Principles and practice of analytical chemistry:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
London [u.a.]
Blackie
1995
|
| Ausgabe: | 4. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XII, 560 S. |
| ISBN: | 0751402265 |
Internformat
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Datensatz im Suchindex
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| adam_text | PRINCIPLES AND PRACTICE OF ANALYTICAL CHEMISTRY FOURTH EDITION F. W.
FIFIELD AND D. KEALEY KINGSTON UNIVERSITY M BLACKIE ACADEMIC &
PROFESSIONAL AN IMPRINT OF CHAPMAN & HALL LONDON * GLASGOW * WEINHEIM *
NEW YORK * TOKYO * MELBOURNE * MADRAS CONTENTS PREFACE IX
ACKNOWLEDGEMENTS XI CHAPTER 1 INTRODUCTION L THE SCOPE OF ANALYTICAL
CHEMISTRY. THE FUNCTION OF ANALY TICAL CHEMISTRY. ANALYTICAL PROBLEMS
AND THEIR SOLUTION. THE NATURE OF ANALYTICAL METHODS. TRENDS IN
ANALYTICAL METHODS AND PROCEDURES. GLOSSARY OF TERMS. CHAPTER 2 THE
ASSESSMENT OF ANALYTICAL DATA 14 2.1 DEFINITIONSANDBASICCONCEPTS 14 2.2
THE NATURE AND ORIGINOFERRORS 16 2.3 THE EVALUATION OF RESULTS AND
METHODS 18 THE RELIABILITY OF MEASUREMENTS. THE ANALYSIS OF DATA. THE
APPLICATION OF STATISTICAL TESTS. LIMITS OF DETECTION. QUALITY CONTROL
CHARTS. STANDARDIZATION OF ANALYTICAL METHODS. CHEMOMETRICS. CHAPTER 3
PH, COMPLEXATION AND SOLUBILITY EQUELIBRIA 37 3.1 CHEMICAL REACTIONS IN
SOLUTION 38 EQUILIBRIUM CONSTANTS. KINETIC FACTORS IN EQUILIBRIA. 3.2
SOLVENTSIN ANALYTICAL CHEMISTRY 42 IONIZING SOLVENTS. NON-IONIZING
SOLVENTS. 3.3 ACID-BASE EQUILIBRIA 43 WEAK ACID AND WEAK BASE
EQUILIBRIA. BUFFERS AND PH CONTROL. THE PH OF SAH SOLUTIONS. 3.4
COMPLEXATION EQUILIBRIA 50 THE FORMATION OF COMPLEXES IN SOLUTION. THE
CHELATE EFFECT. 3.5 SOLUBILITY EQUILIBRIA 53 SOLUBILITY PRODUCTS.
CHAPTER 4 SEPARATION TECHNIQUES 55 4.1 SOLVENT EXTRACTION 56 EFFICIENCY
OF EXTRACTION. SELECTIVITY OF EXTRACTION. EXTRACTION SYSTEMS. EXTRACTION
OF UNCHARGED METAL CHELATES. METHODS OF EXTRACTION. APPLICATIONS OF
SOLVENT EXTRACTION. 4.2 CHROMATOGRAPHY 75 4.2.1 GAS CHROMATOGRAPHY.
4.2.2 HIGH PERFORMANCE LIQUID CHROMA- TOGRAPHY. 4.2.3 SUPERCRITICAL
FLUID CHROMATOGRAPHY. 4.2.4 THIN-LAYER CHROMATOGRAPHY. 4.2.5
ION-EXCHANGE ^CHROMATOGRAPHY. 4.2.6 GEL- PERMEATION CHROMATOGRAPHY. V
VI CONTENTS 4.3 ELECTROPHORESIS 164 FACTORS AFFECTING IONIC MIGRATION.
EFFECT OF TEMPERATURE, PH AND IONIC STRENGTH. ELECTROOSMOSIS. SUPPORTING
MEDIUM. DETECTION OF SEPARATED COMPONENTS. APPLICATIONS OF TRADIONAL
ZONE ELECTROPHORESIS. HIGH PER- FORMANCE CAPILLARY ELECTROPHORESIS.
