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Previous Title:	Davis, Reg Mass spectrometry
Main Author:	Barker, James (Author)
Format:	Book
Language:	English
Published:	Chichester [u.a.] Wiley 1999
Edition:	2. ed.
Series:	Analytical chemistry by open learning
Subjects:	Chimie analytique Chromatographie Spectroscopie de masse Chemistry, Analytic > Programmed instruction Mass spectrometry > Programmed instruction Massenspektrometrie Analytische Chemie Aufsatzsammlung Matériel didactique
Online Access:	Inhaltsverzeichnis Inhaltsverzeichnis
Physical Description:	XXII, 509 S. Ill., graph. Darst.
ISBN:	0471967629 0471967645

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Record in the Search Index

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adam_text	MASS SPECTROMETRY ANALYTICAL CHEMISTRY BY OPEN LEARNING SECOND EDITION AUTHOR: JAMES BARKER UNIVERSITY OF GREENWICH EDITOR: DAVID J. ANDO UNIVERSITY OF GREENWICH AUTHORS OF FIRST EDITION: REGINALD DAVIS UNIVERSITY OF KINGSTON MARTIN J. FREARSON UNIVERSITY OF HERTFORDSHIRE PUBLISHED ON BEHALF OF ACOL (UNIVERSITY OF GREENWICH) BY JOHN WILEY & SONS CHICHESTER * NEW YORK * BRISBANE * SINGAPORE * TORONTO CONTENTS STUDY GUIDE XV SUPPORTING PRACTICAL WORK XVII BIBLIOGRAPHY XIX ACKNOWLEDGEMENTS XXI 1. INTRODUCTION 1 1.1 MASS SPECTROMETRY: ITS CONCEPTS AND BEGINNINGS . . . . 1 1.2 IONISATION AND FRAGMENTATION 2 1.2.1 IONISATION 2 1.2.2 FRAGMENTATION 6 1.2.3 RULES FOR ASSIGNMENT OF FRAGMENTS 9 1.2.4 THE NITROGEN RULE 10 1.2.5 LOW-RELATIVE-ABUNDANCE PEAKS 11 1.3 THE SIMPLE MASS SPECTRUM 11 2. ION SOURCES AND METHODS OF IONISATION 19 2.1 IONISATION BY ELECTRON IMPACT 19 2.2 CHEMICAL IONISATION 27 2.3 FIELD IONISATION AND FIELD DESORPTION 36 2.3.1 FIELD IONISATION 36 2.3.2 FIELD DESORPTION 39 2.4 FAST-ATOM-BOMBARDMENT 40 2.5 PLASMA DESORPTION 45 2.6 LASER DESORPTION 45 2.7 OTHER ION SOURCES 48 2.8 METHODS FOR SAMPLE INTRODUCTION 48 3. THE MASS SPECTROMETER 55 3.1 THE MASS SPECTROMETER SYSTEM: AN OVERVIEW 55 3.2 MASS RESOLUTION 64 XI XII ANALYTICAL CHEMISTRY BY OPEN LEARNING 3.3 DOUBLE-FOCUSING MASS SPECTROMETER 68 3.4 QUADRUPOLE MASS ANALYSER 74 3.5 SCAN RATE 79 3.6 ION-TRAP ANALYSER 81 3.7 TIME-OF-FLIGHT (TOF) ANALYSER 82 3.8 FOURER-TRANSFORM (FT) INSTRUMENTS 84 3.9 TANDEM MASS SPECTROMETRY (MS/MS) 90 4. ION DETECTION, DATA RECORDING AND PROCESSING 95 4.1 ION DETECTION 95 4.1.1 ELECTRON MULTIPLIERS 95 4.1.2 FARADYCUP 98 4.1.3 OTHER TYPES OF DETECTORS 99 4.2 METHODS OF DATA RECORDING 99 4.2.3 OSCILLOSCOPE AND CHART RECORDER 99 4.2.2 COMPUTER-AIDED DATA ACQUISITION AND PROCESSING 101 5. USE OF ISOTOPES IN MASS SPECTROMETRY 117 5.1 INTRODUCTION 117 5.2 ISOTOPE ABUNDANCES: NON-HALOGEN ISOTOPES 