Handbook of industrial crystallization:
Gespeichert in:
Format: | Buch |
---|---|
Sprache: | English |
Veröffentlicht: |
Boston [u.a.]
Butterworth-Heinemann
2002
|
Ausgabe: | 2. ed. |
Schlagworte: | |
Online-Zugang: | Inhaltsverzeichnis |
Beschreibung: | XIII, 313 S. Ill., graph. Darst. |
ISBN: | 0750670126 |
Internformat
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245 | 1 | 0 | |a Handbook of industrial crystallization |c ed. by Allan S. Myerson |
250 | |a 2. ed. | ||
264 | 1 | |a Boston [u.a.] |b Butterworth-Heinemann |c 2002 | |
300 | |a XIII, 313 S. |b Ill., graph. Darst. | ||
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Datensatz im Suchindex
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adam_text | PREFACE TO THE FIRST EDITION xi
PREFACE TO THE SECOND EDITION xiii
CHAPTER 1 SOLUTIONS AND SOLUTION
PROPERTIES /
Albert M. Schwartz and Allan S. Myerson
1.1. Introduction and Motivation /
1.2. Umts 7
1.3. Solubility of Inorganics /
1.3.1. Basic Concepts /
1.3.2. Sparingly Soluble Species—Dilute Solutions 4
1.3.3. Concentrated Solutions 5
1.4. Solubility of Organics 11
1.4.1. Thermodynamic Concepts and Ideal Solubility //
1.4.2. Regulär Solution Theory 13
1.4.3. Group Contribution Methods 14
1.4.4. Solubility in Mixed Solvents 14
1.4.5. Measurement of Solubility 15
1.5. Supersaturation and Metastability 16
1.5.1. Units 16
1.5.2. Metastability and the Metastable Limit 17
1.5.3. Methods to Create Supersaturation 18
1.6. Solution Properties 20
1.6.1. Density 20
1.6.2. Viscosity 20
1.6.3. Diffusivity 22
1.7. Thermal Properties 25
1.7.1. HeatCapacity 26
1.7.2. Latent Heat 27
1.7.3. Heats of Mixing, Solution, and Crystallization 28
Nomenclature 29
References 30
CHAPTER 2 CRYSTALS, CRYSTAL GROWTH, AND
NUCLEATION 33
Allan S. Myerson and Rajiv Ginde
2.1. Crystals 33
2.1.1. Lattices and Crystal Systems 33
2.1.2. Miller Indices and Lattice Planes 35
2.1.3. Crystal Structure and Bonding 35
2.1.4. Polymorphism 38
2.1.5. Isomorphism and Solid Solutions 40
2.1.6. Imperfections in Crystals 40
2.1.7. Crystal Habit 41
2.1.8. Prediction of Crystal Habit 42
2.2. Nucleation 43
2.2.1. Homogeneous Nucleation 45
2.2.2. Heterogeneous Nucleation 46
2.2.3. Secondary Nucleation 46
2.2.4. Nucleation Kinetics 50
2.2.5. Application to Industrial Crystallizers 52
2.3. Crystal Growth 53
2.3.1. Basic Concepts 53
2.3.2. Theories of Crystal Growth 54
2.3.3. Crystal Growth Kinetics 57
2.3.4. Ostwald Ripening 61
2.3.5. Size-Dependent Growth and Growth
Rate Dispersion 62
Nomenclature 63
References 63
CHAPTER 3 THE INFLUENCE OF IMPURITIES
AND SOLVENTS ON CRYSTALLIZATION 67
Paul A. Meenan, Stephen R. Anderson, and Diana L. Klug
3.1. Introduction 67
3.2. Factors Determining Crystal Shape 67
3.2.1. The Role of the Solid State in Shape
Development 68
3.3. Influence of Solvents on Volume and Surface
Diffusion Steps 70
3.4. Structure of the Crystalline Interface 71
3.5. Factors Affecting Impurity Incorporation 72
3.5.1. Equilibrium Separation 72
3.5.2. Nonequilibrium Separation 74
3.5.3. Experimental Approaches to Distinguishing
Impurity Retention Mechanism 78
3.6. Effect of Impurities on Crystal Growth Rate 80
