Process analytical chemistry: control, optimization, quality, economy
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
Berlin [u.a.]
Springer
1999
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben. - Dt. Ausg. u.d.T.: Koch, Karl Heinz: Industrielle Prozessanalytik |
| Beschreibung: | XI, 239 S. graph. Darst. |
| ISBN: | 3540653376 |
Internformat
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| 100 | 1 | |a Koch, Karl Heinz |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Process analytical chemistry |b control, optimization, quality, economy |c Karl Heinz Koch |
| 264 | 1 | |a Berlin [u.a.] |b Springer |c 1999 | |
| 300 | |a XI, 239 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Literaturangaben. - Dt. Ausg. u.d.T.: Koch, Karl Heinz: Industrielle Prozessanalytik | ||
| 650 | 4 | |a Chemical process control | |
| 650 | 4 | |a Chemistry, Analytic | |
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Datensatz im Suchindex
| _version_ | 1807504948509802496 |
|---|---|
| adam_text |
TABLE
OF
CONTENTS
1
INTRODUCTION
.
I
1.1
FIELDS
OF
APPLICATION
OF
INDUSTRIAL
ANALYTICS
.
I
1.2
ON
THE
HISTORY
OF
PROCESS
ANALYTICAL
CHEMISTRY
.
7
1.3
ECONOMIC
IMPORTANCE
OF
PROCESS
ANALYTICAL
CHEMISTRY
.
10
1.4
PRESENTATION
AND
ORGANIZATIONAL
FORMS
OF
PROCESS
ANALYTICAL
CHEMISTRY
.
11
1.5
IMPORTANCE
OF
SAMPLING
.
12
REFERENCES
.
15
2
PROCESS
ANALYTICS
OF
GASES
.
17
2.1
IMPORTANCE
FOR
INDUSTRY
AND
SOCIETY
.
17
2.2
SAMPLING
OF
GASES
.
19
2.3
ANALYSIS
OF
GASES
.
21
2.3.1
MEASUREMENT
OF
PHYSICAL
EFFECTS
.
21
2.3.1.1
PARAMAGNETISM
.
21
2.3.1.2
HEAT
CONDUCTIVITY
.
22
2.3.1.3
HEAT
CHANGE
.
23
2.3.1.4
REACTIONS
ON
SEMICONDUCTOR
SURFACES
.
25
2.3.2
SPECTROSCOPIC
METHODS
.
26
2.3.2.1
UV,
VIS
AND
IR
SPECTROSCOPY
.
*
.
26
2.3.2.2
MASS
SPECTROMETRY
.
31
2.3.2.3
CHEMILUMINESCENCE
.
32
2.3.3
ELECTROMETRIC
METHODS
.
33
2.3.4
GAS
CHROMATOGRAPHY
.
36
2.4
SUPPLIERS
FOR
GAS
ANALYZERS
AND
GAS
SENSORS
.
37
2.4.1
PARAMAGNETIC
GAS
ANALYZERS
.
37
2.4.2
HEAT
CONDUCTIVITY
MEASURING
EQUIPMENT
.
38
2.4.3
GAS
SENSORS
BASED
ON
HEAT
OF
REACTION
.
38
2.4.4
SEMICONDUCTOR
SENSORS
.
38
2.4.5
UV-/VIS-/NIR
PROCESS
PHOTOMETERS
.
38
2.4.6
IR
PROCESS
PHOTOMETERS
.
39
2.4.7
MASS
SPECTROMETRIC
GAS
ANALYZERS
.
39
2.4.8
CHEMILUMINESCENCE
SENSORS
.
39
VIII
TABLE
OF
CONTENTS
2.4.9
ELECTROMETRIC
MEASURING
SYSTEMS
.
39
2.4.10
PROCESS
CHROMATOGRAPHS
.
40
2.4.11
REMARKS
.
40
REFERENCES
.
40
3
PROCESS
ANALYTICS
OF
LIQUID
PHASES
.
42
3.1
SAMPLING
OF
LIQUID
PHASES
.
42
3.1.1
AQUEOUS
AND
ORGANIC
MATERIALS
.
42
3.1.2
MELTS
OF
METALLIC
MATERIALS
.
44
3.2
ANALYSIS
OF
LIQUID
PHASES
.
