Modern techniques for polymer characterisation:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
1999
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVII, 392 S. graph. Darst. |
| ISBN: | 0471960977 |
Internformat
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Datensatz im Suchindex
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| adam_text | MODERN TECHNIQUES FOR POLYMER CHARACTERISATION EDITED BY R.A. PETHRICK
UNIVERSITY OF STRATHCLYDE, GLASGOW, UK AND J.V. DAWKINS LOUGHBOROUGH
UNIVERSITY, LOUGHBOROUGH, UK JOHN WILEY & SONS CHICHESTER * NEW YORK *
WEINHEIM * BRISBANE * SINGAPORE * TORONTO CONTENTS LIST OF CONTRIBUTORS
XIII PREFACE XV 1 TEMPERATURE RISING ELUTION FRACTIONATION 1 CLAUDIA A.
FONSECA AND IAN R. HARRISON 1.1 INTRODUCTION 1 1.2 EXPERIMENTAL
TECHNIQUES 2 1.2.1 TREF MODES AND APPARATUS 2 1.2.2 CRYSTALLIZATION AND
ELUTION 3 1.3 DETAILED TREF EXPERIMENTAL PROCEDURE 7 1.4 DATA ANALYSIS
11 1.5 FUTURE TRENDS 12 2 TEMPERATURE RISING ELUTION FRACTIONATION 15
JOAO B.P. SOARES AND ARCHIE E. HAMIELEC 2.1 INTRODUCTION 15 2.1.1
ORIGINS OF COMPOSITION AND STEREOREGULARITY HETEROGENEITY IN POLYMERS 15
2.1.2 EFFECTS OF COMPOSITION AND STEREOREGULARITY HETEROGENEITY ON
POLYMER PROPERTIES 20 2.2 TREF OPERATION AND CHARACTERISTICS 21 2.2.1
DEFINITION OF TREF 21 2.2.2 MECHANISM OF FRACTIONATION 22 2.2.3 BASIC
EXPERIMENTAL APPARATUS 23 2.2.4 OPERATION CONDITIONS DURING
CRYSTALLIZATION AND ELUTION 27 2.2.5 CALIBRATION CURVE FOR A-TREF 31 2.3
TREF APPLICATIONS 32 2.3.1 POLYMER STRUCTURE AND POLYMERIZATION
CATALYSIS ... 33 2.3.2 EFFECT OF POLYMERIZATION REACTOR CONDITIONS 36
2.3.3 COMBINED TREF AND SEC ANALYSIS 37 VI CONTENTS 2.4 MATHEMATICAL
MODELING OF TREF 39 2.4.1 STOCKMAYER S BIVARIATE DISTRIBUTION 39 2.4.2
MONTE CARLO SIMULATION 42 2.4.3 MODELING BASED ON THERMODYNAMIC
EQUILIBRIUM IN TREF 43 2.5 FUTURE DEVELOPMENTS AND ALTERNATIVE
TECHNIQUES 43 2.5.1 CRYSTALLIZATION FRACTIONATION 44 2.5.2 SUPERCRITICAL
TREF 49 2.5.3 DIFFERENTIAL SCANNING CALORIMETRY 49 2.6 CONCLUSIONS 51 3
FIELD FLOW FRACTIONATION 57 JOSEF JANCA 3.1 INTRODUCTION 57 3.2
THEORETICAL BASIS 59 3.2.1 POLARIZATION AND FOCUSING MECHANISMS 59 3.2.2
RETENTION 60 3.2.3 ZONE DISPERSION 63 3.2.4 STERIC EXCLUSION 63 3.2.5
RELAXATION 65 3.3 METHODS AND TECHNIQUES 65 3.3.1 POLARIZATION FFF 66
3.3.2 FOCUSING FFF 75 3.3.3 SECONDARY EQUILIBRIA IN POLARIZATION AND
FOCUSING FFF 76 3.4 INSTRUMENTATION 76 3.5 DATA TREATMENT 76 3.6
CONCLUDING REMARKS 79 4 STATIC AND DYNAMIC LIGHT SCATTERING 81 GUY C.