118 5.3 ISOTOPE ABUNDANCES: HALOGEN ISOTOPES 132 5.3.1 INTRODUCTION 132 5.3.2 CALCULATION OF CHLORINE AND BROMINE ISOTOPE RATIOS 135 5.4 AN APPROXIMATION METHOD FOR CALCULATING RELATIVE ABUNDANCES OF CLUSTERS DUE TO MINOR ISOTOPES 144 5.5 ISOTOPE-DILUTION MASS SPECTROMETRY 147 6. METASTABLE IONS AND MODES OF FRAGMENTATION 153 6.1 ORIGIN OF METASTABLES 153 6.2 THE USE OF METASTABLE IONS 160 6.3 MODES OF FRAGMENTATION . 164 6.3.1 ENERGY FACTORS 164 6.3.2 STABILISATION FACTORS 166 6.3.3 BASIC RULES CONCERNING RESONANCE STRUCTURES . 180 6.3.4 MECHANISMS OF BOND CLEAVAGES IN MASS SPECTROMETRY 181 6.3.5 THE EVEN-ELECTRON RULE 185 CONTENTS XIII 7. TYPICAL FRAGMENTATION PATTERNS OF COMMON FUNCTIONAL GROUPS 193 7.1 INTERPRETATION PROCEDURES 194 7.1.1 GENERAL PROCEDURE FOR THE INTERPRETATION OF A MASS SPECTRUM 194 7.2 FRAGMENTATIONS OF ALCOHOLS 213 7.3 FRAGMENTATIONS OF ETHERS 228 7.4 FRAGMENTATIONS OF HYDROXYBENZENES (PHENOLS) . . . . 233 7.5 FRAGMENTATIONS OF CARBONYL COMPOUNDS 240 7.5.1 THE MCLAFFERTY REARRANGEMENT 240 7.5.2 FRAGMENTATIONS OF ALDEHYDES 245 7.5.3 FRAGMENTATIONS OF KETONES 250 7.5.4 FRAGMENTATIONS OF ESTERS 254 7.5.5 FRAGMENTATIONS OF ACIDS 258 7.5.6 FRAGMENTATIONS OF AMIDES 259 7.6 FRAGMENTATIONS OF AMINES 263 7.7 FRAGMENTATIONS OF HYDROCARBONS 270 7.8 FRAGMENTATIONS OF HALOCOMPOUNDS 279 7.9 FRAGMENTATIONS OF NITROCOMPOUNDS 285 7.10 FRAGMENTATIONS OF HETEROCYCLIC COMPOUNDS AND SULPHUR COMPOUNDS 287 7.10.1 HETEROCYCLIC COMPOUNDS 287 7.10.2 THIOLS 290 7.10.3 THIOETHERS (SULPHIDES) 291 7.10.4 ARYL ETHERS AND THIOPHENOLS 291 7.11 ANALYSIS OF BIOMOLECULES 295 7.11.1 PROTEIN ANALYSIS 297 8. ANALYSIS OF MIXTURES BY HYPHENATED MASS SPECTRAL TECHNIQUES 305 8.1 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC/MS) . . 306 8.1.1 INSTRUMENTATION 306 8.1.2 DERIVATISATION 313 8.1.3 QUANTITATIVE WORK 317 8.2 LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (LC/MS) . 320 8.2.1 INSTRUMENTATION 320 8.2.2 THERMOSPRAY (TS) INTERFACE 321 8.2.3 MOVING-BELT INTERFACE COUPLING 326 8.2.4 PARTICLE-BEAM INTERFACE COUPLING 327 8.2.5 CONTINUOUS-FLOW FAB COUPLING 328 * XIV ANALYTICAL CHEMISTRY BY OPEN LEARNING 8.2.6 ATMOSPHERIC-PRESSURE CHEMICAL IONISATION (APCI) 329 8.2.7 ELECTROSPRAY (ES) AND IONSPRAY 331 8.3 TANDEM MASS SPECTROMETRY (MS/MS) 335 8.4 CHROMATOGRAPHY DATA: ACQUISITION, RECORDING AND TREATMENT 338 8.4.1 DATA ACQUISITION 338 8.4.2 DATA RECORDING AND TREATMENT 340 9. INORGANIC MASS SPECTROMETRY 34 3 9.1 SURFACE METHODS INVOLVING MASS SPECTROMETRY . . . . 343 9.1.1 SECONDARY-ION MASS SPECTROMETRY (SIMS) . . . 343 9.1.2 ION-MICROPROBE MASS ANALYSIS (IMPMA) AND ION-BEAM LITHOGRAPHY/MODIFICATION . . . . 