1.1
LASER
LIGHT
.
223
8.2
ABSORPTION
AND
EMISSION
PROCESSES
OF
LIGHT
.
225
8.3
LASER
MANIPULATION
OF
ATOMS
.
227
8.3.1
RADIATION
FORCE
.
228
8.3.2
DECELERATION
OF
AN
ATOM
.
230
8.3.3
DEFLECTION
OF
AN
ATOMIC
BEAM
.
232
8.3.4
REFLECTION
AND
FOCUSING
OF
THE
ATOMIC
BEAM
.
233
8.4
LASER
ISOTOPE
SEPARATION
.
235
8.4.1
ATOMIC
VAPOR
LASER
ISOTOPE
SEPARATION
(AVLIS)
OF
URANIUM
.
235
8.4.2
MOLECULAR
LASER
ISOTOPE
SEPARATION
(MLIS)
OF
URANIUM
.
236
8.4.3
OTHER
ELEMENTS
.
237
8.5
LIGHT-INDUCED
DRIFT
.
237
8.5.1
THE
PRINCIPLE
.
238
REFERENCES
.
245
CONTENTS
XI
PART
III
CHARACTERIZATION
9
ELECTRICAL
PROPERTIES
OF
ULTRA-HIGH-PURITY
METALS
E.
HASHIMOTO
AND
Y,
UEDA
.
249
9.1
INTRODUCTION
.
249
9.2
THE
TEMPERATURE
DEPENDENCE
OF
THE
ELECTRICAL
RESISTIVITY
.
249
9.3
SPECIMEN
PREPARATION
AND
RESISTIVITY
MEASUREMENTS
.
254
9.3.1
SPECIMEN
PREPARATION
.
254
9.3.2
RESISTIVITY
MEASUREMENTS
.
255
9.4
THE
ANISOTROPY
OF
THE
SIZE
EFFECT
IN
DE
ELECTRICAL
RESISTIVITY
.
256
9.4.1
DEPENDENCE
ON
THE
SURFACE
ORIENTATION
.
256
9.4.2
DEPENDENCE
ON
THE
AXIS
ORIENTATION
(DIRECTION
OF
CURRENT
FLOW)
.
260
9.5
ANISOTROPY
OF
THE
DE
ELECTRICAL
RESISTIVITY
IN
CUBIC
METALS
.
260
9.5.1
ANISOTROPY
OF
THE
BULK
RESIDUAL
RESISTIVITY
PB
AT
4.2K
.
261
9.5.2
THE
TEMPERATURE
DEPENDENCE
OF
THE
ANISOTROPY
.
264
9.6
NONLINEAR
I-V
CHARACTERISTICS
IN
ULTRA-HIGH-PURITY
METALS
.
265
9.7
BALLISTIC
ELECTRON
TRANSPORT
CHARACTERISTICS
IN
ULTRA-HIGH-PURITY
METALS:
NEGATIVE
BEND
RESISTANCE
.
267
9.8
MAGNETIC
BREAKDOWN
OSCILLATION
IN
MAGNETORESISTANCE
.
271
9.9
SUMMARY
.
274
REFERENCES
.
275
10
SURFACES
AND
INTERFACES
S.
SUZUKI
.
277
10.1
INTRODUCTION
.
277
10.2
THERMODYNAMIC
FEATURES
OF
SURFACES
AND
INTERFACES
.
279
10.2.1
INTERFACIAL
ENERGY
.
279
10.2.2
INTERFACIAL
SEGREGATION
.
279
10.2.3
INTERFACIAL
STRUCTURE
.
281
10.3
MEASUREMENT
OF
SURFACE
AND
INTERFACE
COMPOSITIONS
.
282
10.4
SURFACE
BEHAVIOR
.
286
10.4.1
SURFACE
SEGREGATION
.
286
10.4.2
NATIVE
OXIDE
LAYER
.
288
10.5
INTERFACIAL
BEHAVIOR
.
290
10.5.1
GRAIN
BOUNDARY
SEGREGATION
IN
POLYCRYSTALS
.
291
10.5.2
GRAIN
BOUNDARY
SEGREGATION
IN
BICRYSTALS
.
298
10.6
FURTHER
APPROACHES
FOR
ATTAINING
SURFACE
AND
INTERFACE
CHARACTERIZATION
.
300
10.7
SUMMARY
.
301
REFERENCES
.
302
XII
CONTENTS
11
MECHANICAL
PROPERTIES
L.
HOLLANG
.
305
11.1
INTRODUCTION
.
305
11.2
THE
ONSET
OF
SLIP
.
308
11.3
THE
PLASTIC
BEHAVIOR
OF
FEE
METALS
.
311
11.3.1
THE
WORK-HARDENING
BEHAVIOR
AND
MICROSTRUCTURE
OF
FEE
METALS
.
312
11.3.2
THERMALLY
ACTIVATED
DISLOCATION
MOTION
IN
FEE
METALS
.
315
11.4
THE
PLASTIC
BEHAVIOUR
OF
PURE
BEE
METALS
.
319
11.4.1
THE
SLIP
GEOMETRY
OF
PURE
BEE
METALS
.
320
11.4.2
THE
WORK-HARDENING
BEHAVIOUR
AND
MICROSTRUCTURE
OF
BCC
METALS
.
321
11.4.3
THE
EFFECTIVE
FLOW
STRESS
OF
BCC
METALS
.