BERRY AND PATRICIA M. COTTS 4.1 INTRODUCTION 81 4.2 SCATTERING
RELATIONSHIPS 82 4.2.1 SCATTERED INTENSITY MEASURES 82 4.2.2 STATIC
SCATTERING RELATIONSHIPS 83 4.2.3 DYNAMIC SCATTERING RELATIONSHIPS 88
4.3 EXPERIMENTAL METHODS 89 4.3.1 LIGHT SCATTERING INSTRUMENTATION 89
4.3.2 OPTICAL ALIGNMENT 90 4.3.3 CALIBRATION 91 4.3.4 OPTICAL FACTORS 93
4.3.5 CALIBRATION STANDARD 94 4.3.6 SAMPLE PREPARATION 95 CONTENTS VII
4.4 DATA TREATMENT 96 4.4.1 STATIC SCATTERING 96 4.4.2 DYNAMIC
SCATTERING 98 4.5 EXAMPLES 101 4.5.1 STATIC SCATTERING AND SIZE
EXCLUSION CHROMATOGRAPHY 101 4.5.2 INTERMOLECULAR ASSOCIATION 104 4.5.3
SCATTERING WITH CHARGED SPECIES 105 5 NEUTRON REFLECTION STUDIES OF
POLYMERS 109 DAVID G. BUCKNALL 5.1 INTRODUCTION 109 5.2 THEORETICAL
DESCRIPTION OF REFLECTIVITY ILL 5.3 INSTRUMENTATION 114 5.4 SAMPLE
PREPARATION 118 5.4.1 AIR-LIQUID SAMPLES 118 5.4.2 AIR-SOLID SAMPLES 118
5.4.3 LIQUID-SOLID SAMPLES 121 5.5 DATA ANALYSIS 123 5.5.1 FOURIER
TRANSFORMS 123 5.5.2 MODEL FITTING 128 5.5.3 EXPERIMENTAL DESIGN 131 5.6
DATA INTERPRETATION 133 5.6.1 CONVERTING SCATTERING LENGTH DENSITY
PROFILES INTO VOLUME FRACTION PROFILES 133 5.6.2 DETERMINING THE
FLORY-HUGGINS PARAMETER AND INTERFACIAL TENSION FROM THE WIDTH OF THE
POLYMER-POLYMER INTERFACES 134 5.6.3 DETERMINATION OF THE
POLYMER-POLYMER DIFFUSION COEFFICIENT 136 5.6.4 CALCULATING AREA PER
MOLECULE AND SURFACE EXCESS FOR MONOLAYERS USING MODEL FITS 138 6
NEUTRON SCATTERING STUDIES OF POLYMER DYNAMICS 141 VALERIA ARRIGHI 6.1
INTRODUCTION 141 6.2 PRINCIPLES OF INELASTIC SCATTERING 143 6.3
SPECTROMETERS 149 6.3.1 TIME-OF-FLIGHT SPECTROMETERS 149 6.3.2
BACK-SCATTERING SPECTROMETERS 152 6.3.3 NEUTRON SPIN-ECHO SPECTROMETERS
153 6.4 EXPERIMENTAL CONSIDERATIONS 154 6.4.1 SEPARATION OF MOLECULAR
MOTIONS 154 6.4.2 CHOOSING A SPECTROMETER 155 VIII CONTENTS 6.4.3
SAMPLES 157 6.4.4 MEASUREMENTS 159 6.4.5 DATA CORRECTION 159 6.5 DATA
ANALYSIS AND INTERPRETATION OF THE RESULTS 160 6.5.1 VIBRATIONAL MOTION
BY INCOHERENT INELASTIC NEUTRON SCATTERING 160 6.5.2 QUASIELASTIC
NEUTRON SCATTERING 160 6.5.3 NEUTRON SPIN-ECHO 169 7 SMALL-ANGLE NEUTRON
SCATTERING 171 STEPHEN M. KING 7.1 INTRODUCTION 171 7.2 BACKGROUND 171
7.2.1 SMALL-ANGLE SCATTERING TECHNIQUES 171 7.2.2 SMALL-ANGLE NEUTRON
SCATTERING 173 7.3 ESSENTIAL CONCEPTS 175 7.3.1 SCATTERING VECTOR 175
7.3.2 DIFFERENTIAL SCATTERING CROSS-SECTION 177 7.3.3 SCATTERING LENGTH
DENSITY AND CONTRAST 178 7.3.4 FORM AND STRUCTURE FACTORS 182 7.4
PREPARING FOR THE EXPERIMENT 183 7.4.1 ARE NEUTRONS APPROPRIATE? 183
7.4.2 CHOOSING A FACILITY AND AN INSTRUMENT 183 7.4.3 INSTRUMENT
SCIENTIST 187 7.4.4 APPLYING FOR BEAM TIME 188 7.4.5 PREPARING THE
SAMPLE 189 7.4.6 USING D 2 0 192 7.4.7 EFFECTS OF DEUTERIUM SUBSTITUTION
193 7.5 DURING THE EXPERIMENT 194 7.5.1 WHAT NEEDS TO BE MEASURED 194
7.5.2 DATA COLLECTION STRATEGIES 197 7.5.3 SAMPLE ALIGNMENT
CONSIDERATIONS 197 7.6 DATA INTERPRETATION 198 7.6.1 DATA REDUCTION .