3.6.1. Effect on the Movement of Steps 80
3.6.2. Impurity Adsorption Isotherms 82
3.6.3. Growth Models Based on Adsorption Isotherms 83
3.7. Some Chemical Aspects of Solvent and Impurity
Interactions 86
3.8. Tailor-Made Additives 90
3.9. Effect of Solvents on Crystal Growth 93
3.9.1. Role of the Solvent 93
3.9.2. Jackson a-Factor 94
3.9.3. Effect of a-Factor on Growth Mechanism 95
3.10. Summary 96
References 97
CHAPTER 4 ANALYSIS AND MEASUREMENT
OF CRYSTALLIZATION UTILIZING THE
POPULATION BALANCE 101
K.A. Berglund
4.1. Particle Size and Distribution 101
4.2. Measurement of Size Distribution 102
4.3. The Mixed Suspension, Mixed Product Removal
(MSMPR) Formalism for the Population Balance 104
4.3.1. Mass Balance 106
4.4. Generalized Population Balance 107
4.5. Extension and Violations of the MSMPR Model 107
4.5.1. Size-Dependent Crystal Growth 107
4.5.2. Growth Rate Dispersion 108
4.5.3. Methods to Treat Experimental Data 108
4.5.4. Agglomeration 110
4.5.5. Alteration of Residence Time Distribution to
Control CSD ///
4.6. Summary 113
Nomenclature 113
References 113
CHAPTER 5 CRYSTALLIZER SELECTION
AND DESIGN 115
Richard C. Bennett
5.1. Fundamentals 115
5.1.1. Definition 115
5.1.2. Heat Effects in a Crystallization Process 115
5.1.3. Yield of a Crystallization Process 116
5.1.4. Fractional Crystallization H6
5.1.5. Nucleation ll7
5.1.6. Population Density Balance HS
5.1.7. Crystal Size Distribution HS
5.1.8. Crystal Wcight Distribution H9
5.1.9. Conlact Nucleation 120
5.1.10. Crystallizers with Fines Removal 120
5.1.11. Cyclic Behavior 122
5.2. Sclcction of a Crystallizer 123
5.2.1. Information Required for Evaluation 123
5.2.2. Solubility ^i
5.2.3. Scale of Operation 124
5.2.4. Batch or Continuous Operation /24
5.2.5. Multistagc Crystallizers 124
5.2.6. Mechanical Vapor Recompression /26
5.2.7. Rcuctive Crystallizers 126
5.3. Equipment Typcs ^-27
5.3.1. Batch Crystallizers /27
5.3.2. Fluidized Suspension Crystallizer 128
5.3.3. Forced-Circulation Crystallizer /29
5.3.4. Draft Tube Baffle (DTB) Crystallizer 129
5.3.5. Surface-Cooled Crystallizers 130
5.3.6. Dircct-Contact Refrigeration Crystallizers /i/
5.3.7. Teflon Tube Crystallizer 131
5.3.8. Spray Crystallization /J2
5.3.9. General Characteristics 133
5.4. Crystallizer Design Procedure 133
5.5. Instrumentation and Control 136
5.5.1. Liquid Level Control /iö
5.5.2. Absolute Pressure Control 136
5.5.3. Magma (Slurry) Density Recorder Controller 136
5.5.4. Steam Flow Recorder Controller 137
5.5.5. Feed-Flow Recording Controller 137
5.5.6. Discharge Control 137
5.5.7. Miscellaneous 137
5.5.8. Distributed Control Systems 137
5.5.9. Discharging 137
5 5.10. Sampling 137
5.6. Crystallizer Costs ]38
Nomcnclature 139
Rcferenccs 140
CHAPTF.R6 PRECIPITATION PROCESSES 141
P.H. Kurpinski and J.S. Wvy
6.1. Introduction 14 j
6.2. Physical and Thermodynamic Properties 141
6.2.1 Supersaturation Driving Force and Solubility 141
6.2.2. The Gibbs-Thomson Equation and Surface Energy 142
6.2.3. Precipitation Diagrams 142
6.2.4. Surface Chemistry and Colloid Stability 143
6.3. Nucleation Kinetics y^j
6.3 1 Kinetics of Primary Nucleation 143
