Principles of analytical chemistry: a textbook
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2000
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XV, 371 S. Ill., graph. Darst. |
| ISBN: | 354064007X |
Internformat
MARC
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| 035 | |a (OCoLC)247449222 | ||
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| 084 | |a CHE 200f |2 stub | ||
| 100 | 1 | |a Valcárcel, Miguel |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Principles of analytical chemistry |b a textbook |c Miguel Valcárcel |
| 264 | 1 | |a Berlin [u.a.] |b Springer |c 2000 | |
| 300 | |a XV, 371 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 4 | |a Analytische Chemie | |
| 650 | 4 | |a Chemistry, Analytic | |
| 650 | 0 | 7 | |a Analytische Chemie |0 (DE-588)4129906-1 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4123623-3 |a Lehrbuch |2 gnd-content | |
| 689 | 0 | 0 | |a Analytische Chemie |0 (DE-588)4129906-1 |D s |
| 689 | 0 | |5 DE-604 | |
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| 999 | |a oai:aleph.bib-bvb.de:BVB01-009007080 | ||
Datensatz im Suchindex
| _version_ | 1804127975513260032 |
|---|---|
| adam_text | 1
INTRODUCTION TO ANALYTICAL CHEMISTRY
. . . . . . . . . . . . . . . . .
1
1.1
ANALYTICAL CHEMISTRY TODAY . . . . . . . . . . . . . . . . . . . . . . .
1
1.2
ANALYTICAL CHEMICAL INFORMATION . . . . . . . . . . . . . . . . . . . .
6
1.3
ANALYTICAL CHEMICAL REFERENCES . . . . . . . . . . . . . . . . . . . .
10
1.4
ESSENTIAL FEATURES OF
ANALYTICAL CHEMISTRY . . . . . . . . . . . . . .
11
1.4.1
BASIC ELEMENTS . . . . . . . . . . . . . . . . . . . . . . . . . .
12
1.4.2
FUNDAMENTALS . . . . . . . . . . . . . . . . . . . . . . . . . . .
13
1.4.3
KEY WORDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
14
1.4.4
DEVELOPMENTS . . . . . . . . . . . . . . . . . . . . . . . . . . .
15
1.4.5
PLACEMENT . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
17
1.4.6
BOUNDARIES . . . . . . . . . . . . . . . . . . . . . . . . . . . .
18
1.5
EVOLUTION OF
ANALYTICAL CHEMISTRY . . . . . . . . . . . . . . . . . . .
19
1.6
CONCEPTUAL AND TECHNICAL HIERARCHIES . . . . . . . . . . . . . . . . .
22
1.7
CLASSIFICATIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. .
28
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
34
S
E
MI
NARS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
36
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . .
37
2
ANALYTICAL PROPERTIES
. . . . . . . . . . . . . . . . . . . . . . . . . . .
3
9
2.
1
INT
RO
DUC
T
I
ON . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
40
2.2
THE CHEMICAL METROLOGICAL HIERARCHY:
UNCERTAINTY AND TRUENESS . .
41
2.3
ERRORS IN ANALYTICAL CHEMISTRY . . . . . . . . . . . . . . . . . . . . .
45
2.4
CAPITAL ANALYTICAL PROPERTIES . . . . . . . . . . . . . . . . . . . . .
.
52
2.4.1
ACCURACY . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
53
2.4.2
REPRESENTATIVENESS . . . . . . . . . . . . . . . . . . . . . . . .
54
2.5
BASIC ANALYTICAL PROPERTIES . . . . . . . . . . . . . . . . . . . . . .
.
56
2.5.1
PRECISION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
57
2.5.2
SENSITIVITY . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
65
2.5.3
SELECTIVITY . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
69
2.6
ACCESSORY ANALYTICAL PROPERTIES . . . . . . . . . . . . . . . . . . . .
