Mass spectrometry:
Gespeichert in:
| Vorheriger Titel: | Davis, Reg Mass spectrometry |
|---|---|
| 1. Verfasser: | |
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
1999
|
| Ausgabe: | 2. ed. |
| Schriftenreihe: | Analytical chemistry by open learning
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | XXII, 509 S. Ill., graph. Darst. |
| ISBN: | 0471967629 0471967645 |
Internformat
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Datensatz im Suchindex
| _version_ | 1804127099633532928 |
|---|---|
| adam_text | MASS SPECTROMETRY ANALYTICAL CHEMISTRY BY OPEN LEARNING SECOND EDITION
AUTHOR: JAMES BARKER UNIVERSITY OF GREENWICH EDITOR: DAVID J. ANDO
UNIVERSITY OF GREENWICH AUTHORS OF FIRST EDITION: REGINALD DAVIS
UNIVERSITY OF KINGSTON MARTIN J. FREARSON UNIVERSITY OF HERTFORDSHIRE
PUBLISHED ON BEHALF OF ACOL (UNIVERSITY OF GREENWICH) BY JOHN WILEY &
SONS CHICHESTER * NEW YORK * BRISBANE * SINGAPORE * TORONTO CONTENTS
STUDY GUIDE XV SUPPORTING PRACTICAL WORK XVII BIBLIOGRAPHY XIX
ACKNOWLEDGEMENTS XXI 1. INTRODUCTION 1 1.1 MASS SPECTROMETRY: ITS
CONCEPTS AND BEGINNINGS . . . . 1 1.2 IONISATION AND FRAGMENTATION 2
1.2.1 IONISATION 2 1.2.2 FRAGMENTATION 6 1.2.3 RULES FOR ASSIGNMENT OF
FRAGMENTS 9 1.2.4 THE NITROGEN RULE 10 1.2.5 LOW-RELATIVE-ABUNDANCE
PEAKS 11 1.3 THE SIMPLE MASS SPECTRUM 11 2. ION SOURCES AND METHODS OF
IONISATION 19 2.1 IONISATION BY ELECTRON IMPACT 19 2.2 CHEMICAL
IONISATION 27 2.3 FIELD IONISATION AND FIELD DESORPTION 36 2.3.1 FIELD
IONISATION 36 2.3.2 FIELD DESORPTION 39 2.4 FAST-ATOM-BOMBARDMENT 40 2.5
PLASMA DESORPTION 45 2.6 LASER DESORPTION 45 2.7 OTHER ION SOURCES 48
2.8 METHODS FOR SAMPLE INTRODUCTION 48 3. THE MASS SPECTROMETER 55 3.1
THE MASS SPECTROMETER SYSTEM: AN OVERVIEW 55 3.2 MASS RESOLUTION 64 XI
XII ANALYTICAL CHEMISTRY BY OPEN LEARNING 3.3 DOUBLE-FOCUSING MASS
SPECTROMETER 68 3.4 QUADRUPOLE MASS ANALYSER 74 3.5 SCAN RATE 79 3.6
ION-TRAP ANALYSER 81 3.7 TIME-OF-FLIGHT (TOF) ANALYSER 82 3.8
FOURER-TRANSFORM (FT) INSTRUMENTS 84 3.9 TANDEM MASS SPECTROMETRY
(MS/MS) 90 4. ION DETECTION, DATA RECORDING AND PROCESSING 95 4.1 ION
DETECTION 95 4.1.1 ELECTRON MULTIPLIERS 95 4.1.2 FARADYCUP 98 4.1.3
OTHER TYPES OF DETECTORS 99 4.2 METHODS OF DATA RECORDING 99 4.2.3
OSCILLOSCOPE AND CHART RECORDER 99 4.2.2 COMPUTER-AIDED DATA ACQUISITION
AND PROCESSING 101 5. USE OF ISOTOPES IN MASS SPECTROMETRY 117 5.1
INTRODUCTION 117 5.2 ISOTOPE ABUNDANCES: NON-HALOGEN ISOTOPES 118 5.3
ISOTOPE ABUNDANCES: HALOGEN ISOTOPES 132 5.3.1 INTRODUCTION 132 5.3.2
CALCULATION OF CHLORINE AND BROMINE ISOTOPE RATIOS 135 5.4 AN
APPROXIMATION METHOD FOR CALCULATING RELATIVE ABUNDANCES OF CLUSTERS DUE
TO MINOR ISOTOPES 144 5.5 ISOTOPE-DILUTION MASS SPECTROMETRY 147 6.