6.3.2. Investigations of Nucleation Kinetics 144
6.4. Crystal Growth Kinetics y^g
6.4.1. Growth Controlled by Mass Transport 146
6.4.2. Growth Controlled by Surface Integration 146
6.4.3. Growth Controlled by Combined Mechanisms 147
6.4.4. Critical Growth Rate ^7
6.4.5. Other Factors Affecting Crystal Growth 148
6.5. Other Processes Attributes in Precipitation 148
6.5.1. Ostwald Ripening j^g
6.5.2. Aggregation ]49
6.5.3. Mixing /50
6.6. Experimental Techniques 152
6.6.1. Supersaturation Measurements 152
6.6.2. Constant Composition Method 152
6.6.3. Critical Growth Rate Measurements 153
6.6.4. Instantaneous Mixing Devices 153
6.6.5. Sizing ofPrecipitates 153
6.7. Modeling and Control of Crystal
Size and CSD 154
6.7.1. Modeling of Crystal Size Distribution 154
6.7.2. Size Control 156
6.8. Precipitation in Practice 157
6.8.1. Continuous Precipitation 158
6.8.2. Batch Precipitation 158
6.9. Summary 158
Nomenclature 159
References 159
CHAPTER7 MELT CRYSTALLIZATION 161
J. Ulrich and H.C. Bülau
7.1. Definitions 161
7.2. Benefits of Melt Crystallization 161
7.3. Phase Diagrams 162
7.3.1. What to Learn from Phase Diagrams 162
7.3.2. How to Obtain Phase Diagrams 163
7.4. Crystallization Kinetics 163
7.4.1. Importance of the Crystallization Kinetics to
Melt Crystallization 163
7.4.2. Theoretical Approach to Crystallization
Kinetics 164
7.5. Solid Layer Crystallization 166
7.5.1. Advantages - 166
7.5.2. Limitations 167
7.6. Suspension Crystallization 167
7.6.1. Advantages 167
7.6.2. Limitations 167
7.7. Concepts of Existing Plants 167
7.7.1. Solid Layer Processes 167
7.7.2. Suspension Process Concepts 171
7.8. The Sweating Step 173
7.9. The Washing Step 174
7.10. Continuous Plants 175
7.10.1. Advantages 175
7.10.2. Process Concepts 175
7.10.3. Problems 177
7.10.4. Summary and a View to the Future 177
References 177
CHAPTER 8 CRYSTALLIZER MIXING:
UNDERSTANDING AND MODELING
CRYSTALLIZER MIXING AND SUSPENSION FLOW 181
Daniel Green
8.1. Introduction 181
8.2. Crystallizer Flows 181
8.3. Distribution of Key Variables in Crystallizers 182
8.4. Crystallizers 184
8.4.1. Agitated Suspension 184
8.4.2. Fluidized Bed 757
8.4.3. Melt Crystallizers 188
8.4.4. Feed Strategies 188
8.4.5. Agitators J88
8.5. Scale-Up /§p
8.6. Modeling jgj
8.6.1. Experimental Modeling 191
8.6.2. Computational Modeling 194
8.6.3. Impeller Treatment 195
8.6.4. Treatment ofTurbulence 195
8.6.5. Modeling Multiphase Flow 195
8.6.6. Mixing Models 197
8.6.7. Comprehensive Models 197
8.7. Summary 197
Acknowledgment 198
References 198
CHAPTER 9 CONTROL OF CRYSTALLIZATION
PROCESSES 201
J.B. Rawlings, C. W. Sink, and S.M. Miller
9.1. Introduction 201
9.1.1. Overview 201
9.1.2. Typical Crystallizer Design 202
9.1.3. Measurements 202
9.1.4. Manipulated Variables 203
9.1.5. Control Algorithm 203
9.2. Feedback Controllers 204
9.2.1. Three Mode (PID) Controllers 204
9.2.2. Stability Considerations 205
9.2.3. Automatic/Manual Control Modes 206
9.2.4. Tuning of PID Controllers 206
9.2.5. Further Feedback Control Techniques 207
9.3. Industrial Crystallizer Control 209
9.3.1. Crystallizer Control Objectives 209
9.3.2. Continuous Crystallization Control 210
