Hydride generation atomic absorption spectrometry:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
1995
|
| Schriftenreihe: | Chemical analysis
130 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVIII, 526 S. |
| ISBN: | 0471953644 |
Internformat
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Datensatz im Suchindex
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|---|---|
| adam_text | HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY JIRI DEDINA ACADEMY OF
SCIENCES OF THE CZECH REPUBLIC INSTITUTE OF ANALYTICAL CHEMISTRY
LABORATORY OF TRACE ELEMENT ANALYSIS VIDEIISKAE 1083 142 20 PRAGUE 4
CZECH REPUBLIC DIMITER L. TSALEV FACULTY OF CHEMISTRY UNIVERSITY OF
SOFIA SOFIA 1126 BULGARIA JOHN WILEY & SONS CHICHESTER / NEW YORK /
BRISBANE / TORONTO / SINGAPORE CONTENTS PREFACE XI LIST OF SYMBOLS AND
ABBREVIATIONS XUEI PART I FUNDAMENTALS AND GENERAL APPROACHES CHAPTER 1
THEORY 3 1.1 BASIC DEFINITIONS 3 1.2 DEPENDENCE OF FREE ATOM
DISTRIBUTION IN TUBULAER ATOMIZERS ON GENERATOR OUTLET FUNCTIONS * 5
1.2.1 WELL-STIRRED TANK MODEL 6 1.2.2 PLUG FLOW MODEL 7 1.2.3 COMMON
FEATURES OF WELL-STIRRED TANK AND PLUG FLOW MODELS 9 1.2.4 LAMINAR FLOW
MODEL 9 1.2.5 DIFFUSION COEFFICIENTS 10 1.3 DEPENDENCE OF ABSORBANCE ON
THE FREE ATOM DISTRIBUTION IN TUBULAER ATOMIZERS 13 CHAPTER 2 HYDRIDE
GENERATION 17 2.1 HYDRIDE RELEASE 18 2.2 HYDRIDE TRANSPORT 25 2.3
METHODS OF HYDRIDE GENERATION 27 2.4 CONTINUOUS FLOW AND FLOW
INJECTION*OUTLET GENERATOR FUNCTIONS 29 2.5 CONTINUOUS FLOW AND FLOW
INJECTION*EXPERIMENTAL APPROACHES 33 2.6 BATCH MODE 39 2.7 COLLECTION IN
ABSORBING MEDIA 43 2.8 PRESSURE COLLECTION 44 2.9 CRYOGENIC TRAPPING 44
2.10 ELECTROCHEMICAL HYDRIDE GENERATION 48 2.11 COMPARISON OF
SENSITIVITY FOR INDIVIDUAL HYDRIDE GENERATION METHODS - 49 CHAPTER 3
HYDRIDE ATOMIZATION 51 3.1 CHEMICAL EQUILIBRIA IN HYDRIDE ATOMIZERS 51
3.2 INERT GAS-HYDROGEN DIFFUSION FLAMES 54 3.3 GRAPHITE FURNACES 56
3.3.1 IN-SITU TRAPPING 56 3.3.2 ON-LINE ATOMIZATION 58 VI CONTENTS 3.4
QUARTZ-TUBE ATOMIZERS 62 3.4.1 DESIGN 63 3.4.2 MECHANISM OF HYDRIDE
ATOMIZATION IN FLAME-IN-TUBE ATOMIZERS 68 3.4.3 MECHANISM OF HYDRIDE
ATOMIZATION IN EXTERNALLY HEATED QUARTZ TUBES 70 3.4.4 FATE OF FREE
ANALYTE ATOMS IN QUARTZ-TUBE ATOMIZERS 74 3.4.5 DESCRIPTION OF ANALYTE
TRANSFER IN THE HORIZONTAL BAR-TUBE OF UNHEATED FLAME-IN-TUBE ATOMIZERS
77 3.4.6 INFLUENCE OF EXTERNAL HEATING 83 3.4.7 INFLUENCE OF ATOMIZATION
PARAMETERS ON THE SENSITIVITY OF QUARTZ-TUBE ATOMIZERS 85 3.4.8
THERMOCHEMICAL HYDRIDE GENERATION 89 CHAPTER 4 INTERFERENCES 91 4.1
INFLUENCE OF NONSPECTRAL INTERFERENCES ON THE SIGNAL SHAPE 94 4.2 LIQUID
PHASE INTERFERENCES 96 4.2.1 CATEGORIZATION OF MATRIX INTERFERENCES 96