72
2.6.1
EXPEDITIOUSNESS . . . . . . . . . . . . . . . . . . . . . . . . . .
73
2.6.2
COST-EFFECTIVENESS . . . . . . . . . . . . . . . . . . . . . . . . .
73
2.6.3
PERSONNEL-RELATED FACTORS . . . . . . . . . . . . . . . . . . . .
75
2.7
RELATIONSHIPS AMONG ANALYTICAL PROPERTIES . . . . . . . . . . . . . .
75
2.7.1
HIERARCHICAL RELATIONSHIPS . . . . . . . . . . . . . . . . . . . .
76
2.7.2
FOUNDATION RELATIONSHIPS . . . . . . . . . . . . . . . . . . . .
77
2.7.3
CONTRADICTORY RELATIONSHIPS . . . . . . . . . . . . . . . . . . .
77
2.7.4
COMPLEMENTARY RELATIONSHIPS . . . . . . . . . . . . . . . . . .
81
TABLE OF CONTENTS
2.8
OTHER ANALYTICAL PROPERTIES . . . . . . . . . . . . . . . . . . . . . .
.
83
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
87
SEMINARS:
NUMERICAL PROBLEMS . . . . . . . . . . . . . . . . . . . . . . .
89
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . .
100
3
TRACEABILITY:
REFERENCE MATERIALS
. . . . . . . . . . . . . . . . . . .
1
0
1
3.
1
INT
RO
DUC
T
I
ON . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
102
3.2
THE INTEGRAL CONCEPT OF
TRACEABILITY . . . . . . . . . . . . . . . . . .
102
3.3
PHYSICAL AND CHEMICAL TRACEABILITY . . . . . . . . . . . . . . . . . . .
105
3.4
TYPES OF
STANDARDS AND THEIR TRACEABILITY . . . . . . . . . . . . . . .
107
3.5
ANALYTICAL CHEMICAL STANDARDS . . . . . . . . . . . . . . . . . . . . .
112
3.5.1
TYPES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
113
3.5.2
GENERAL PROPERTIES . . . . . . . . . . . . . . . . . . . . . . . .
116
3.5.3
PREPARATION AND STORAGE . . . . . . . . . . . . . . . . . . . . .
119
3.5.4
USES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
122
3.5.4.1
CALIBRATION OF
EQUIPMENT AND METHODS . . . . . . . .
123
3.5.4.2
EVALUATION OF
ANALYTICAL PROCESSES . . . . . . . . . . .
128
3.6
SPECIFIC MEANINGS OF
TRACEABILITY . . . . . . . . . . . . . . . . . . .
130
3.6.1
TRACEABILITY OF
AN ANALYTICAL RESULT . . . . . . . . . . . . . . .
130
3.6.2
TRACEABILITY OF
A SAMPLE (ALIQUOT) . . . . . . . . . . . . . . .
132
3.6.3
TRACEABILITY OF
AN INSTRUMENT . . . . . . . . . . . . . . . . . .
134
3.6.4
TRACEABILITY OF
A SAMPLE STANDARD . . . . . . . . . . . . . . . .
134
3.6.5
TRACEABILITY OF
A METHOD . . . . . . . . . . . . . . . . . . . . .
135
3.6.6
RELATIONSHIPS AMONG TRACEABILITY MEANINGS . . . . . . . . . .
135
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
137
S
E
MI
NARS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
.
139
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. .
141
4
THE MEASUREMENT PROCESS IN CHEMISTRY
. . . . . . . . . . . . . . .
1
4
3
4.
1
DEF
I
NI
T
I
ON
OFC
HE
MI
CAL
MEASURE
ME
NT
PRO
CESS . . . . . . . . . . . .
144
4.2 GENERAL STEPS OF
A CHEMICAL MEASUREMENT PROCESS . . . . . . . . .
147
4.3 PRELIMINARY OPERATIONS . . . . . . . . . . . . . . . . . . . . . . .
. .