CHAPTER5 TITRIMETRYANDGRAVIMETRY 184 5.1 TITRIMETRY 184 DEFINITIONS.
TITRIMETRIC REACTIONS. ACID-BASE TITRATIONS. APPLICATIONS OF ACID-BASE
TITRATIONS. REDOX TITRATIONS. APPLICATIONS OF REDOX TITRATIONS.
COMPLEXOMETRIC TITRATIONS. EDTA. APPLICATIONS OF EDTA TITRATIONS.
TITRATIONS WITH COMPLEXING AGENTS OTHER THAN EDTA. PRECIPITATION
TITRATIONS. 5.2 GRAVIMETRY 211 PRECIPITATION REACTIONS. PRACTICAL
GRAVIMETRIC PROCEDURES. APPLICATIONS OF GRAVIMETRY. CHAPTER6
ELECTROCHEMICALTECHNIQUES 223 6.1 POTENTIOMETRY 227 ELECTRODE SYSTEMS.
DIRECT POTENTIOMETRIE MEASUREMENTS. POTENTIO- METRIE TITRATIONS.
NULL-POINT POTENTIOMETRY. APPLICATIONS OF POTENTIO- METRY. 6.2
POLAROGRAPHY, STRIPPING VOLTAMMETRY AND AMPEROMETRIC TECHNIQUES 243
DIFFUSION CURRENTS. HALF-WAVE POTENTIALS. CHARACTERISTICS OF THE DME.
QUANTITATIVE ANALYSIS. MODES OF OPERATION USED IN POLAROGRAPHY. THE
DISSOLVED OXYGEN ELECTRODE AND BIOCHEMICAL ENZYME SENSORS. AMPEROMETRIC
TITRATIONS. APPLICATIONS OF POLAROGRAPHY AND AMPERO- METRIC TITRATIONS.
6.3 ELECTROGRAVIMETRY AND COULOMETRY 257 COULOMETRY. COULOMETRY AT
CONSTANT POTENTIAL. COULOMETRIC TITRATIONS. APPLICATIONS OF COULOMETRIC
TITRATIONS. 6.4 CONDUCTOMETRIC TITRATIONS 261 IONIC CONDUETANCES.
CHAPTER7 ANINTRODUCTIONTOANALYTICAL SPECTROMETRY 267 ELECTROMAGNETIC
RADIATION. ATOMIC AND MOLECULAR ENERGY. THE ABSORPTION AND EMISSION OF
ELECTROMAGNETIC RADIATION. THE COMPLEXITY OF SPECTRA AND THE INTENSITY
OF SPECTRAL LINES. ANALYTICAL SPECTROMETRY. INSTRUMENTATION. CHAPTER8
ATOMIC SPECTROMETRY 282 8.1 ARC/SPARK ATOMIC (OPTICAL) EMISSION
SPECTROMETRY 287 INSTRUMENTATION. SAMPLE PREPARATION. QUALITATIVE AND
QUANTITATIVE ANALYSIS. INTERFERENCES AND ERRORS ASSOCIATED WITH THE
EXCITATION PROCESS. APPLICATIONS OF ARC/SPARK EMISSION SPECTROMETRY. 8.2
GLOW DISCHARGE ATOMIC EMISSION SPECTROMETRY 294 INSTRUMENTATION.
APPLICATIONS. CONTENTS VLL 8.3 PLASMA EMISSION SPECTROMETRY 296
INSTRUMENTATION. SAMPLE INTRODUCTION FOR PLASMA SOURCES. ANALYTICAL
MEASUREMENTS. APPLICATIONS OF PLASMA EMISSION SPECTROMETRY. 8.4
INDUCTIVELY COUPLED PLASMA-MASS SPECTROMETRY (ICP-MS) 304 PRINCIPLES.
INSTRUMENTATION. APPLICATIONS. 8.5 FLAME EMISSION SPECTROMETRY 308
INSTRUMENTATION. FLAME CHARACTERISTICS. FLAME PROCESSES. EMISSION
SPECTRA. QUANTITATIVE MEASUREMENTS AND INTERFERENCES. APPLICATIONS OF
FLAME PHOTOMETRY AND FLAME ATOMIC EMISSION SPECTROMETRY. 8.6 ATOMIC
ABSORPTION SPECTROMETRY 317 ABSORPTION OF CHARACTERISTIC RADIATION.
