Principles of protein X-ray crystallography:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
New York [u.a.]
Springer
1999
|
| Ausgabe: | 2. ed. |
| Schriftenreihe: | Springer advanced texts in chemistry
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturverz. S. 323 - 330 |
| Beschreibung: | XV, 341 S. Ill., graph. Darst. |
| ISBN: | 0387985875 |
Internformat
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| 100 | 1 | |a Drenth, Jan |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Principles of protein X-ray crystallography |c Jan Drenth |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a New York [u.a.] |b Springer |c 1999 | |
| 300 | |a XV, 341 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Springer advanced texts in chemistry | |
| 500 | |a Literaturverz. S. 323 - 330 | ||
| 650 | 7 | |a Eiwitten |2 gtt | |
| 650 | 7 | |a Kristallografie |2 gtt | |
| 650 | 4 | |a Crystallography, X-Ray |x methods | |
| 650 | 4 | |a Proteins |x Analysis | |
| 650 | 4 | |a Proteins |x analysis | |
| 650 | 4 | |a X-ray crystallography | |
| 650 | 0 | 7 | |a Proteine |0 (DE-588)4076388-2 |2 gnd |9 rswk-swf |
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-008454694 | |
Datensatz im Suchindex
| _version_ | 1828745194429743105 |
|---|---|
| adam_text |
CONTENTS
SERIES
PREFACE
V
PREFACE
TO
THE
SECOND
EDITION
VII
PREFACE
TO
THE
FIRST
EDITION
IX
CHAPTER
1
CRYSTALLIZING
A
PROTEIN
1
1.1
INTRODUCTION
1
1.2
PRINCIPLES
OF
PROTEIN
CRYSTALLIZATION
1
1.3
CRYSTALLIZATION
TECHNIQUES
4
1.4
CRYSTALLIZATION
OF
LYSOZYME
8
1.5
A
PRELIMINARY
NOTE
ON
CRYSTALS
11
1.6
PREPARATION
FOR
AN
X-RAY
DIFFRACTION
EXPERIMENT
12
1.7
CRYOCOOLING
16
1.8
NOTES
18
SUMMARY
21
CHAPTER
2
X-RAY
SOURCES
AND
DETECTORS
22
2.1
INTRODUCTION
22
2.2
X-RAY
SOURCES
22
2.3
MONOCHROMATORS
32
2.4
INTRODUCTION
TO
CAMERAS
AND
DETECTORS
34
2.5
DETECTORS
35
2.6
THE
ROTATION
(OSCILLATION)
INSTRUMENT
41
2.7
ELECTRONIC
AREA
DETECTORS
47
SUMMARY
49
XII
CONTENTS
CHAPTER
3
CRYSTALS
50
3.1
INTRODUCTION
50
3.2
SYMMETRY
55
3.3
POSSIBLE
SYMMETRY
FOR
PROTEIN
CRYSTALS
58
3.4
COORDINATE
TRIPLETS:
GENERAL
AND
SPECIAL
POSITIONS
62
3.5
ASYMMETRIC
UNIT
63
3.6
POINT
GROUPS
64
3.7
CRYSTAL
SYSTEMS
64
3.8
RADIATION
DAMAGE
66
3.9
CHARACTERIZATION
OF
THE
CRYSTALS
67
SUMMARY
69
CHAPTER
4
THE
THEORY
OF
X-RAY
DIFFRACTION
BY
A
CRYSTAL
70
4.1
INTRODUCTION
70
4.2
WAVES
AND
THEIR
ADDITION
71
4.3
A
SYSTEM
OF
TWO
ELECTRONS
74
4.4
SCATTERING
BY
AN
ATOM
78
4.5
SCATTERING
BY
A
UNIT
CELL
80
4.6
SCATTERING
BY
A
CRYSTAL
81
4.7
DIFFRACTION
CONDITIONS
82
4.8
RECIPROCAL
LATTICE
AND
EWALD
CONSTRUCTION
84
4.9
THE
TEMPERATURE
FACTOR
89
4.10
CALCULATION
OF
THE
ELECTRON
DENSITY
P
(X
Y
Z)
92
4.11
COMPARISON
OF
F(H
K
I)
AND
F(A
K.