149
4.3.1
GENERAL FEATURES . . . . . . . . . . . . . . . . . . . . . . . . .
150
4.3.2 SUB-STEPS . . . . . . . . . . . . . . . . . . . . . . . . . . . .
.
154
4.3.3 SAMPLING . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
155
4.3.4 SAMPLE TREATMENT . . . . . . . . . . . . . . . . . . . . . . . .
161
4.4 MEASUREMENT AND TRANSDUCING OF
THE ANALYTICAL SIGNAL . . . . . . .
168
4.5 SIGNAL ACQUISITION AND DATA PROCESSING . . . . . . . . . . . . . . .
.
171
4.6 VALIDATION OF
A CHEMICAL MEASUREMENT PROCESS . . . . . . . . . . . .
173
4.7 SALIENT CURRENT TRENDS . . . . . . . . . . . . . . . . . . . . . . .
. .
174
ANNEX I . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
177
ANNEX II . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
182
ANNEX III . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
186
XII
TABLE OF
CONTENTS
ANNEX IV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
189
ANNEX V . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
190
ANN
EX
VI
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
192
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
194
S
E
MI
NARS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
196
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. .
199
5
QUALITATIVE ASPECTS OF ANALYTICAL CHEMISTRY
. . . . . . . . . . . . .
2
0
1
5.
1
INT
RO
DUC
T
I
ON . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
202
5.2
THE BINARY RESPONSE . . . . . . . . . . . . . . . . . . . . . . . . . .
203
5.2.1
TYPES OF
BINARY RESPONSE . . . . . . . . . . . . . . . . . . . .
204
5.2.2
QUANTITATIVE CONNOTATIONS . . . . . . . . . . . . . . . . . . . .
205
5.2.3
ANALYTICAL FEATURES . . . . . . . . . . . . . . . . . . . . . . . .
208
5.2.4
ERRORS:
FALSE POSITIVES AND FALSE NEGATIVES . . . . . . . . . . .
210
5.3 TYPES OF
QUALITATIVE IDENTIFICATION . . . . . . . . . . . . . . . . . . .
212
5.4 STANDARDS AND CALIBRATION IN QUALITATIVE ANALYSIS . . . . . . . . .
.
214
5.5 CLASSICAL QUALITATIVE ANALYSIS . . . . . . . . . . . . . . . . . . .
. . .
215
5.5.1 GENERAL NOTIONS . . . . . . . . . . . . . . . . . . . . . . . . .
215
5.5.2 TYPES OF
REAGENTS . . . . . . . . . . . . . . . . . . . . . . . .
217
5.5.3 ANALYTICAL SCHEMES . . . . . . . . . . . . . . . . . . . . . . . .
221
5.5.3.1 SCHEMES WITHOUT GROUP SEPARATION . . . . . . . . . .
222
5.5.3.2 SCHEMES WITH GROUP SEPARATION . . . . . . . . . . . .
224
5.6 INSTRUMENTAL QUALITATIVE ANALYSIS . . . . . . . . . . . . . . . . .
. .
229
5.6.1 GENERAL NOTIONS . . . . . . . . . . . . . . . . . . . . . . . . .
229
5.6.2 STATIC SYSTEMS . . . . . . . . . . . . . . . . . . . . . . . . . .
.
232
5.6.3 DYNAMIC SYSTEMS . . . . . . . . . . . . . . . . . . . . . . . . .
235
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
240
S
E
MI
NARS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
242
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. .
244
6
QUANTITATIVE ASPECTS OF ANALYTICAL CHEMISTRY
. . . . . . . . . . . .
2
4
7
6.
1
FUNDAME
NT
AL
S . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
248
6.1.1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . .
.
248
6.1.2 ANALYTICAL PROPERTIES . . . . . . . . . . . . . . . . . . . . . .
.