INSTRUMENTATION. SAMPLE VAPORIZATION. QUANTITATIVE MEASUREMENTS AND
INTERFERENCES. ATOMIC FLUORESCENCE SPECTROMETRY. 8.7 X-RAY EMISSION
SPECTROMETRY 331 X-RAY PROCESSES. INSTRUMENTATION. APPLICATIONS OF X-RAY
EMISSION SPECTROMETRY. CHAPTER 9 MOLECULAR SPECTROMETRY 35 1 9.1 VISIBLE
AND ULTRAVIOLET SPECTROMETRY 361 POLYATOMIC ORGANIC MOLECULES. METAL
COMPLEXES. QUALITATIVE ANALYSIS - THE IDENTIFICATION OF STRUCTURAL
FEATURES. QUANTITATIVE ANALYSIS - ABSORPTIOMETRY. CHOICE OF COLORIMETRIC
AND SPECTROPHOTOMETRIC PROCEDURES. FLUORIMETRY. APPLICATIONS OF
UV/VISIBLE SPECTROMETRY AND FLUORIMETRY. 9.2 INFRARED SPECTROMETRY 377
DIATOMIC MOLECULES. POLYATOMIC MOLECULES. CHARACTERISTIC VIBRATION
FREQUENCIES. FACTORS AFFECTING GROUP FREQUENCIES. QUALITATIVE ANALYSIS -
THE IDENTIFICATION OF STRUCTURAL FEATURES. QUANTITATIVE ANALYSIS.
SAMPLING PROCEDURES. APPLICATIONS OF INFRARED SPECTROMETRY. 9.3 NUCLEAR
MAGNETIC RESONANCE SPECTROMETRY (NMR) 393 INSTRUMENTATION. THE NMR
PROCESS. CHEMICAL SHIFT. SPIN-SPIN COUPLING. CARBON-13 NMR. PULSED
FOURIER TRANSFORM NMR (FT-NMR). QUANTITATIVE ANALYSIS - THE
IDENTIFICATION OF STRUCTURAL FEATURES. QUANTITATIVE ANALYSIS.
APPLICATIONS OF NMR SPECTROMETRY. 9.4 MASS SPECTROMETRY 425
INSTRUMENTATION. PRINCIPLE OF MASS SPECTROMETRY. CHARACTERISTICS AND
INTERPRETATION OF MOLECULAR MASS SPECTRA. APPLICATIONS OF MASS SPECTRO-
METRY. 9.5 SPECTROMETRIC IDENTIFICATION OF ORGANIC COMPOUNDS 436 CHAPTER
10 RADIOCHEMICAL METHODS IN ANALYSIS 447 10.1 NUCLEAR STRUCTURE AND
NUCLEAR REACTIONS 448 DECAY REACTIONS. THE KINETICS OF DECAY REACTIONS.