344 9.1.3 LASER-ASSISTED MICROPROBE MASS ANALYSIS (LAMMA) 346 9.1.4 PARTICLE-INDUCED X-RAY/GAMMA EMISSION (PIXE/PIGE) AND RUTHERFORD BACKSCATTERING (RBS) 348 9.1.5 GLOW-DISCHARGE MASS SPECTROMETRY (GDMS) . . 350 9.2 ANALYSIS OF BULK SOLIDS 351 9.2.1 ACCELERATOR MASS SPECTROMETRY (AMS) . . . . 351 9.2.2 SPARK-SOURCE MASS SPECTROMETRY 354 9.2.3 RESONANCE IONISATION MASS SPECTROMETRY (RIMS) 356 9.3 ANALYSIS OF SOLUTIONS 356 9.3.1 INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS) 356 APPENDIX 363 1. TABLE OF ISOTOPES IN ASCENDING MASS ORDER 363 2. ISOTOPIC ABUNDANCES FOR VARIOUS ELEMENTAL COMPOSITION CHON 372 SELF-ASSESSMENT QUESTIONS AND RESPONSES 385 UNITS OF MEASUREMENT 499 INDEX 505 MASS SPECTROMETRY ANALYTICAL CHEMISTRY BY OPEN LEARNING SECOND EDITION AUTHOR: JAMES BARKER UNIVERSITY OF GREENWICH EDITOR: DAVID J. ANDO UNIVERSITY OF GREENWICH AUTHORS OF FIRST EDITION: REGINALD DAVIS UNIVERSITY OF KINGSTON MARTIN J. FREARSON UNIVERSITY OF HERTFORDSHIRE PUBLISHED ON BEHALF OF ACOL (UNIVERSITY OF GREENWICH) BY JOHN WILEY & SONS CHICHESTER * NEW YORK * BRISBANE * SINGAPORE * TORONTO CONTENTS STUDY GUIDE XV SUPPORTING PRACTICAL WORK XVII BIBLIOGRAPHY XIX ACKNOWLEDGEMENTS XXI 1. INTRODUCTION 1 1.1 MASS SPECTROMETRY: ITS CONCEPTS AND BEGINNINGS . . . . 1 1.2 IONISATION AND FRAGMENTATION 2 1.2.1 IONISATION 2 1.2.2 FRAGMENTATION 6 1.2.3 RULES FOR ASSIGNMENT OF FRAGMENTS 9 1.2.4 THE NITROGEN RULE 10 1.2.5 LOW-RELATIVE-ABUNDANCE PEAKS 11 1.3 THE SIMPLE MASS SPECTRUM 11 2. ION SOURCES AND METHODS OF IONISATION 19 2.1 IONISATION BY ELECTRON IMPACT 19 2.2 CHEMICAL IONISATION 27 2.3 FIELD IONISATION AND FIELD DESORPTION 36 2.3.1 FIELD IONISATION 36 2.3.2 FIELD DESORPTION 39 2.4 FAST-ATOM-BOMBARDMENT 40 2.5 PLASMA DESORPTION 45 2.6 LASER DESORPTION 45 2.7 OTHER ION SOURCES 48 2.8 METHODS FOR SAMPLE INTRODUCTION 48 3. THE MASS SPECTROMETER 55 3.1 THE MASS SPECTROMETER SYSTEM: AN OVERVIEW 55 3.2 MASS RESOLUTION 64 XI XII ANALYTICAL CHEMISTRY BY OPEN LEARNING 3.3 DOUBLE-FOCUSING MASS SPECTROMETER 68 3.4 QUADRUPOLE MASS ANALYSER 74 3.5 SCAN RATE 79 3.6 ION-TRAP ANALYSER 81 3.7 TIME-OF-FLIGHT (TOF) ANALYSER 82 3.8 FOURER-TRANSFORM (FT) INSTRUMENTS 84 3.9 TANDEM MASS SPECTROMETRY (MS/MS) 90 4. ION DETECTION, DATA RECORDING AND PROCESSING 95 4.1 ION DETECTION 95 4.1.1 ELECTRON MULTIPLIERS 95 4.1.2 FARADYCUP 98 4.1.3 OTHER TYPES OF DETECTORS 99 4.2 METHODS OF DATA RECORDING 99 4.2.3 OSCILLOSCOPE AND CHART RECORDER 99 4.2.2 COMPUTER-AIDED DATA ACQUISITION AND PROCESSING 101 5. USE OF ISOTOPES IN MASS SPECTROMETRY 117 5.1 INTRODUCTION 117 5.2 ISOTOPE ABUNDANCES: NON-HALOGEN ISOTOPES 118 5.3 ISOTOPE ABUNDANCES: HALOGEN ISOTOPES 132 5.3.1 INTRODUCTION 132 5.3.2 CALCULATION OF CHLORINE AND BROMINE ISOTOPE RATIOS 135 5.4 AN APPROXIMATION METHOD FOR CALCULATING RELATIVE ABUNDANCES OF CLUSTERS DUE TO MINOR ISOTOPES 144 5.5 ISOTOPE-DILUTION MASS SPECTROMETRY 147 6. METASTABLE IONS AND MODES OF FRAGMENTATION 153 6.1 ORIGIN OF METASTABLES 153 6.2 THE USE OF METASTABLE IONS 160 6.3 MODES OF FRAGMENTATION . 