198 7.6.2 DATA NORMALISATION 200 7.6.3 DATA ANALYSIS 202 7.6.4 EXAMPLE
APPLICATIONS 222 7.7 SUMMARY 222 8 RECENT ADVANCES IN MASS SPECTROMETRY
OF POLYMERS 233 EMILIO SCAMPORRINO AND DANIELE VITALINI 8.1 INTRODUCTION
233 8.2 ELECTROSPRAY MASS SPECTROMETRY 235 8.3 MALDI-TOF MASS
SPECTROMETRY 246 CONTENTS IX 9 VAPOUR PRESSURE OSMOMETRY/MEMBRANE
OSMOMETRY/VISCOMETRY 267 BARRY J. HUNT 9.1 GENERAL INTRODUCTION 267 9.2
VAPOUR PRESSURE OSMOMETRY 268 9.2.1 INTRODUCTION 268 9.2.2 THEORY 268
9.2.3 EQUIPMENT 269 9.2.4 EXPERIMENTAL PROCEDURES 271 9.2.5 CALCULATION
OF RESULTS 272 9.2.6 ERRORS 272 9.3 MEMBRANE OSMOMETRY 273 9.3.1
INTRODUCTION 273 9.3.2 THEORY 273 9.3.3 INSTRUMENTATION 274 9.3.4
EXPERIMENTAL PROCEDURES 276 9.3.5 MEMBRANES 277 9.3.6 SOLVENTS 277 9.3.7
CALCULATION OF RESULTS 278 9.3.8 ERRORS 278 9.4 VISCOMETRY 279 9.4.1
INTRODUCTION 279 9.4.2 THEORY 279 9.4.3 APPARATUS 280 9.4.4 TECHNIQUE
FOR CAPILLARY VISCOMETRY 282 9.4.5 CALCULATION OF RESULTS 284 9.4.6
ERRORS 284 10 GEL ELECTROPHORESIS OF BIOLOGICAL MACROMOLECULES 287
CHRISTOPHER VINEY AND LISA K. GILLILAND 10.1 INTRODUCTION 287 10.1.1
BACKGROUND 287 10.1.2 AIMS 288 10.1.3 TYPES OF MOLECULES THAT CAN BE
CHARACTERIZED .... 288 10.2 PHYSICAL BASIS OF GEL ELECTROPHORESIS 288
10.3 CHEMICALS, HARDWARE AND PROTOCOLS FOR GEL ELECTROPHORESIS 294
10.3.1 GEL CHEMISTRY AND PREPARATION 294 10.3.2 BUFFERS 296 10.3.3
MOLECULAR WEIGHT MARKERS 298 10.3.4 GEL SHAPE, THICKNESS AND ORIENTATION
299 10.3.5 LOADING THE SAMPLES AND MOLECULAR WEIGHT MARKERS 301 X
CONTENTS 10.3.6 POWER SUPPLY 301 10.3.7 TRACKING DYE 302 10.4 LOCATING,
CHARACTERIZING AND RECOVERING THE SEPARATED MACROMOLECULES 302 10.4.1
STAINING AND DESTAINING 302 10.4.2 MOBILITY 303 10.4.3 TECHNIQUES FOR
DETECTING BANDS AND QUANTIFYING CONCENTRATION IN SEPARATED PROTEINS 304
10.4.4 ARCHIVAL USE OF GELS 305 10.4.5 RECOVERING SEPARATED
MACROMOLECULES FOR FURTHER CHARACTERIZATION OR PROCESSING 305 10.4.6
BLOTTING 306 10.5 OPTIMIZING RESOLUTION AND CONTRAST 306 10.5.1
RESOLUTION 306 10.5.2 METHODS FOR IMPROVING RESOLUTION 307 10.5.3
CONCENTRATION GRADIENT GELS 308 10.5.4 TWO-DIMENSIONAL GELS 308 10.5.5
CONTRAST . . 312 10.6 SOURCES OF ERROR 312 11 UITRACENTRIFUGATION AND
SEDIMENTATION 317 WERNER BORCHARD AND EVA SELIC 11.1 INTRODUCTION 317
11.2 EXPERIMENTAL ASPECTS OF ANALYTICAL UITRACENTRIFUGATION . 318 11.2.1
ULTRACENTRIFUGE ASSEMBLY 318 11.2.2 SAMPLE PREPARATION 321 11.3 STANDARD
METHODS 322 11.3.1 SEDIMENTATION EQUILIBRIUM OF A POLYDISPERSE POLYMER
IN SOLUTION 322 11.3.2 SEDIMENTATION VELOCITY OF POLYMER SOLUTIONS 325
11.3.3 SPECIAL APPLICATIONS 329 11.4 CHARACTERIZATION OF GELS BY MEANS
OF ANALYTICAL UITRACENTRIFUGATION 335 11.4.1 SEDIMENTATION-DIFFUSION
EQUILIBRIUM OF A BINARY GEL 336 11.4.2 SEDIMENTATION VELOCITY OF A
BINARY GEL 346 11.5 CONCLUSIONS 348 12 TERMINOLOGY FOR POLYMER CHEMISTRY