BOMBARDMENT REACTIONS AND THE GROWTH OF RADIOACTIVITY. 10.2
INSTRUMENTATION AND MEASUREMENT OF RADIOACTIVITY 455 RADIATION
DETECTORS. SOME IMPORTANT ELECTRONIC CIRCUITS. THE STATISTICS OF
RADIOACTIVE MEASUREMENTS. VU1 CONTENTS 10.3 ANALYTICAL USES OF
RADIONUCLEIDES 465 CHEMICAL PATHWAY STUDIES. RADIOISOTOPE DILUTION
METHODS. RADIO- IMMUNOASSAY. RADIOACTIVATION ANALYSIS. ENVIRONMENTAL
MONITORING. CHAPTER 11 THERMAL TECHNIQUES 475 11.1 THERMOGRAVIMETRY 477
INSTRUMENTATION. APPLICATIONS OF TG.. 11.2 DIFFERENTIAL THERMAL ANALYSIS
(DTA) 482 INSTRUMENTATION. APPLICATIONS OF DTA 11.3 DIFFERENTIAL
SCANNING CALORIMETRY (DSC) 489 INSTRUMENTATION. APPLICATIONS OF DSC. DTA
AND DSC. 11.4 THERMOMECHANICAL ANALYSIS (TMA) AND DYNAMIC MECHANICAL
ANALYSIS (DMA) 493 INSTRUMENTATION. APPLICATIONS OF TMA. DYNAMIC
MECHANICAL ANALYSIS. 11.5 PYROLYSIS-GASCHROMATOGRAPHY 497
INSTRUMENTATION. CHAPTER 12 OVERALL ANALYTICAL PROCEDURES AND THEIR
AUTOMATION 504 12.1 SAMPLING AND SAMPLE PRETREATMENT 504 REPRESENTATIVE
SAMPLES AND SAMPLE STORAGE. SAMPLE CONCENTRATION AND CLEAN-UP: SOLID
PHASE EXTRACTION. 12.2 EXAMPLES OF ANALYTICAL PROBLEMS AND PROCEDURES
509 1: EVALUATION OF METHODS FOR THE DETERMINATION OF FLUORIDE IN WATER
SAMPLES. 2: ANALYSIS OF A COMPETITIVE PRODUCT. 3: THE ASSESSMENT OF THE
HEAVY METAL POLLUTION IN A RIVER ESTUARY. 4: THE ANALYSIS OF HYDROCARBON
PRODUCTS IN A CATALYTIC REFORMING STUDY. 12.3 THE AUTOMATIONOF
ANALYTICAL PROCEDURES. 519 THE AUTOMATION OF REPETITIVE ANALYSIS.
CONSTANT MONITORING AND ON LINE ANALYSIS. LABORATORY ROBOTICS. CHAPTER
13 THE ROLE OF COMPUTERS AND MICRO- PROCESSORS IN ANALYTICAL CHEMISTRY
528 13.1 INTRODUCTION 528 INSTRUMENT OPTIMIZATION. DATA RECORDING AND
STORAGE. DATA PROCESSING AND DATA ANALYSIS (CHEMOMETRICS). LABORATORY
MANAGEMENT. EXPERT SYSTEMS. 13.2 COMPUTERS AND MICROPROCESSORS 534 MINI-
AND MICROCOMPUTERS. MICROPROCESSORS. 13.3 INSTRUMENT-COMPUTER INTERFACES
537 13.4 THE SCOPE OF MICROPROCESSOR CONTROL AND COMPUTERS IN ANALYTICAL
LABORATORIES 542 1. A MICROPROCESSOR-CONTROLLED POTENTIOMETRIE TITRATOR.
2. AN INFRARED SPECTROMETER INTERFACED TO A DEDICATED MICROCOMPUTER. 3.
A COMPUTING INTEGRATOR FOR CHROMATOGRAPHIE ANALYSIS. 4. A
MICROPROCESSOR-BASED X-RAY OR -Y-RAY SPECTROMETER. INDEX 551
|
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| discipline | Chemie / Pharmazie Chemie |
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| isbn | 0751402265 |
| language | English |
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| spelling | Fifield, Frederick William Verfasser aut Principles and practice of analytical chemistry F. W. Fifield and D. Kealey 4. ed. London [u.a.] Blackie 1995 XII, 560 S. txt rdacontent n rdamedia nc rdacarrier Chimie analytique ram Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s DE-604 Kealey, David Verfasser aut GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008757544&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Fifield, Frederick William Kealey, David Principles and practice of analytical chemistry Chimie analytique ram Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4129906-1 |
| title | Principles and practice of analytical chemistry |
| title_auth | Principles and practice of analytical chemistry |
| title_exact_search | Principles and practice of analytical chemistry |
| title_full | Principles and practice of analytical chemistry F. W. Fifield and D. Kealey |
| title_fullStr | Principles and practice of analytical chemistry F. W. Fifield and D. Kealey |
| title_full_unstemmed | Principles and practice of analytical chemistry F. W. Fifield and D. Kealey |
| title_short | Principles and practice of analytical chemistry |
| title_sort | principles and practice of analytical chemistry |
| topic | Chimie analytique ram Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Chimie analytique Chemistry, Analytic Analytische Chemie |
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