I
)
98
4.12
SYMMETRY
IN
THE
DIFFRACTION
PATTERN
99
4.13
INTEGRAL
REFLECTION
CONDITIONS
FOR
CENTERED
LATTICES
103
4.14
THE
INTENSITY
DIFFRACTED
BY
A
CRYSTAL
103
4.15
SCATTERING
BY
A
PLANE
OF
ATOMS
111
4.16
CHOICE
OF
WAVELENGTH,
SIZE
OF
UNIT
CELL,
AND
CORRECTION
OF
THE
DIFFRACTED
INTENSITY
113
SUMMARY
115
CHAPTER
5
AVERAGE
REFLECTION
INTENSITY
AND
DISTRIBUTION
OF
STRUCTURE
FACTOR
DATA
11
7
5.1
INTRODUCTION
117
5.2
AVERAGE
INTENSITY;
WILSON
PLOTS
120
5.3
THE
DISTRIBUTION
OF
STRUCTURE
FACTORS
F
AND
STRUCTURE
FACTOR
AMPLITUDES
IFI
122
SUMMARY
124
CHAPTER
6
SPECIAL
FORMS
OF
THE
STRUCTURE
FACTOR
125
6.1
INTRODUCTION
125
6.2
THE
UNITARY
STRUCTURE
FACTOR
125
6.3
THE
NORMALIZED
STRUCTURE
FACTOR
126
SUMMARY
128
CONTENTS
XIII
CHAPTER
7
THE
SOLUTION
OF
THE
PHASE
PROBLEM
BY
THE
ISOMORPHOUS
REPLACEMENT
METHOD
129
7.1
INTRODUCTION
129
7.2
THE
PATTERSON
FUNCTION
130
7.3
THE
ISOMORPHOUS
REPLACEMENT
METHOD
139
7.4
EFFECT
OF
HEAVY
ATOMS
ON
X-RAY
INTENSITIES
145
7.5
DETERMINATION
OF
THE
HEAVY
ATOM
PARAMETERS
FROM
CENTROSYMMETRIC
PROJECTIONS
149
7.6
PARAMETERS
OF
HEAVY
ATOMS
DERIVED
FROM
ACENTRIC
REFLECTIONS
151
7.7
THE
DIFFERENCE
FOURIER
SUMMATION
152
7.8
ANOMALOUS
SCATTERING
155
7.9
THE
ANOMALOUS
PATTERSON
SUMMATION
159
7.10
ONE
COMMON
ORIGIN
FOR
ALL
DERIVATIVES
161
7.11
REFINEMENT
OF
THE
HEAVY
ATOM
PARAMETERS
USING
PRELIMINARY
PROTEIN
PHASE
ANGLES
165
7.12
PROTEIN
PHASE
ANGLES
168
7.13
THE
REMAINING
ERROR
IN
THE
BEST
FOURIER
MAP
174
7.14
THE
SINGLE
ISOMORPHOUS
REPLACEMENT
(SIR)
METHOD
178
SUMMARY
179
CHAPTER
8
PHASE
IMPROVEMENT
180
8.1
INTRODUCTION
180
8.2
THE
OMIT
MAP
WITH
AND
WITHOUT
SIM
WEIGHTING
181
8.3
SOLVENT
FLATTENING
188
8.4
NONCRYSTALLOGRAPHIC
SYMMETRY
AND
MOLECULAR
AVERAGING
194
8.5
HISTOGRAM
MATCHING
198
8.6
WARP:
WEIGHTED
AVERAGING
OF
MULTIPLE-REFINED
DUMMY
ATOMIC
MODELS
199
8.7
FURTHER
CONSIDERATIONS
CONCERNING
DENSITY
MODIFICATION
200
SUMMARY
202
CHAPTER
9
ANOMALOUS
SCATTERING
IN
THE
DETERMINATION
OF
THE
PROTEIN
PHASE
ANGLES
AND
THE
ABSOLUTE
CONFIGURATION
203
9.1
INTRODUCTION
203
9.2
PROTEIN
PHASE
ANGLE
DETERMINATION
WITH
ANOMALOUS
SCATTERING
203
9.3
IMPROVEMENT
OF
PROTEIN
PHASE
ANGLES
WITH
ANOMALOUS
SCATTERING
205
9.4
THE
DETERMINATION
OF
THE
ABSOLUTE
CONFIGURATION
207
9.5
MULTIPLE
WAVELENGTH
ANOMALOUS
DISPERSION
(MAD)
209
SUMMARY
218
CHAPTER
10
MOLECULAR
REPLACEMENT
219
10.1
INTRODUCTION
219
10.2
THE
ROTATION
FUNCTION
220
10.3
THE
TRANSLATION
FUNCTION
229
SUMMARY
243
XIV
CONTENTS
CHAPTER
11
DIRECT
METHODS
244
11.1
INTRODUCTION
244
11.2
SHAKE-AND-BAKE
244
11.3
THE
PRINCIPLE
OF
MAXIMUM
ENTROPY
249
SUMMARY
252
CHAPTER
12
LAUE
DIFFRACTION
253
12.1
INTRODUCTION
253
12.2
THE
ACCESSIBLE
REGION
OF
RECIPROCAL
SPACE
254
12.3
THE
MULTIPLE
PROBLEM
255
12.4
UNSCRAMBLING
OF
MULTIPLE
INTENSITIES
256
12.5
THE
SPATIAL
OVERLAP
PROBLEM
257
12.6
WAVELENGTH
NORMALIZATION
257
SUMMARY
259
CHAPTER
13
REFINEMENT
OF
THE
MODEL
STRUCTURE
260
13.1
INTRODUCTION
260
13.2
THE
MATHEMATICS
OF
REFINEMENT
263
13.3
THE
PRINCIPLE
OF
THE
FAST
FOURIER
TRANSFORM
(FFT)
METHOD
275
13.4
SPECIFIC
REFINEMENT
METHODS
277
SUMMARY
291
CHAPTER
14
THE
COMBINATION
OF
PHASE
INFORMATION
292
14.1
INTRODUCTION
292
14.2
PHASE
INFORMATION
FROM
ISOMORPHOUS
REPLACEMENT
293
14.3
PHASE
INFORMATION
FROM
ANOMALOUS
SCATTERING
295
14.4
PHASE
INFORMATION
FROM
MAD
296
14.5
PHASE