325
11.4.4
THE
FLOW-STRESS
ASYMMETRY
OF
BCC
METALS
.
329
11.4.5
ANOMALOUS
SLIP
IN
BCC
METALS
.
332
11.4.6
SOFTENING
OF BCC
METALS
BY
ATOMIC
DEFECTS
.
333
11.4.7
THE
KINK
THEORY
OF
BCC
METALS
.
334
11.4.8
ELEMENTARY
SLIP
STEPS
IN
HIGH-PURITY
BCC
METALS
.
338
11.4.9
CONCLUSIONS
FOR
SLIP
IN
BCC
METALS
.
341
11.5
SUMMARY
.
343
REFERENCES
.
345
12
ATOMIC
DEFECTS
IN
HIGH-PURITY
METALS:
FUNDAMENTALS
AND
EQUILIBRIUM
CONCENTRATIONS
A.
SEEGER
.
349
12.1
WHAT
IS
AN
ATOMIC
DEFECT?
.
349
12.2
HOW
DO
WE
CHARACTERIZE
INTRINSIC
ATOMIC
DEFECTS?
.
351
12.3
HOW
ARE
ATOMIC
DEFECTS
GENERATED?
.
354
12.4
INTRINSIC
ATOMIC
DEFECTS
IN
THERMAL
EQUILIBRIUM
.
358
12.5
THE
INFLUENCE
OF
IMPURITIES
ON
THE
VACANCY
CONCENTRATION
IN
THERMAL
EQUILIBRIUM
.
362
12.6
EXPERIMENTAL
STUDIES
OF
THERMAL-EQUILIBRIUM
DEFECTS
.
363
12.6.1
GENERAL
REMARKS
.
363
12.6.2
CALORIMETRY
.
364
12.6.3
DIFFERENTIAL
DILATOMETRY
.
366
12.6.4
POSITRON
ANNIHILATION
.
370
12.6.5
SPIN
ROTATION
OF
POSITIVE
MUONS
(/Z
+
SR)
.
380
12.7
A
COMPARISON
OF
THE
DIFFERENT
TECHNIQUES
.
385
REFERENCES
.
398
INDEX
.
403 |
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| discipline | Chemie / Pharmazie Physik Werkstoffwissenschaften |
| format | Book |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV013520414 |
| illustrated | Illustrated |
| indexdate | 2024-08-22T00:34:47Z |
| institution | BVB |
| isbn | 3540413227 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009228710 |
| oclc_num | 45583531 |
| open_access_boolean | |
| owner | DE-703 DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-91G DE-BY-TUM |
| owner_facet | DE-703 DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-91G DE-BY-TUM |
| physical | XIV, 411 S. graph. Darst. |
| publishDate | 2002 |
| publishDateSearch | 2002 |
| publishDateSort | 2002 |
| publisher | Springer |
| record_format | marc |
| series2 | Springer series in materials processing Physics and astronomy online library |
| spelling | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing Yoshio Waseda ... (eds.) Berlin [u.a.] Springer 2002 XIV, 411 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Springer series in materials processing Physics and astronomy online library Metals Refining Mikrostruktur (DE-588)4131028-7 gnd rswk-swf Stoffeigenschaft (DE-588)4192147-1 gnd rswk-swf Metall (DE-588)4038860-8 gnd rswk-swf Raffination (DE-588)4048288-1 gnd rswk-swf Reinstmetall (DE-588)4177597-1 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Reinstmetall (DE-588)4177597-1 s DE-604 Metall (DE-588)4038860-8 s Raffination (DE-588)4048288-1 s Stoffeigenschaft (DE-588)4192147-1 s Mikrostruktur (DE-588)4131028-7 s Waseda, Yoshio Sonstige oth DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009228710&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing Metals Refining Mikrostruktur (DE-588)4131028-7 gnd Stoffeigenschaft (DE-588)4192147-1 gnd Metall (DE-588)4038860-8 gnd Raffination (DE-588)4048288-1 gnd Reinstmetall (DE-588)4177597-1 gnd |
| subject_GND | (DE-588)4131028-7 (DE-588)4192147-1 (DE-588)4038860-8 (DE-588)4048288-1 (DE-588)4177597-1 (DE-588)4143413-4 |
| title | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing |
| title_auth | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing |
| title_exact_search | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing |
| title_full | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing Yoshio Waseda ... (eds.) |
| title_fullStr | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing Yoshio Waseda ... (eds.) |
| title_full_unstemmed | Purification process and characterization of ultra high purity metals application of basic science to metallurgical processing Yoshio Waseda ... (eds.) |
| title_short | Purification process and characterization of ultra high purity metals |
| title_sort | purification process and characterization of ultra high purity metals application of basic science to metallurgical processing |
| title_sub | application of basic science to metallurgical processing |
| topic | Metals Refining Mikrostruktur (DE-588)4131028-7 gnd Stoffeigenschaft (DE-588)4192147-1 gnd Metall (DE-588)4038860-8 gnd Raffination (DE-588)4048288-1 gnd Reinstmetall (DE-588)4177597-1 gnd |
| topic_facet | Metals Refining Mikrostruktur Stoffeigenschaft Metall Raffination Reinstmetall Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009228710&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT wasedayoshio purificationprocessandcharacterizationofultrahighpuritymetalsapplicationofbasicsciencetometallurgicalprocessing |