44
3.2.1
AQUEOUS
AND
ORGANIC
MATERIALS
.
44
3.2.1.1
ON-LINE
CONCEPTS
.
44
3.2.1.2
IN-LINE
ANALYTICS
AND
SENSOR
TECHNOLOGY
.
55
3.2.1.3
OFF-LINE
CONCEPTS
.
57
3.2.2
MELTS
.
62
3.3
SUPPLIERS
FOR
PROCESS
ANALYZERS
AND
OFF-LINE
ANALYTICAL
EQUIPMENT
FOR
PROCESS
CONTROL
.
63
3.3.1
PROCESS
TITRATORS
.
63
3.3.2
ELECTROCHEMICAL
ANALYZERS
.
63
3.3.3
PROCESS
PHOTOMETERS
.
64
3.3.4
X-RAY
FLUORESCENCE
SPECTROMETER/X-RAY
DIFFRACTION
SPECTROMETER
.
64
3.3.5
FT-IR/RAMAN
SPECTROMETER
.
64
3.3.6
LABORATORY
ROBOTS
.
65
3.3.7
FLUORESCENCE/STRAY
LIGHT
SENSORS
.
65
3.3.8
REMARKS
.
65
REFERENCES
.
65
4
PROCESS
ANALYTICS
OF
SOLID
MATERIALS
.
67
4.1
SAMPLING
OF
PRODUCT
FLOWS
.
67
4.2
ANALYTICAL
METHODS
FOR
SOLIDS
.
70
4.2.1
X-RAY
FLUORESCENCE
ANALYSIS
.
70
4.2.2
X-RAY
DIFFRACTION
.
72
4.2.3
NEUTRON
SCATTERING
.
72
4.2.4
MICROWAVE
TRANSMISSION
.
74
4.3
EXAMPLES
FOR
INDUSTRIAL
APPLICATIONS
.
74
4.3.1
PROCESS
CONTROL
OF
CEMENT
PRODUCTION
.
74
4.3.2
ON-LINE
ANALYSIS
OF
FLOTATION
PROCESSES
.
77
4.3.3
PROCESS
ANALYTICS
OF
COPPER
METALLURGY
.
80
4.3.4
CONTINUOUS
CONTROL
OF
IRON
ORE
SINTER
PRODUCTION
.
81
4.3.5
ON-LINE
ANALYSIS
OF
LUMP
MATERIALS
.
84
4.4
SUPPLIERS
FOR
SAMPLING
AND
SAMPLE
PREPARATION
DEVICES
AND
FOR
ANALYTICAL
AND
AUTOMATION
SYSTEMS
.
86
4.4.1
SAMPLING
AND
SAMPLE
PREPARATION
.
86
TABLE
OF
CONTENTS
IX
4.4.2
WAVELENGTH-DISPERSIVE
X-RAY
FLUORESCENCE
SPECTROMETERS
.
86
4.4.3
ENERGY-DISPERSIVE
X-RAY
FLUORESCENCE
SPECTROMETERS
.
86
4.4.4
X-RAY
DIFFRACTOMETERS
.
87
4.4.5
RADIOMETRIC
ANALYTICAL
SYSTEMS
.
87
4.4.6
REMARKS
.
87
REFERENCES
.
87
5
PROCESS
ANALYTICS
IN
THE
CHEMICAL
INDUSTRY
.
89
5.1
THE
ROLE
OF
ANALYTICS
IN
THE
CHEMICAL
INDUSTRY
.
89
5.2
PROCESS
ANALYTICS
FOR
DYE-STUFF
PRODUCTION
(BATCH
PROCESS
CONTROL)
.
90
5.3
ON-LINE
ANALYTICS
AND
BIOSENSORICS
IN
BIOTECHNOLOGY
.
92
5.3.1
BIOTECHNOLOGY
AND
BIOPROCESSES
.
92
5.3.2
TOTAL
CHEMICAL
ANALYSIS
SYSTEMS
(TAS)
.
93
5.3.3
FLOW
INJECTION
ANALYSIS
(FIA)
.
95
5.3.4
HIGH
PERFORMANCE
LIQUID
CHROMATOGRAPHY
(HPLC)
.
98
5.3.5
CAPILLARY
ELECTROPHORESIS
(CE)
.