INFORMATION
FROM
PARTIAL
STRUCTURE
DATA,
SOLVENT
FLATTENING,
AND
MOLECULAR
AVERAGING
297
SUMMARY
297
CHAPTER
15
CHECKING
FOR
GROSS
ERRORS
AND
ESTIMATING
THE
ACCURACY
OF
THE
STRUCTURAL
MODEL
298
15.1
INTRODUCTION
298
15.2
R-FACTORS
298
15.3
THE
RAMACHANDRAN
PLOT
300
15.4
STEREOCHEMISTRY
CHECK
302
15.5
THE
3D-1D
PROFILE
METHOD
303
15.6
QUANTITATIVE
ESTIMATION
OF
THE
COORDINATE
ERROR
IN
THE
FINAL
MODEL
305
SUMMARY
310
CONTENTS
XV
APPENDIX
1
A
COMPILATION
OF
EQUATIONS
FOR
CALCULATING
ELECTRON
DENSITY
MAPS
311
APPENDIX
2
A
COMPILATION
OF
RELIABILITY
INDICES
315
APPENDIX
3
THE
VARIATION
IN
THE
INTENSITY
OF
X-RAY
RADIATION
321
REFERENCES
323
INDEX
331 |
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| author | Drenth, Jan |
| author_facet | Drenth, Jan |
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| dewey-search | 547/.75046 |
| dewey-sort | 3547 575046 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Biologie Chemie |
| edition | 2. ed. |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2025-04-07T12:02:03Z |
| institution | BVB |
| isbn | 0387985875 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008454694 |
| oclc_num | 39322756 |
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| spelling | Drenth, Jan Verfasser aut Principles of protein X-ray crystallography Jan Drenth 2. ed. New York [u.a.] Springer 1999 XV, 341 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Springer advanced texts in chemistry Literaturverz. S. 323 - 330 Eiwitten gtt Kristallografie gtt Crystallography, X-Ray methods Proteins Analysis Proteins analysis X-ray crystallography Proteine (DE-588)4076388-2 gnd rswk-swf Röntgenstrukturanalyse (DE-588)4137203-7 gnd rswk-swf Proteine (DE-588)4076388-2 s Röntgenstrukturanalyse (DE-588)4137203-7 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008454694&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Drenth, Jan Principles of protein X-ray crystallography Eiwitten gtt Kristallografie gtt Crystallography, X-Ray methods Proteins Analysis Proteins analysis X-ray crystallography Proteine (DE-588)4076388-2 gnd Röntgenstrukturanalyse (DE-588)4137203-7 gnd |
| subject_GND | (DE-588)4076388-2 (DE-588)4137203-7 |
| title | Principles of protein X-ray crystallography |
| title_auth | Principles of protein X-ray crystallography |
| title_exact_search | Principles of protein X-ray crystallography |
| title_full | Principles of protein X-ray crystallography Jan Drenth |
| title_fullStr | Principles of protein X-ray crystallography Jan Drenth |
| title_full_unstemmed | Principles of protein X-ray crystallography Jan Drenth |
| title_short | Principles of protein X-ray crystallography |
| title_sort | principles of protein x ray crystallography |
| topic | Eiwitten gtt Kristallografie gtt Crystallography, X-Ray methods Proteins Analysis Proteins analysis X-ray crystallography Proteine (DE-588)4076388-2 gnd Röntgenstrukturanalyse (DE-588)4137203-7 gnd |
| topic_facet | Eiwitten Kristallografie Crystallography, X-Ray methods Proteins Analysis Proteins analysis X-ray crystallography Proteine Röntgenstrukturanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008454694&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT drenthjan principlesofproteinxraycrystallography |