4.2.2 INTERFERENCES OF STRONG OXIDANTS 98 4.2.3 INTERFERENCES OF
TRANSITION AND NOBLE METALS 98 4.2.4 INTERFERENCES OF OTHER SPECIES 102
4.2.5 CONTROL OF MATRIX INTERFERENCES 102 4.3 TRANSPORT INTERFERENCES
105 4.4 INTERFERENCES IN THE ATOMIZER 106 4.4.1 DIFFUSION FLAMES 107
4.4.2 IN-SITU TRAPPING IN GRAPHITE FURNACES 109 4.4.3 ON-LINE
ATOMIZATION IN GRAPHITE FURNACES 110 4.4.4 FLAME-IN-TUBE ATOMIZERS 111
4.4.5 EXTERNALLY HEATED QUARTZ TUBES 115 118 118 119 119 120 121 121
CHAPTER 5.1 5.2 5.3 5.4 5 GENERAL ASSESSMENT OF HYDRIDE GENERATION AND
ATOMIZATION METHODS ACCURACY SENSITIVITY 5.2.1 MICROANALYSIS 5.2.2 TRACE
ANALYSIS OTHER CRITERIA CONCLUSION CHAPTER 6 OTHER VOLATILE COMPOUNDS
123 6.1 CHELATES 123 6.2 ALKYLS 126 CONTENTS VLL 6.3 CARBONYLS 127 6.4
OXIDES AND HALIDES 128 APPENDIX TO PART I ATOMIC ABSORPTION COEFFICIENT
129 LINE SHAPES 130 DOPPLER BROADENING 133 LORENTZ BROADENING 134
COMBINATION OF LORENTZ AND DOPPLER BROADENING 136 SELF-ABSORPTION 137
HYPERFINE SPLITTING 137 ASSESSMENT OF THE MAGNITUDE OF THE ATOMIC
ABSORPTION COEFFICIENT 139 ATOMIC ABSORPTION COEFFICIENT OF THE SELENIUM
196 NM LINE 142 ATOMIC ABSORPTION COEFFICIENT OF THE ARSENIC 193.7 NM
LINE 146 PART II METHODOLOGY AND ANALYTICAL APPLICATIONS CHAPTER 7
ANTIMONY 151 7.1 GENERAL CHARACTERISTICS 151 7.2 OPTIMIZATION OF
INSTRUMENTAL AND CHEMICAL PARAMETERS 152 7.3 CONTROL OF INTERFERENCES
159 7.4 PRECONCENTRATION AND SEPARATION TECHNIQUES 164 7.5 SPECIATION
STUDIES 169 7.6 ANALYSIS OF REAL SAMPLES 172 7.6.1 ENVIRONMENTAL SAMPLES
172 7.6.2 AGRICULTURAL SAMPLES 175 7.6.3 FOOD AND BEVERAGES 178 7.6.4
BIOLOGICAL AND CLINICAL SAMPLES 178 7.6.5 GEOCHEMICAL SAMPLES 179 7.6.6
METALLURGICAL AND INDUSTRIAL SAMPLES 180 CHAPTER 8 ARSENIC 182 8.1
GENERAL CHARACTERISTICS 182 8.2 OPTIMIZATION OF INSTRUMENTAL AND
CHEMICAL PARAMETERS 184 8.3 CONTROL OF INTERFERENCES 193 8.3.1 GENERAL
CHARACTERISTICS OF INTERFERENCES 193 8.3.2 APPROACHES TO INTERFERENCE
CONTROL 195 8.3.3 MASKING ADDITIVES AND BUFFERS 199 8.4 PRECONCENTRATION
AND SEPARATION TECHNIQUES 203 8.5 SPECIATION STUDIES 212 8.6 ANALYSIS OF
REAL SAMPLES 222 8.6.1 ENVIRONMENTAL SAMPLES 223 8.6.2 AGRICULTURAL
SAMPLES 227 8.6.3 FOOD AND BEVERAGES 229 8.6.4 BIOLOGICAL AND CLINICAL
SAMPLES 232 VLLL CONTENTS 8.6.5 GEOCHEMICAL SAMPLES 237 8.6.6
METALLURGICAL AND INDUSTRIAL SAMPLES 241 CHAPTER 9 BISMUTH 246 9.1
GENERAL CHARACTERISTICS 246 9.2 OPTIMIZATION OF INSTRUMENTAL AND
CHEMICAL PARAMETERS 247 9.3 CONTROL OF INTERFERENCES 251 9.4
PRECONCENTRATION AND SEPARATION TECHNIQUES 255 9.5 SPECIATION STUDIES
259 9.6 ANALYSIS OF REAL SAMPLES 260 9.6.1 ENVIRONMENTAL SAMPLES 260
9.6.2 AGRICULTURAL SAMPLES 261 9.6.3 FOOD AND BEVERAGES 261 9.6.4
BIOLOGICAL AND CLINICAL SAMPLES 261 9.6.5 GEOCHEMICAL SAMPLES 262 9.6.6