98
5.4
SUPPLIERS
FOR
SENSORS
AND
APPLIANCES
.
99
5.4.1
REMARKS
.
99
REFERENCES
.
99
6
METALLURGICAL
PROCESS
TECHNOLOGY
AND
CHEMICAL
PROCESS
ANALYTICS
.
101
6.1
INTRODUCTION
.
101
6.1.1
ECONOMIC
IMPORTANCE
OF
IRON
(STEEL)
AND
ITS
METALLURGY
.
101
6.1.2
PRESENCE
OF
IRON
IN
NATURE
.
103
6.1.3
HISTORY
.
104
6.1.4
THE
METALLURGICAL
PRODUCTS
PIG
IRON
AND
STEEL
.
105
6.2
PROCESS
ANALYTICS
OF
THE
BLAST
FURNACE
PROCESS
.
108
6.2.1
METALLURGY
AND
ITS
ANALYTICAL
REQUISITES
.
108
6.2.2
PROCESS
TECHNOLOGY
AND
PROCESS
ANALYTICS
.
112
6.3
PROCESS
ANALYTICS
OF
STEEL
PRODUCTION
.
118
6.3.1
METALLURGY
AND
ITS
ANALYTICAL
PRESUPPOSITIONS
.
118
6.3.2
METHODS
OF
PROCESS
ANALYTICS
.
126
6.3.2.1
SAMPLING
AND
SAMPLE
PREPARATION
.
126
6.3.2.2
ANALYTICAL
METHODS
.
128
6.3.2.3
AUTOMATIZATION
OF
PROCESS
ANALYTICS
METHODS
IN
CENTRAL
LABORATORIES
.
131
6.3.2.4
ON-SITE
ANALYTICS
.
134
6.3.2.5
IN-LINE
ANALYTICS
.
137
6.4
PROCESS
ANALYTICS
IN
NON-FERROUS
METALLURGY
.
138
6.5
ANALYTICAL
INVESTIGATIONS
OF
METAL
FORMING
AND
ANNEALING
PROCESSES
FOR
SHEET
PRODUCTION
.
139
6.6
CONTROL
OF
SURFACE
COATING
PROCESSES
.
146
6.7
ANALYTICS
OF
METALLIC
MATERIALS
.
148
X
TABLE
OF
CONTENTS
6.7.1
MATERIAL
PROPERTIES
AND
TRACE
ANALYSIS
OF
STEEL
MATERIALS
.
148
6.7.2
PHASE
AND
MICROANALYTICS
.
150
6.7.3
SURFACE
TECHNOLOGY
AND
SURFACE
ANALYTICS
.
152
6.7.3.1
IMPORTANCE
OF
SURFACE
ANALYTICAL
METHODS
.
152
6.7.3.2
APPLICATION
OF
GLOW
DISCHARGE
EMISSION
SPECTROMETRY
.
155
67.3.3
INVESTIGATIONS
OF
COATED
MATERIALS
WITH
SECONDARY
NEUTRAL
PARTICLE
MASS
SPECTROMETRY
.
159
6.8
SUPPLIERS
OF
SAMPLING,
SAMPLE
PREPARATION,
ANALYSIS
AND
AUTOMATION
SYSTEMS
.
163
6.8.1
SAMPLING
PROBES
.
163
6.8.2
PNEUMATIC
TUBE
SYSTEMS
FOR
SAMPLE
TRANSPORT
.
163
6.8.3
AUTOMATED
SAMPLE
PREPARATION
BY
CUTTING,
GRINDING
OR
CRUSHING
AND
PRESSING
RESPECTIVELY
.
164
6.8.4
LABORATORY
AUTOMATION
.
164
6.8.5
CALIBRATION
SAMPLES/REFERENCE
MATERIALS
.
164
6.8.6
OPTICAL
EMISSION
SPECTROMETER
.
164
6.8.7
X-RAY
FLUORESCENCE
SPECTROMETER
.
165
6.8.8
ANALYSERS
FOR
THE
DETERMINATION
OF
CARBON,
SULPHUR,
NITROGEN,
OXYGEN
AND
HYDROGEN
IN
METALS
.
165
6.8.9
CONTAINER/CABIN
LABORATORIES
.
165
6.8.10
MOBILE
SPECTROMETER
.