353 AUBREY D. JENKINS 12.1 INTRODUCTION 353 12.2 THE STIPULATION 354
12.3 POLYMERS AND POLYMER MOLECULES: BASIC DEFINITIONS OF TERMS 355
CONTENTS XI 12.4 SOURCE-BASED AND STRUCTURE-BASED NOMENCLATURE 356 12.5
MACROMOLECULAR ARCHITECTURE 357 12.6 REGULAR SINGLE-STRAND,
QUASI-SINGLE-STRAND, AND DOUBLE-STRAND POLYMERS 357 12.7 POLYMER
FORMULAE 358 12.8 OTHER COMMISSION DOCUMENTS 359 12.9 DEFINITIONS
SELECTED FROM **** NOMENCLATURE DOCUMENTS 359 12.9.1 GLOSSARY OF BASIC
TERMS IN POLYMER SCIENCE (1996) 359 12.9.2 DEFINITIONS OF TERMS RELATING
TO INDIVIDUAL MACROMOLECULES, THEIR ASSEMBLIES, AND DILUTE POLYMER
SOLUTIONS (1988) 366 13 COLLIGATIVE PROPERTIES 375 HIDEMATSU SUZUKI AND
KENJI KAMIDE 13.1 INTRODUCTION 375 13.2 VAPOUR-PRESSURE OSMOMETRY 377
13.2.1 PRINCIPLES 377 13.2.2 APPARATUS AND MEASUREMENT 379 13.3 MEMBRANE
OSMOMETRY 383 13.3.1 PRINCIPLES 383 13.3.2 APPARATUS AND MEASUREMENT 384
INDEX 389
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| spelling | Modern techniques for polymer characterisation ed. by R. A. Pethrick ... Chichester [u.a.] Wiley 1999 XVII, 392 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polimeros (quimica) larpcal Polymères - Analyse Polymères - Analyse ram Polymers Analysis Spektroskopie (DE-588)4056138-0 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Polymere (DE-588)4046699-1 s Spektroskopie (DE-588)4056138-0 s DE-604 Pethrick, Richard A. Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008563240&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Modern techniques for polymer characterisation Polimeros (quimica) larpcal Polymères - Analyse Polymères - Analyse ram Polymers Analysis Spektroskopie (DE-588)4056138-0 gnd Polymere (DE-588)4046699-1 gnd |
| subject_GND | (DE-588)4056138-0 (DE-588)4046699-1 |
| title | Modern techniques for polymer characterisation |
| title_auth | Modern techniques for polymer characterisation |
| title_exact_search | Modern techniques for polymer characterisation |
| title_full | Modern techniques for polymer characterisation ed. by R. A. Pethrick ... |
| title_fullStr | Modern techniques for polymer characterisation ed. by R. A. Pethrick ... |
| title_full_unstemmed | Modern techniques for polymer characterisation ed. by R. A. Pethrick ... |
| title_short | Modern techniques for polymer characterisation |
| title_sort | modern techniques for polymer characterisation |
| topic | Polimeros (quimica) larpcal Polymères - Analyse Polymères - Analyse ram Polymers Analysis Spektroskopie (DE-588)4056138-0 gnd Polymere (DE-588)4046699-1 gnd |
| topic_facet | Polimeros (quimica) Polymères - Analyse Polymers Analysis Spektroskopie Polymere |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008563240&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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