METALLURGICAL AND INDUSTRIAL SAMPLES 263 CHAPTER 10 GERMANIUM 267 10.1
GENERAL CHARACTERISTICS 267 10.2 OPTIMIZATION OF INSTRUMENTAL AND
CHEMICAL PARAMETERS 268 10.3 CONTROL OF INTERFERENCES 272 10.4
PRECONCENTRATION AND SEPARATION TECHNIQUES 275 10.5 SPECIATION STUDIES
278 10.6 ANALYSIS OF REAL SAMPLES 279 10.6.1 ENVIRONMENTAL SAMPLES 279
10.6.2 AGRICULTURAL SAMPLES 280 10.6.3 FOOD 282 10.6.4 BIOLOGICAL AND
CLINICAL SAMPLES 282 10.6.5 GEOCHEMICAL SAMPLES 282 10.6.6 METALLURGICAL
AND INDUSTRIAL SAMPLES 283 CHAPTER 11 INDIUM 285 11.1 GENERAL
CHARACTERISTICS 285 11.2 OPTIMIZATION OF INSTRUMENTAL AND CHEMICAL
PARAMETERS 286 CHAPTER 12 LEAD 288 12.1 GENERAL CHARACTERISTICS 288 12.2
OPTIMIZATION OF INSTRUMENTAL AND CHEMICAL PARAMETERS 290 12.3 REACTION
MEDIA AND CONTROL OF INTERFERENCES 293 12.4 PRECONCENTRATION AND
SEPARATION TECHNIQUES 297 12.5 SPECIATION STUDIES 301 CONTENTS IX 12.6
ANALYSIS OF REAL SAMPLES 303 12.6.1 ENVIRONMENTAL SAMPLES 303 12.6.2
AGRICULTURAL SAMPLES 304 12.6.3 FOOD AND BEVERAGES 305 12.6.4 BIOLOGICAL
AND CLINICAL SAMPLES 306 12.6.5 GEOCHEMICAL SAMPLES 307 12.6.6
METALLURGICAL AND INDUSTRIAL SAMPLES 307 CHAPTER 13 SELENIUM 308 13.1
GENERAL CHARACTERISTICS 308 13.2 OPTIMIZATION OF INSTRUMENTAL AND
CHEMICAL PARAMETERS 310 13.3 CONTROL OF INTERFERENCES 318 13.3.1 GENERAL
CHARACTERISTICS OF INTERFERENCES 318 13.3.2 APPROACHES TO INTERFERENCE
CONTROL 321 13.3.3 MASKING ADDITIVES AND BUFFERS 323 13.4
PRECONCENTRATION AND SEPARATION TECHNIQUES 326 13.5 SPECIATION STUDIES
333 13.6 ANALYSIS OF REAL SAMPLES 339 13.6.1 ENVIRONMENTAL SAMPLES 339
13.6.2 AGRICULTURAL SAMPLES 343 13.6.3 FOOD AND BEVERAGES 344 13.6.4
BIOLOGICAL AND CLINICAL SAMPLES 345 13.6.5 GEOCHEMICAL SAMPLES 349
13.6.6 METALLURGICAL AND INDUSTRIAL SAMPLES 350 CHAPTER 14 TELLURIUM 355
14.1 GENERAL CHARACTERISTICS 355 14.2 OPTIMIZATION OF INSTRUMENTAL AND
CHEMICAL PARAMETERS 355 14.3 CONTROL OF INTERFERENCES 358 14.4
PRECONCENTRATION AND SEPARATION TECHNIQUES 359 14.5 SPECIATION STUDIES
364 14.6 ANALYSIS OF REAL SAMPLES 365 14.6.1 ENVIRONMENTAL SAMPLES 365
14.6.2 AGRICULTURAL SAMPLES 367 14.6.3 FOOD 367 14.6.4 BIOLOGICAL AND
CLINICAL SAMPLES 368 14.6.5 GEOCHEMICAL SAMPLES 368 14.6.6 METALLURGICAL
AND INDUSTRIAL SAMPLES 368 CHAPTER 15 THALLIUM 371 CHAPTER 16 TIN 372
16.1 GENERAL CHARACTERISTICS 372 16.2 OPTIMIZATION OF INSTRUMENTAL AND
CHEMICAL PARAMETERS 373 X CONTENTS 16.3 CONTROL OF INTERFERENCES 378
16.4 PRECONCENTRATION AND SEPARATION TECHNIQUES 380 16.5 SPECIATION
STUDIES 384 16.6 ANALYSIS OF REAL SAMPLES 389 16.6.1 ENVIRONMENTAL
SAMPLES 389 16.6.2 AGRICULTURAL SAMPLES 392 16.6.3 FOOD AND BEVERAGES
393 16.6.4 BIOLOGICAL AND CLINICAL SAMPLES 393 16.6.5 GEOCHEMICAL