9.3.3. Batch Crystallization Control 215
9.3.4. Sensor and Control Element Considerations 219
9.4. Advanced Continuous Crystallizer Control 221
9.4.1. Model Identification 221
9.4.2. Stability Considerations 222
9A3. Feedback Controller Design 222
9.5. Advanced Batch Crystallizer Control 223
9.5.1. Model Identification 224
9.5.2. Optimal Open-Loop Control 224
9.5.3. Feedback Controller Design 228
Nomenclature 228
References 229
CHAPTER 10 BATCH CRYSTALLIZATION 231
J.S. Wey and P.H. Karpinski
10.1. Introduction 231
10.2. Batch Crystallizers 231
10.2.1. Laboratory Batch Crystallizers 231
10.2.2. Industrial Batch Crystallizers 233
10.3. Batch Crystallization Analysis 234
10.3.1. Batch Conservation Equations 234
10.3.2. CSD Analysis and Kinetic Studies 236
10.4. Factors Affecting Batch Crystallization 238
10.4.1. Batch Cycle Time 238
10.4.2. Supersaturation Profile 239
10.4.3. External Seeding 239
10.4.4. Fouling Control 241
10.4.5. CSD Control 241
10.4.6. Growth Rate Dispersions 242
10.4.7. Mixing 243
10.5. Batch Crystallization Operations 244
10.5.1. Cooling Crystallization 244
10.5.2. Evaporative Crystallization 246
10.5.3. Antisolvent Crystallization (Salting-Out) 246
10.6. Summary 246
Nomenclature 247
References 248
CHAPTER 11 CRYSTALL1ZATION IN THE
PHARMACEUTICAL AND BIOPROCESSING
INDUSTRIES 249
DJ. Kirwan and C.J. Oreila
11.1. The Role of Crystallization in Bioprocesses 249
11.2. Solubility and the Creation of Supersaturation 249
11.2.1. Temperature Effects on Solubility 250
11.2.2. pH Effects on Solubility 250
11.2.3. Reduction of Solubility with Anti-Solvents 251
11.2.4. Effects of Salts on Solubility 252
11.3. Control of Particle Size and Morphology 253
11.3.1. Crystal Growth Kinetics 254
11.3.2. Effects of Additives, Solvents, and Impurities 255
11.3.3. Nucleation and Seeding 256
11.4. The Purity of Biochemicals Produced by Crystallization 258
11.4.1. Solvent Occlusion 258
11.4.2. Incorporation of Solute Impurities 259
11.4.3. Co-Crystallization of Solutes and Polymorphs 260
11.4.4. Improving Purity by Change of Crystal Form 260
11.5. Applications of Crystallization in the Pharmaceutical
Industry 261
11.5.1. The Separation of Optical Isomers 261
11.5.2. Rapid Mixing and Rapid Precipitation 264
11.5.3. Ethanol Fractionation of Plasma Proteins 264
Nomenclature 265
Acknowledgment 266
References 266
CHAPTER 12 CRYSTALLIZATION OF PROTEINS 267
John Wiencek
12.1. Introduction 267
12.2. Protein Chemistry 269
12.2.1. Amino Acids and the Peptide Bond 269
12.2.2. Levels of Structure: Primary, Secondary,
Tertiary, Quaternary 269
12.2.3. Ionizable Sidechains and Protein Net Charge 270
12.2.4. Disulfide Bonds as Crosslinkers within Proteins 270
12.2.5. Chemical Modifications of
Proteins—Glycosolation, Lipidation,
Phosphorylation 270
12.2.6. Effectors 271
12.2.7. Determining Protein Concentration 271
12.2.8. Protein Purity and Homogeniety 272
12.3. Variables Affecting Protein Solubility 274
12.3.1. The Effect of pH on Protein Solubility 274
12.3.2. The Effect of Electrolyte on Protein Solubility 275
12.3.3. The Effect of Anti-Solvents on Protein
Solubility 276
12.3.4. The Effect of Soluble Synthetic Polymers on