165
6.8.11
REMARKS
.
165
REFERENCES
.
166
7
PROCESS
ANALYTICS
IN
THE
SEMICONDUCTOR
INDUSTRY
.
169
7.1
INTRODUCTION
.
169
7.1.1
MICROELECTRONIC
TECHNOLOGY
.
169
7.1.2
SEMICONDUCTOR
TECHNOLOGY
.
170
7.1.3
SOLAR
TECHNOLOGY
.
171
7.2
INVESTIGATION
OF
SILICON
SUBSTRATES
.
172
7.3
SURFACE
AND
THIN
LAYER
ANALYTICS
.
174
7.4
ANALYTICAL
CONTROL
OF
ULTRA-PURE
CHEMICALS
AND
CHEMICAL
PROCESSES
.
177
7.5
CONTAMINATION
CONTROL
OF
PROCESSES
AND
PRODUCTION
INSTALLATIONS
177
REFERENCES
.
180
8
PROCESS
TECHNOLOGY
AND
ENVIRONMENT
.
183
8.1
PROTECTION
OF
THE
ENVIRONMENT
AND
SOCIETY
.
183
8.2
ANALYSIS
OF
AIR
AND
ITS
POLLUTANTS
.
186
8.3
ANALYSIS
OF
THE
CONSTITUENTS
OF
DRINKING
WATER,
WATER
FIT
FOR
INDUSTRIAL
USE
AND
WASTE
WATER
.
188
8.3.1
PROCESS
TECHNOLOGY
AND
LEGISLATION
.
188
8.3.2
WATER
TREATMENT
AND
WASTE
WATER
ANALYTICS
.
190
8.3.3
WASTE
WATER
LAW
AND
WASTE
WATER
ANALYTICS
.
194
TABLE
OF
CONTENTS
XI
8.3.4
INSTRUMENTAL
METHODS
IN
WATER
ANALYTICS
.
195
8.3.5
DETERMINATION
OF
CUMULATIVE
PARAMETERS
WITHIN
WATER
ANALYTICS
197
8.4
INVESTIGATION
OF
SOLID
INDUSTRIAL
WASTE
.
199
REFERENCES
.
199
9
CHEMICAL
PROCESS
ANALYTICS
AS
PART
OF
QUALITY
MANAGEMENT
AND
QUALITY
ASSURANCE
.
201
9.1
ON
QUALITY
ASSURANCE
.
201
9.2
QUALITY
MANAGEMENT
WITHIN
ANALYTICAL
LABORATORIES
.
203
9.2.1
SIGNIFICANCE
OF
QUALITY
ASSURANCE
FOR
AND
IN
CHEMICAL
INDUSTRIAL
ANALYTICS
.
203
9.2.2
THE
QUALITY
MANUAL
.
206
9.3
CONSEQUENCES
FOR
QUALITY
ASSURANCE
IN
ANALYTICAL
LABORATORIES
.
209
9.3.1
PERSONNEL
QUALIFICATIONS
AND
EQUIPMENT
.
209
9.3.2
CHECKING
MEASURING
AND
TEST
EQUIPMENT
.
209
9.3.3
TEST
CONTROL
.
210
9.3.4
TEST
INSTRUCTIONS
.
210
9.3.5
CONTROL
ANALYSES
.
217
9.3.6
REFERENCE
MATERIALS
.
218
9.3.7
INTERLABORATORY
STUDIES
.
219
9.3.8
QUALITY
AUDITS
.
219
9.4
PROCESS
CAPABILITY
AND
MACHINE
CAPABILITY
.
220
9.5
ACCREDITATION
OF
ANALYTICAL
LABORATORIES
.
222
REFERENCES
.
223
10
ECONOMY
OF
INDUSTRIAL
ANALYTICS
.
225
REFERENCES
.
230
11
OUTLOOK
ON
RESEARCH
AND
DEVELOPMENT
TRENDS
IN
INDUSTRIAL
PROCESS
AND
PRODUCT
ANALYTICS
.
231
11.1
PROCESS
ANALYTICS
AND
AUTOMATION
.
231
11.2
SPECTROSCOPIC
METHOD
DEVELOPMENTS
.
233
11.3
MATERIAL
SCIENCES
.