SAMPLES 394 16.6.6 METALLURGICAL AND INDUSTRIAL SAMPLES 395 APPENDICES:
INDEXES TO THE BIBLIOGRAPHY 397 APPENDIX 1 TECHNIQUE AND ANALYTE ELEMENT
399 APPENDIX 2 SPECIATION 409 APPENDIX 3 SAMPLE MATRIX: HGAAS
APPLICATIONS 411 APPENDIX 4 SAMPLE MATRIX: PROCEDURES OTHER THAN HGAAS
420 APPENDIX 5 OTHER KEYWORDS 425 BIBLIOGRAPHY 430 INDEX 513
|
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| illustrated | Not Illustrated |
| indexdate | 2024-07-09T18:35:09Z |
| institution | BVB |
| isbn | 0471953644 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008757348 |
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| physical | XVIII, 526 S. |
| publishDate | 1995 |
| publishDateSearch | 1995 |
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| publisher | Wiley |
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| series | Chemical analysis |
| series2 | Chemical analysis |
| spelling | Dědina, Jiří Verfasser aut Hydride generation atomic absorption spectrometry Jiří Dědina ; Dimiter L. Tsalev Chichester [u.a.] Wiley 1995 XVIII, 526 S. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 130 Atomic absorption spectroscopy Hydrides Atomabsorptionsspektroskopie (DE-588)4068917-7 gnd rswk-swf Atomabsorptionsspektroskopie (DE-588)4068917-7 s DE-604 Calev, Dimiter L. Verfasser (DE-588)1031493255 aut Chemical analysis 130 (DE-604)BV000008780 130 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008757348&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Dědina, Jiří Calev, Dimiter L. Hydride generation atomic absorption spectrometry Chemical analysis Atomic absorption spectroscopy Hydrides Atomabsorptionsspektroskopie (DE-588)4068917-7 gnd |
| subject_GND | (DE-588)4068917-7 |
| title | Hydride generation atomic absorption spectrometry |
| title_auth | Hydride generation atomic absorption spectrometry |
| title_exact_search | Hydride generation atomic absorption spectrometry |
| title_full | Hydride generation atomic absorption spectrometry Jiří Dědina ; Dimiter L. Tsalev |
| title_fullStr | Hydride generation atomic absorption spectrometry Jiří Dědina ; Dimiter L. Tsalev |
| title_full_unstemmed | Hydride generation atomic absorption spectrometry Jiří Dědina ; Dimiter L. Tsalev |
| title_short | Hydride generation atomic absorption spectrometry |
| title_sort | hydride generation atomic absorption spectrometry |
| topic | Atomic absorption spectroscopy Hydrides Atomabsorptionsspektroskopie (DE-588)4068917-7 gnd |
| topic_facet | Atomic absorption spectroscopy Hydrides Atomabsorptionsspektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008757348&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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