249
6.1.3 EQUIPMENT AND METHOD CALIBRATION . . . . . . . . . . . . . . .
249
6.1.4 CLASSICAL AND INSTRUMENTAL QUANTITATIVE ANALYSIS . . . . . . .
250
6.1.5 QUANTITATION METHODOLOGIES . . . . . . . . . . . . . . . . . . .
252
6.1.6 EXPRESSING QUANTITATIVE RESULTS . . . . . . . . . . . . . . . . .
253
6.2 CALCULABLE QUANTITATION METHODS . . . . . . . . . . . . . . . . . .
.
256
6.2.1 ABSOLUTE METHODS INVOLVING NO ANALYTICAL STANDARD . . . . .
257
6.2.1.1 GRAVIMETRY . . . . . . . . . . . . . . . . . . . . . . . .
259
6.2.1.2 COULOMETRY . . . . . . . . . . . . . . . . . . . . . . . .
262
6.2.2 ABSOLUTE METHODS INVOLVING ANALYTICAL STANDARDS . . . . . .
263
TABLE OF
CONTENTS
XIII
6.2.2.1 ISOTOPE DILUTION MASS SPECTROMETRY . . . . . . . . . .
263
6.2.2.2 TITRIMETRY . . . . . . . . . . . . . . . . . . . . . . . . .
264
6.3 RELATIVE QUANTITATION METHODS . . . . . . . . . . . . . . . . . . .
. .
271
6.3.1 INTERPOLATION AND EXTRAPOLATION METHODS . . . . . . . . . . .
271
6.3.2 COMPARATIVE METHODS . . . . . . . . . . . . . . . . . . . . . .
275
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
276
S
E
MI
NARS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
278
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. .
281
7
THE ANALYTICAL PROBLEM
. . . . . . . . . . . . . . . . . . . . . . . . . .
2
8
3
7.1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . .
283
7.2 MEANINGS OF
PROBLEM IN ANALYTICAL CHEMISTRY . . . . . . . . . . .
286
7.3 INTEGRAL DEFINITION OF
THE ANALYTICAL PROBLEM . . . . . . . . . . . . .
286
7.4 ELEMENTS OF
THE ANALYTICAL PROBLEM . . . . . . . . . . . . . . . . . .
289
7.5 STEPS OF
THE ANALYTICAL PROBLEM-SOLVING PROCESS . . . . . . . . . . .
290
7.5.1 IDENTIFYING AND CONFIRMING THE INFORMATION REQUIRED . . . .
291
7.5.2 PINPOINTING THE ANALYTICAL INFORMATION REQUIRED . . . . . . .
292
7.5.3 PLANNING THE ANALYTICAL APPROACH . . . . . . . . . . . . . . .
294
7.5.4 MONITORING THE RESULTS . . . . . . . . . . . . . . . . . . . . . .
296
7.5.5 IMPLEMENTING CORRECTIVE ACTIONS . . . . . . . . . . . . . . . .
297
7.6 CONSISTENCY BETWEEN REQUIRED INFORMATION AND SUPPLIED
INFORMATION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
.
297
7.7 THE ANALYTICAL PROBLEM IN THE CONTEXT OF
QUALITY . . . . . . . . . .
299
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
301
S
E
MI
NARS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
.
304
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. .
305
8
ANALYTICAL CHEMISTRY AND QUALITY
. . . . . . . . . . . . . . . . . . .
3
0
7
8.1 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . .
308
8.2 A GENERIC APPROACH TO QUALITY . . . . . . . . . . . . . . . . . . .
. .
310
8.2.1 INTEGRAL DEFINITION OF
QUALITY . . . . . . . . . . . . . . . . . .
310
8.2.2 TYPES OF
QUALITY . . . . . . . . . . . . . . . . . . . . . . . . . .
313
8.2.3 QUALITY COMPROMISES . . . . . . . . . . . . . . . . . . . . . .
314
8.2.4 STRUCTURE OF
QUALITY . . . . . . . . . . . . . . . . . . . . . . . .