METASTABLE IONS AND MODES OF FRAGMENTATION 153 6.1 ORIGIN OF METASTABLES
153 6.2 THE USE OF METASTABLE IONS 160 6.3 MODES OF FRAGMENTATION . 164
6.3.1 ENERGY FACTORS 164 6.3.2 STABILISATION FACTORS 166 6.3.3 BASIC
RULES CONCERNING RESONANCE STRUCTURES . 180 6.3.4 MECHANISMS OF BOND
CLEAVAGES IN MASS SPECTROMETRY 181 6.3.5 THE EVEN-ELECTRON RULE 185
CONTENTS XIII 7. TYPICAL FRAGMENTATION PATTERNS OF COMMON FUNCTIONAL
GROUPS 193 7.1 INTERPRETATION PROCEDURES 194 7.1.1 GENERAL PROCEDURE FOR
THE INTERPRETATION OF A MASS SPECTRUM 194 7.2 FRAGMENTATIONS OF ALCOHOLS
213 7.3 FRAGMENTATIONS OF ETHERS 228 7.4 FRAGMENTATIONS OF
HYDROXYBENZENES (PHENOLS) . . . . 233 7.5 FRAGMENTATIONS OF CARBONYL
COMPOUNDS 240 7.5.1 THE MCLAFFERTY REARRANGEMENT 240 7.5.2
FRAGMENTATIONS OF ALDEHYDES 245 7.5.3 FRAGMENTATIONS OF KETONES 250
7.5.4 FRAGMENTATIONS OF ESTERS 254 7.5.5 FRAGMENTATIONS OF ACIDS 258
7.5.6 FRAGMENTATIONS OF AMIDES 259 7.6 FRAGMENTATIONS OF AMINES 263 7.7
FRAGMENTATIONS OF HYDROCARBONS 270 7.8 FRAGMENTATIONS OF HALOCOMPOUNDS
279 7.9 FRAGMENTATIONS OF NITROCOMPOUNDS 285 7.10 FRAGMENTATIONS OF
HETEROCYCLIC COMPOUNDS AND SULPHUR COMPOUNDS 287 7.10.1 HETEROCYCLIC
COMPOUNDS 287 7.10.2 THIOLS 290 7.10.3 THIOETHERS (SULPHIDES) 291 7.10.4
ARYL ETHERS AND THIOPHENOLS 291 7.11 ANALYSIS OF BIOMOLECULES 295 7.11.1
PROTEIN ANALYSIS 297 8. ANALYSIS OF MIXTURES BY HYPHENATED MASS SPECTRAL
TECHNIQUES 305 8.1 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC/MS) . . 306
8.1.1 INSTRUMENTATION 306 8.1.2 DERIVATISATION 313 8.1.3 QUANTITATIVE
WORK 317 8.2 LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (LC/MS) . 320 8.2.1
INSTRUMENTATION 320 8.2.2 THERMOSPRAY (TS) INTERFACE 321 8.2.3
MOVING-BELT INTERFACE COUPLING 326 8.2.4 PARTICLE-BEAM INTERFACE
COUPLING 327 8.2.5 CONTINUOUS-FLOW FAB COUPLING 328 * XIV ANALYTICAL
CHEMISTRY BY OPEN LEARNING 8.2.6 ATMOSPHERIC-PRESSURE CHEMICAL
IONISATION (APCI) 329 8.2.7 ELECTROSPRAY (ES) AND IONSPRAY 331 8.3
TANDEM MASS SPECTROMETRY (MS/MS) 335 8.4 CHROMATOGRAPHY DATA:
ACQUISITION, RECORDING AND TREATMENT 338 8.4.1 DATA ACQUISITION 338
8.4.2 DATA RECORDING AND TREATMENT 340 9. INORGANIC MASS SPECTROMETRY 34
3 9.1 SURFACE METHODS INVOLVING MASS SPECTROMETRY . . . . 343 9.1.1
SECONDARY-ION MASS SPECTROMETRY (SIMS) . . . 343 9.1.2 ION-MICROPROBE
MASS ANALYSIS (IMPMA) AND ION-BEAM LITHOGRAPHY/MODIFICATION . . . . 344
9.1.3 LASER-ASSISTED MICROPROBE MASS ANALYSIS (LAMMA) 346 9.1.4
PARTICLE-INDUCED X-RAY/GAMMA EMISSION (PIXE/PIGE) AND RUTHERFORD
BACKSCATTERING (RBS) 348 9.1.5 GLOW-DISCHARGE MASS SPECTROMETRY (GDMS) .