234
REFERENCES
.
235
SUBJECT
INDEX
.
236 |
| any_adam_object | 1 |
| author | Koch, Karl Heinz |
| author_facet | Koch, Karl Heinz |
| author_role | aut |
| author_sort | Koch, Karl Heinz |
| author_variant | k h k kh khk |
| building | Verbundindex |
| bvnumber | BV012728397 |
| callnumber-first | T - Technology |
| callnumber-label | TP155 |
| callnumber-raw | TP155.75 |
| callnumber-search | TP155.75 |
| callnumber-sort | TP 3155.75 |
| callnumber-subject | TP - Chemical Technology |
| classification_rvk | VN 7000 VN 7500 |
| ctrlnum | (OCoLC)41981236 (DE-599)BVBBV012728397 |
| dewey-full | 660/.2815 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660/.2815 |
| dewey-search | 660/.2815 |
| dewey-sort | 3660 42815 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV012728397 |
| illustrated | Illustrated |
| indexdate | 2024-08-16T01:17:24Z |
| institution | BVB |
| isbn | 3540653376 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008654114 |
| oclc_num | 41981236 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-384 DE-1050 DE-526 |
| owner_facet | DE-19 DE-BY-UBM DE-384 DE-1050 DE-526 |
| physical | XI, 239 S. graph. Darst. |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Springer |
| record_format | marc |
| spelling | Koch, Karl Heinz Verfasser aut Process analytical chemistry control, optimization, quality, economy Karl Heinz Koch Berlin [u.a.] Springer 1999 XI, 239 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturangaben. - Dt. Ausg. u.d.T.: Koch, Karl Heinz: Industrielle Prozessanalytik Chemical process control Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Metallurgie (DE-588)4074756-6 gnd rswk-swf Verfahrenstechnik (DE-588)4062781-0 gnd rswk-swf Instrumentelle Analytik (DE-588)4222592-9 gnd rswk-swf Technische Chemie (DE-588)4078178-1 gnd rswk-swf Prozessanalyse (DE-588)4136607-4 gnd rswk-swf Prozessanalyse (DE-588)4136607-4 s DE-604 Metallurgie (DE-588)4074756-6 s Instrumentelle Analytik (DE-588)4222592-9 s 1\p DE-604 Verfahrenstechnik (DE-588)4062781-0 s 2\p DE-604 Technische Chemie (DE-588)4078178-1 s Analytische Chemie (DE-588)4129906-1 s 3\p DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008654114&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Koch, Karl Heinz Process analytical chemistry control, optimization, quality, economy Chemical process control Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd Metallurgie (DE-588)4074756-6 gnd Verfahrenstechnik (DE-588)4062781-0 gnd Instrumentelle Analytik (DE-588)4222592-9 gnd Technische Chemie (DE-588)4078178-1 gnd Prozessanalyse (DE-588)4136607-4 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4074756-6 (DE-588)4062781-0 (DE-588)4222592-9 (DE-588)4078178-1 (DE-588)4136607-4 |
| title | Process analytical chemistry control, optimization, quality, economy |
| title_auth | Process analytical chemistry control, optimization, quality, economy |
| title_exact_search | Process analytical chemistry control, optimization, quality, economy |
| title_full | Process analytical chemistry control, optimization, quality, economy Karl Heinz Koch |
| title_fullStr | Process analytical chemistry control, optimization, quality, economy Karl Heinz Koch |
| title_full_unstemmed | Process analytical chemistry control, optimization, quality, economy Karl Heinz Koch |
| title_short | Process analytical chemistry |
| title_sort | process analytical chemistry control optimization quality economy |
| title_sub | control, optimization, quality, economy |
| topic | Chemical process control Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd Metallurgie (DE-588)4074756-6 gnd Verfahrenstechnik (DE-588)4062781-0 gnd Instrumentelle Analytik (DE-588)4222592-9 gnd Technische Chemie (DE-588)4078178-1 gnd Prozessanalyse (DE-588)4136607-4 gnd |
| topic_facet | Chemical process control Chemistry, Analytic Analytische Chemie Metallurgie Verfahrenstechnik Instrumentelle Analytik Technische Chemie Prozessanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008654114&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kochkarlheinz processanalyticalchemistrycontroloptimizationqualityeconomy |