315
8.2.5 BENEFITS OF
QUALITY . . . . . . . . . . . . . . . . . . . . . . . .
316
8.3 GENERAL ASPECTS OF
QUALITY IN ANALYTICAL CHEMISTRY . . . . . . . . .
317
8.3.1 TYPES OF
QUALITY IN ANALYTICAL CHEMISTRY . . . . . . . . . . .
317
8.3.2 QUALITY AND ANALYTICAL PROPERTIES . . . . . . . . . . . . . . . .
318
8.3.3 QUALITY AND THE ANALYTICAL PROBLEM . . . . . . . . . . . . . . .
319
8.4 QUALITY SYSTEMS IN THE ANALYTICAL LABORATORY . . . . . . . . . . . .
.
319
8.4.1 ELEMENTS OF
QUALITY ASSURANCE . . . . . . . . . . . . . . . . . .
319
8.4.2 ISO GUIDE 25 (EN-45000) . . . . . . . . . . . . . . . . . . . .
321
8.4.3 GOOD LABORATORY PRACTICES . . . . . . . . . . . . . . . . . . . .
323
XIV
TABLE OF
CONTENTS
8.4.4 SPECIFIC QUALITY SYSTEMS USED IN ANALYTICAL CHEMISTRY . . . .
324
8.5 ANALYTICAL QUALITY CONTROL . . . . . . . . . . . . . . . . . . . . .
. .
326
8.6 ASSESSMENT OF
ANALYTICAL QUALITY . . . . . . . . . . . . . . . . . . . .
327
8.6.1 TYPES OF
ASSESSMENT SYSTEMS . . . . . . . . . . . . . . . . . .
327
8.6.2 LABORATORY ACCREDITATION . . . . . . . . . . . . . . . . . . . . .
330
8.6.3 PROFICIENCY TESTING . . . . . . . . . . . . . . . . . . . . . . .
.
331
8.7 SUPPORTS OF
ANALYTICAL QUALITY ASSURANCE . . . . . . . . . . . . . . .
334
8.8 COSTS AND BENEFITS OF
ANALYTICAL QUALITY SYSTEMS . . . . . . . . . . .
336
QUESTIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . . .
339
S
E
MI
NARS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
341
SUGGESTED READINGS . . . . . . . . . . . . . . . . . . . . . . . . . . .
. . .
341
GLOSSARY OF TERMS
. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .
345
SYMBOLS AND ABBREVIATIONS USED IN THE TEXT
. . . . . . . . . . . . . .
367
TABLE OF
CONTENTS
XV
|
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| dewey-ones | 543 - Analytical chemistry |
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| discipline | Chemie / Pharmazie Chemie |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T18:41:53Z |
| institution | BVB |
| isbn | 354064007X |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-009007080 |
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| spelling | Valcárcel, Miguel Verfasser aut Principles of analytical chemistry a textbook Miguel Valcárcel Berlin [u.a.] Springer 2000 XV, 371 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Analytische Chemie Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Analytische Chemie (DE-588)4129906-1 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=009007080&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Valcárcel, Miguel Principles of analytical chemistry a textbook Analytische Chemie Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4123623-3 |
| title | Principles of analytical chemistry a textbook |
| title_auth | Principles of analytical chemistry a textbook |
| title_exact_search | Principles of analytical chemistry a textbook |
| title_full | Principles of analytical chemistry a textbook Miguel Valcárcel |
| title_fullStr | Principles of analytical chemistry a textbook Miguel Valcárcel |
| title_full_unstemmed | Principles of analytical chemistry a textbook Miguel Valcárcel |
| title_short | Principles of analytical chemistry |
| title_sort | principles of analytical chemistry a textbook |
| title_sub | a textbook |
| topic | Analytische Chemie Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Analytische Chemie Chemistry, Analytic Lehrbuch |
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