. 350 9.2 ANALYSIS OF BULK SOLIDS 351 9.2.1 ACCELERATOR MASS
SPECTROMETRY (AMS) . . . . 351 9.2.2 SPARK-SOURCE MASS SPECTROMETRY 354
9.2.3 RESONANCE IONISATION MASS SPECTROMETRY (RIMS) 356 9.3 ANALYSIS OF
SOLUTIONS 356 9.3.1 INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY
(ICP-MS) 356 APPENDIX 363 1. TABLE OF ISOTOPES IN ASCENDING MASS ORDER
363 2. ISOTOPIC ABUNDANCES FOR VARIOUS ELEMENTAL COMPOSITION CHON 372
SELF-ASSESSMENT QUESTIONS AND RESPONSES 385 UNITS OF MEASUREMENT 499
INDEX 505
MASS SPECTROMETRY ANALYTICAL CHEMISTRY BY OPEN LEARNING SECOND EDITION
AUTHOR: JAMES BARKER UNIVERSITY OF GREENWICH EDITOR: DAVID J. ANDO
UNIVERSITY OF GREENWICH AUTHORS OF FIRST EDITION: REGINALD DAVIS
UNIVERSITY OF KINGSTON MARTIN J. FREARSON UNIVERSITY OF HERTFORDSHIRE
PUBLISHED ON BEHALF OF ACOL (UNIVERSITY OF GREENWICH) BY JOHN WILEY &
SONS CHICHESTER * NEW YORK * BRISBANE * SINGAPORE * TORONTO CONTENTS
STUDY GUIDE XV SUPPORTING PRACTICAL WORK XVII BIBLIOGRAPHY XIX
ACKNOWLEDGEMENTS XXI 1. INTRODUCTION 1 1.1 MASS SPECTROMETRY: ITS
CONCEPTS AND BEGINNINGS . . . . 1 1.2 IONISATION AND FRAGMENTATION 2
1.2.1 IONISATION 2 1.2.2 FRAGMENTATION 6 1.2.3 RULES FOR ASSIGNMENT OF
FRAGMENTS 9 1.2.4 THE NITROGEN RULE 10 1.2.5 LOW-RELATIVE-ABUNDANCE
PEAKS 11 1.3 THE SIMPLE MASS SPECTRUM 11 2. ION SOURCES AND METHODS OF
IONISATION 19 2.1 IONISATION BY ELECTRON IMPACT 19 2.2 CHEMICAL
IONISATION 27 2.3 FIELD IONISATION AND FIELD DESORPTION 36 2.3.1 FIELD
IONISATION 36 2.3.2 FIELD DESORPTION 39 2.4 FAST-ATOM-BOMBARDMENT 40 2.5
PLASMA DESORPTION 45 2.6 LASER DESORPTION 45 2.7 OTHER ION SOURCES 48
2.8 METHODS FOR SAMPLE INTRODUCTION 48 3. THE MASS SPECTROMETER 55 3.1
THE MASS SPECTROMETER SYSTEM: AN OVERVIEW 55 3.2 MASS RESOLUTION 64 XI
XII ANALYTICAL CHEMISTRY BY OPEN LEARNING 3.3 DOUBLE-FOCUSING MASS
SPECTROMETER 68 3.4 QUADRUPOLE MASS ANALYSER 74 3.5 SCAN RATE 79 3.6
ION-TRAP ANALYSER 81 3.7 TIME-OF-FLIGHT (TOF) ANALYSER 82 3.8
FOURER-TRANSFORM (FT) INSTRUMENTS 84 3.9 TANDEM MASS SPECTROMETRY
(MS/MS) 90 4. ION DETECTION, DATA RECORDING AND PROCESSING 95 4.1 ION
DETECTION 95 4.1.1 ELECTRON MULTIPLIERS 95 4.1.2 FARADYCUP 98 4.1.3
OTHER TYPES OF DETECTORS 99 4.2 METHODS OF DATA RECORDING 99 4.2.3
OSCILLOSCOPE AND CHART RECORDER 99 4.2.2 COMPUTER-AIDED DATA ACQUISITION
AND PROCESSING 101 5. USE OF ISOTOPES IN MASS SPECTROMETRY 117 5.1
INTRODUCTION 117 5.2 ISOTOPE ABUNDANCES: NON-HALOGEN ISOTOPES 118 5.3
ISOTOPE ABUNDANCES: HALOGEN ISOTOPES 132 5.3.1 INTRODUCTION 132 5.3.2
CALCULATION OF CHLORINE AND BROMINE ISOTOPE RATIOS 135 5.4 AN
APPROXIMATION METHOD FOR CALCULATING RELATIVE ABUNDANCES OF CLUSTERS DUE
TO MINOR ISOTOPES 144 5.5 ISOTOPE-DILUTION MASS SPECTROMETRY 147 6.
