Capillary electrophoresis for food analysis: method development
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| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Cambridge
Royal Soc. of Chemisty
2000
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XIV, 127 S. Ill., graph. Darst. |
| ISBN: | 0854044922 |
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Record in the Search Index
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| adam_text | Titel: Capillary electrophoresis for food analysis
Autor: Frazier, Richard A.
Jahr: 2000
Contents
Preface
Glossary
1 Abbreviations
2 Symbols
3 Definitions
Chapter 1 Background Theory and Principles of
Capillary Electrophoresis
Chapter
v
xi
xi
xii
xiii
I 2 introduction What is Capillary Electrophoresis? 1 1
3 Instrumentation 1
4 Electrophoresis Theory 2
5 Electroosmotic Flow (EOF) 3
6 The Electropherogram 6
7 Summary 6
2 Modes of Separation 8
1 Introduction 8
2 Capillary Zone Electrophoresis (CZE) 8
3 Micellar Electrokinetic Chromatography (MEKC) 9
4 Chiral Separations 10
5 Separation by Sieving Mechanisms 12
6 Capillary Isoelectric Focusing (CIEF) 12
7 Capillary Isotachophoresis (CFTP) 13
8 Capillary Electrochromatography (CEC) 14
9 References 15
VM
viii Contents
Chapter 3 Experimental Variables in Capillary
Electrophoresis 16
1 Introduction 16
2 Buffer Properties 16
3 Buffer Additives 17
4 Capillary Properties 17
5 Capillary Conditioning 19
6 Instrumental Parameters 19
7 Detection Mode 22
Chapter 4 Method Development for Capillary
Electrophoresis 25
1 Introduction 25
2 Is CE the Appropriate Technique? 25
3 Aims 28
4 Literature Resources 28
5 Sample Considerations 28
6 Choice of Mode of CE and Detection 31
Chapter 5 Method Development: Capillary Zone
Electrophoresis 32
1 Introduction 32
2 Resolution 32
3 Stability 39
4 Quantification 41
5 Summary 46
6 References 46
Chapter 6 Method Development: Micellar Electrokinetic
Chromatography 47
1 Introduction 47
2 Resolution 47
3 Stability 55
4 Quantification 56
5 Summary 56
6 Reference 56
Chapter 7 Method Validation and Transfer 57
3 Validation 57
2 Method Transfer 57
3 Summary 59
4 References 60
Contents
Chapter 8 CE Troubleshooting
1 Introduction
2 Unstable Current
3 Unstable Baselines
4 Low Detector Signal
5 Poor Migration Time Reproducibility
6 Non-Reproducible Peak Areas
7 Irregular Peak Shapes
8 Summary
9 References
Chapter 9 CE Applications for Food Analy
1 Introduction
2 Proteins and Peptides
3 Amino Acids and Biogenic Amines
4 Maillard Reaction Products
5 Food Additives
6 Specific Nutrients
7 Phenolic Compounds
8 Organic Acids
9 Toxin and Residue Analysis
10 References
61
61
61
63
63
63
65
65
66
66
67
67
67
76
80
80
80
81
84
84
84
Appendices
Appendix A Example 1 of CE Method Development:
The Determination of Niacin by CZE
1 Introduction
2 Aim
3 Sample Preparation
4 Selection of Mode and Detection
5 CZE Method Development
6 References
88
89
89
89
89
90
90
93
Appendix B Example 2 of CE Method Development: The
Separation of Green Tea Catechins by MEKC 95
1 Introduction 95
2 Aim 95
3 Sample Considerations 95
4 Selection of Mode and Detection 96
5 CZE Method Development 96
6 MEKC Method Development 98
7 References 102
x Contents
Appendix C Example 3 of CE Method Development: The
Development of a CE Method for the
Simultaneous Analysis of Artificial
Sweeteners, Preservatives and Colours
in Soft Drinks 104
1 Introduction 104
2 Aim 105
3 Sample Preparation 105
4 Selection of Mode and Detection 106
5 CZE Method Development 106
6 MEKC Method Development 108
7 References 110
Bibliography
1 Books
2 CD-ROMs
3 Internet Websites
4 Instrument Manufacturers
5 Consumables Suppliers
113
113
114
115
115
116
Subject Index
118
|
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| language | English |
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| spelling | Frazier, Richard A. Verfasser aut Capillary electrophoresis for food analysis method development Richard A. Frazier, Jennifer M. Ames and Harry E. Nursten Cambridge Royal Soc. of Chemisty 2000 XIV, 127 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Capillary electrophoresis Food Analysis Kapillarelektrophorese (DE-588)4290002-5 gnd rswk-swf Lebensmittelanalyse (DE-588)4167032-2 gnd rswk-swf Lebensmittelanalyse (DE-588)4167032-2 s Kapillarelektrophorese (DE-588)4290002-5 s DE-604 Ames, Jennifer M. Verfasser aut Nursten, Harry E. Verfasser (DE-588)127383654 aut HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009226426&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Frazier, Richard A. Ames, Jennifer M. Nursten, Harry E. Capillary electrophoresis for food analysis method development Capillary electrophoresis Food Analysis Kapillarelektrophorese (DE-588)4290002-5 gnd Lebensmittelanalyse (DE-588)4167032-2 gnd |
| subject_GND | (DE-588)4290002-5 (DE-588)4167032-2 |
| title | Capillary electrophoresis for food analysis method development |
| title_auth | Capillary electrophoresis for food analysis method development |
| title_exact_search | Capillary electrophoresis for food analysis method development |
| title_full | Capillary electrophoresis for food analysis method development Richard A. Frazier, Jennifer M. Ames and Harry E. Nursten |
| title_fullStr | Capillary electrophoresis for food analysis method development Richard A. Frazier, Jennifer M. Ames and Harry E. Nursten |
| title_full_unstemmed | Capillary electrophoresis for food analysis method development Richard A. Frazier, Jennifer M. Ames and Harry E. Nursten |
| title_short | Capillary electrophoresis for food analysis |
| title_sort | capillary electrophoresis for food analysis method development |
| title_sub | method development |
| topic | Capillary electrophoresis Food Analysis Kapillarelektrophorese (DE-588)4290002-5 gnd Lebensmittelanalyse (DE-588)4167032-2 gnd |
| topic_facet | Capillary electrophoresis Food Analysis Kapillarelektrophorese Lebensmittelanalyse |
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