164 6.3.1 ENERGY FACTORS 164 6.3.2 STABILISATION FACTORS 166 6.3.3 BASIC RULES CONCERNING RESONANCE STRUCTURES . 180 6.3.4 MECHANISMS OF BOND CLEAVAGES IN MASS SPECTROMETRY 181 6.3.5 THE EVEN-ELECTRON RULE 185 CONTENTS XIII 7. TYPICAL FRAGMENTATION PATTERNS OF COMMON FUNCTIONAL GROUPS 193 7.1 INTERPRETATION PROCEDURES 194 7.1.1 GENERAL PROCEDURE FOR THE INTERPRETATION OF A MASS SPECTRUM 194 7.2 FRAGMENTATIONS OF ALCOHOLS 213 7.3 FRAGMENTATIONS OF ETHERS 228 7.4 FRAGMENTATIONS OF HYDROXYBENZENES (PHENOLS) . . . . 233 7.5 FRAGMENTATIONS OF CARBONYL COMPOUNDS 240 7.5.1 THE MCLAFFERTY REARRANGEMENT 240 7.5.2 FRAGMENTATIONS OF ALDEHYDES 245 7.5.3 FRAGMENTATIONS OF KETONES 250 7.5.4 FRAGMENTATIONS OF ESTERS 254 7.5.5 FRAGMENTATIONS OF ACIDS 258 7.5.6 FRAGMENTATIONS OF AMIDES 259 7.6 FRAGMENTATIONS OF AMINES 263 7.7 FRAGMENTATIONS OF HYDROCARBONS 270 7.8 FRAGMENTATIONS OF HALOCOMPOUNDS 279 7.9 FRAGMENTATIONS OF NITROCOMPOUNDS 285 7.10 FRAGMENTATIONS OF HETEROCYCLIC COMPOUNDS AND SULPHUR COMPOUNDS 287 7.10.1 HETEROCYCLIC COMPOUNDS 287 7.10.2 THIOLS 290 7.10.3 THIOETHERS (SULPHIDES) 291 7.10.4 ARYL ETHERS AND THIOPHENOLS 291 7.11 ANALYSIS OF BIOMOLECULES 295 7.11.1 PROTEIN ANALYSIS 297 8. ANALYSIS OF MIXTURES BY HYPHENATED MASS SPECTRAL TECHNIQUES 305 8.1 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC/MS) . . 306 8.1.1 INSTRUMENTATION 306 8.1.2 DERIVATISATION 313 8.1.3 QUANTITATIVE WORK 317 8.2 LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (LC/MS) . 320 8.2.1 INSTRUMENTATION 320 8.2.2 THERMOSPRAY (TS) INTERFACE 321 8.2.3 MOVING-BELT INTERFACE COUPLING 326 8.2.4 PARTICLE-BEAM INTERFACE COUPLING 327 8.2.5 CONTINUOUS-FLOW FAB COUPLING 328 * XIV ANALYTICAL CHEMISTRY BY OPEN LEARNING 8.2.6 ATMOSPHERIC-PRESSURE CHEMICAL IONISATION (APCI) 329 8.2.7 ELECTROSPRAY (ES) AND IONSPRAY 331 8.3 TANDEM MASS SPECTROMETRY (MS/MS) 335 8.4 CHROMATOGRAPHY DATA: ACQUISITION, RECORDING AND TREATMENT 338 8.4.1 DATA ACQUISITION 338 8.4.2 DATA RECORDING AND TREATMENT 340 9. INORGANIC MASS SPECTROMETRY 34 3 9.1 SURFACE METHODS INVOLVING MASS SPECTROMETRY . . . . 343 9.1.1 SECONDARY-ION MASS SPECTROMETRY (SIMS) . . . 343 9.1.2 ION-MICROPROBE MASS ANALYSIS (IMPMA) AND ION-BEAM LITHOGRAPHY/MODIFICATION . . . . 344 9.1.3 LASER-ASSISTED MICROPROBE MASS ANALYSIS (LAMMA) 346 9.1.4 PARTICLE-INDUCED X-RAY/GAMMA EMISSION (PIXE/PIGE) AND RUTHERFORD BACKSCATTERING (RBS) 348 9.1.5 GLOW-DISCHARGE MASS SPECTROMETRY (GDMS) . . 