METASTABLE IONS AND MODES OF FRAGMENTATION 153 6.1 ORIGIN OF METASTABLES
153 6.2 THE USE OF METASTABLE IONS 160 6.3 MODES OF FRAGMENTATION . 164
6.3.1 ENERGY FACTORS 164 6.3.2 STABILISATION FACTORS 166 6.3.3 BASIC
RULES CONCERNING RESONANCE STRUCTURES . 180 6.3.4 MECHANISMS OF BOND
CLEAVAGES IN MASS SPECTROMETRY 181 6.3.5 THE EVEN-ELECTRON RULE 185
CONTENTS XIII 7. TYPICAL FRAGMENTATION PATTERNS OF COMMON FUNCTIONAL
GROUPS 193 7.1 INTERPRETATION PROCEDURES 194 7.1.1 GENERAL PROCEDURE FOR
THE INTERPRETATION OF A MASS SPECTRUM 194 7.2 FRAGMENTATIONS OF ALCOHOLS
213 7.3 FRAGMENTATIONS OF ETHERS 228 7.4 FRAGMENTATIONS OF
HYDROXYBENZENES (PHENOLS) . . . . 233 7.5 FRAGMENTATIONS OF CARBONYL
COMPOUNDS 240 7.5.1 THE MCLAFFERTY REARRANGEMENT 240 7.5.2
FRAGMENTATIONS OF ALDEHYDES 245 7.5.3 FRAGMENTATIONS OF KETONES 250
7.5.4 FRAGMENTATIONS OF ESTERS 254 7.5.5 FRAGMENTATIONS OF ACIDS 258
7.5.6 FRAGMENTATIONS OF AMIDES 259 7.6 FRAGMENTATIONS OF AMINES 263 7.7
FRAGMENTATIONS OF HYDROCARBONS 270 7.8 FRAGMENTATIONS OF HALOCOMPOUNDS
279 7.9 FRAGMENTATIONS OF NITROCOMPOUNDS 285 7.10 FRAGMENTATIONS OF
HETEROCYCLIC COMPOUNDS AND SULPHUR COMPOUNDS 287 7.10.1 HETEROCYCLIC
COMPOUNDS 287 7.10.2 THIOLS 290 7.10.3 THIOETHERS (SULPHIDES) 291 7.10.4
ARYL ETHERS AND THIOPHENOLS 291 7.11 ANALYSIS OF BIOMOLECULES 295 7.11.1
PROTEIN ANALYSIS 297 8. ANALYSIS OF MIXTURES BY HYPHENATED MASS SPECTRAL
TECHNIQUES 305 8.1 GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC/MS) . . 306
8.1.1 INSTRUMENTATION 306 8.1.2 DERIVATISATION 313 8.1.3 QUANTITATIVE
WORK 317 8.2 LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY (LC/MS) . 320 8.2.1
INSTRUMENTATION 320 8.2.2 THERMOSPRAY (TS) INTERFACE 321 8.2.3
MOVING-BELT INTERFACE COUPLING 326 8.2.4 PARTICLE-BEAM INTERFACE
COUPLING 327 8.2.5 CONTINUOUS-FLOW FAB COUPLING 328 * XIV ANALYTICAL
CHEMISTRY BY OPEN LEARNING 8.2.6 ATMOSPHERIC-PRESSURE CHEMICAL
IONISATION (APCI) 329 8.2.7 ELECTROSPRAY (ES) AND IONSPRAY 331 8.3
TANDEM MASS SPECTROMETRY (MS/MS) 335 8.4 CHROMATOGRAPHY DATA:
ACQUISITION, RECORDING AND TREATMENT 338 8.4.1 DATA ACQUISITION 338
8.4.2 DATA RECORDING AND TREATMENT 340 9. INORGANIC MASS SPECTROMETRY 34
3 9.1 SURFACE METHODS INVOLVING MASS SPECTROMETRY . . . . 343 9.1.1
SECONDARY-ION MASS SPECTROMETRY (SIMS) . . . 343 9.1.2 ION-MICROPROBE
MASS ANALYSIS (IMPMA) AND ION-BEAM LITHOGRAPHY/MODIFICATION . . . . 344
9.1.3 LASER-ASSISTED MICROPROBE MASS ANALYSIS (LAMMA) 346 9.1.4
PARTICLE-INDUCED X-RAY/GAMMA EMISSION (PIXE/PIGE) AND RUTHERFORD
BACKSCATTERING (RBS) 348 9.1.5 GLOW-DISCHARGE MASS SPECTROMETRY (GDMS) .