Protein Solubility 277
12.3.5. The Effect of Pressure on Protein Solubility 277
12.3.6. The Effect of Temperature on Protein Solubility 277
12.3.7. Case Studies in Lysozyme and the Generic
Protein Phase Diagram 278
12.4. Nucleation and Growth Mechanisms 280
12.5. Physicochemical Measurements 280
12.5.1. Solubility Determination 280
12.5.2. Growth Rate Determination 280
12.6. Traditional Screening Tools 281
12.6.1. Vapor Diffusion Experiments 281
12.6.2. Free Interface Diffusion 282
12.6.3. Dialysis 282
12.6.4. Batch Growth 283
12.6.5. Seeding Techniques 283
x CONTENTS
12.7. Summary 283
Nomenclature 283
Acknowledgment 284
Refercnces 284
CHAPTER 13 CRYSTALLIZATION IN FOODS 287
Richard W. Harlel
13.1. Controlling Crystallization in Foods 287
13.2. Control to Produce Desired Crystalline
Structure 290
13.2.1. Control for Product Quality 290
13.2.2. Control for Separation 292
13.3. Control to Prevent Crystallization 293
13.4. Factors Affecting Control of Crystallization 293
13.4.1. Heat and Mass Transfer Rates 293
13.4.2. Product Formulation 296
13.4.3. Post-Processing Effects 297
13.5. Summary 303
Acknowledgment 303
References 304
INDEX 305
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language | English |
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spelling | Handbook of industrial crystallization ed. by Allan S. Myerson 2. ed. Boston [u.a.] Butterworth-Heinemann 2002 XIII, 313 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Cristalização industrial larpcal Crystallization Industrial applications Verfahrenstechnik (DE-588)4062781-0 gnd rswk-swf Kristallisation (DE-588)4033215-9 gnd rswk-swf Kristallisation (DE-588)4033215-9 s Verfahrenstechnik (DE-588)4062781-0 s DE-604 Myerson, Allan S. Sonstige oth HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009011992&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
spellingShingle | Handbook of industrial crystallization Cristalização industrial larpcal Crystallization Industrial applications Verfahrenstechnik (DE-588)4062781-0 gnd Kristallisation (DE-588)4033215-9 gnd |
subject_GND | (DE-588)4062781-0 (DE-588)4033215-9 |
title | Handbook of industrial crystallization |
title_auth | Handbook of industrial crystallization |
title_exact_search | Handbook of industrial crystallization |
title_full | Handbook of industrial crystallization ed. by Allan S. Myerson |
title_fullStr | Handbook of industrial crystallization ed. by Allan S. Myerson |
title_full_unstemmed | Handbook of industrial crystallization ed. by Allan S. Myerson |
title_short | Handbook of industrial crystallization |
title_sort | handbook of industrial crystallization |
topic | Cristalização industrial larpcal Crystallization Industrial applications Verfahrenstechnik (DE-588)4062781-0 gnd Kristallisation (DE-588)4033215-9 gnd |
topic_facet | Cristalização industrial Crystallization Industrial applications Verfahrenstechnik Kristallisation |
url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009011992&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
work_keys_str_mv | AT myersonallans handbookofindustrialcrystallization |