350 9.2 ANALYSIS OF BULK SOLIDS 351 9.2.1 ACCELERATOR MASS SPECTROMETRY (AMS) . . . . 351 9.2.2 SPARK-SOURCE MASS SPECTROMETRY 354 9.2.3 RESONANCE IONISATION MASS SPECTROMETRY (RIMS) 356 9.3 ANALYSIS OF SOLUTIONS 356 9.3.1 INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY (ICP-MS) 356 APPENDIX 363 1. TABLE OF ISOTOPES IN ASCENDING MASS ORDER 363 2. ISOTOPIC ABUNDANCES FOR VARIOUS ELEMENTAL COMPOSITION CHON 372 SELF-ASSESSMENT QUESTIONS AND RESPONSES 385 UNITS OF MEASUREMENT 499 INDEX 505
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owner	DE-20 DE-91G DE-BY-TUM DE-29T DE-522 DE-634
owner_facet	DE-20 DE-91G DE-BY-TUM DE-29T DE-522 DE-634
physical	XXII, 509 S. Ill., graph. Darst.
publishDate	1999
publishDateSearch	1999
publishDateSort	1999
publisher	Wiley
record_format	marc
series2	Analytical chemistry by open learning
spelling	Barker, James Verfasser aut Mass spectrometry author: James Barker 2. ed. Chichester [u.a.] Wiley 1999 XXII, 509 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Analytical chemistry by open learning Chimie analytique ram Chromatographie ram Spectroscopie de masse ram Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie (DE-588)4037882-2 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Matériel didactique Massenspektrometrie (DE-588)4037882-2 s Analytische Chemie (DE-588)4129906-1 s 1\p DE-604 Ersatz von Davis, Reg Mass spectrometry GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk
spellingShingle	Barker, James Mass spectrometry Chimie analytique ram Chromatographie ram Spectroscopie de masse ram Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie (DE-588)4037882-2 gnd Analytische Chemie (DE-588)4129906-1 gnd
subject_GND	(DE-588)4037882-2 (DE-588)4129906-1 (DE-588)4143413-4
title	Mass spectrometry
title_auth	Mass spectrometry
title_exact_search	Mass spectrometry
title_full	Mass spectrometry author: James Barker
title_fullStr	Mass spectrometry author: James Barker
title_full_unstemmed	Mass spectrometry author: James Barker
title_old	Davis, Reg Mass spectrometry
title_short	Mass spectrometry
title_sort	mass spectrometry
topic	Chimie analytique ram Chromatographie ram Spectroscopie de masse ram Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie (DE-588)4037882-2 gnd Analytische Chemie (DE-588)4129906-1 gnd
topic_facet	Chimie analytique Chromatographie Spectroscopie de masse Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie Analytische Chemie Aufsatzsammlung Matériel didactique
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT barkerjames massspectrometry

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