. 350 9.2 ANALYSIS OF BULK SOLIDS 351 9.2.1 ACCELERATOR MASS
SPECTROMETRY (AMS) . . . . 351 9.2.2 SPARK-SOURCE MASS SPECTROMETRY 354
9.2.3 RESONANCE IONISATION MASS SPECTROMETRY (RIMS) 356 9.3 ANALYSIS OF
SOLUTIONS 356 9.3.1 INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY
(ICP-MS) 356 APPENDIX 363 1. TABLE OF ISOTOPES IN ASCENDING MASS ORDER
363 2. ISOTOPIC ABUNDANCES FOR VARIOUS ELEMENTAL COMPOSITION CHON 372
SELF-ASSESSMENT QUESTIONS AND RESPONSES 385 UNITS OF MEASUREMENT 499
INDEX 505
|
| any_adam_object | 1 |
| author | Barker, James |
| author_facet | Barker, James |
| author_role | aut |
| author_sort | Barker, James |
| author_variant | j b jb |
| building | Verbundindex |
| bvnumber | BV012460868 |
| classification_rvk | VG 9800 |
| classification_tum | CHE 254f |
| ctrlnum | (OCoLC)300071121 (DE-599)BVBBV012460868 |
| dewey-full | 543.65 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543.65 |
| dewey-search | 543.65 |
| dewey-sort | 3543.65 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | 2. ed. |
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content Matériel didactique |
| genre_facet | Aufsatzsammlung Matériel didactique |
| id | DE-604.BV012460868 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:27:58Z |
| institution | BVB |
| isbn | 0471967629 0471967645 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008455695 |
| oclc_num | 300071121 |
| open_access_boolean | |
| owner | DE-20 DE-91G DE-BY-TUM DE-29T DE-522 DE-634 |
| owner_facet | DE-20 DE-91G DE-BY-TUM DE-29T DE-522 DE-634 |
| physical | XXII, 509 S. Ill., graph. Darst. |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Wiley |
| record_format | marc |
| series2 | Analytical chemistry by open learning |
| spelling | Barker, James Verfasser aut Mass spectrometry author: James Barker 2. ed. Chichester [u.a.] Wiley 1999 XXII, 509 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Analytical chemistry by open learning Chimie analytique ram Chromatographie ram Spectroscopie de masse ram Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie (DE-588)4037882-2 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Matériel didactique Massenspektrometrie (DE-588)4037882-2 s Analytische Chemie (DE-588)4129906-1 s 1\p DE-604 Ersatz von Davis, Reg Mass spectrometry GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Barker, James Mass spectrometry Chimie analytique ram Chromatographie ram Spectroscopie de masse ram Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie (DE-588)4037882-2 gnd Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4037882-2 (DE-588)4129906-1 (DE-588)4143413-4 |
| title | Mass spectrometry |
| title_auth | Mass spectrometry |
| title_exact_search | Mass spectrometry |
| title_full | Mass spectrometry author: James Barker |
| title_fullStr | Mass spectrometry author: James Barker |
| title_full_unstemmed | Mass spectrometry author: James Barker |
| title_old | Davis, Reg Mass spectrometry |
| title_short | Mass spectrometry |
| title_sort | mass spectrometry |
| topic | Chimie analytique ram Chromatographie ram Spectroscopie de masse ram Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie (DE-588)4037882-2 gnd Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Chimie analytique Chromatographie Spectroscopie de masse Chemistry, Analytic Programmed instruction Mass spectrometry Programmed instruction Massenspektrometrie Analytische Chemie Aufsatzsammlung Matériel didactique |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008455695&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT barkerjames massspectrometry |
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