Organic structure analysis:
"Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage,...
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
Oxford Univ. Press
1998
|
| Schriftenreihe: | Topics in organic chemistry
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Zusammenfassung: | "Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage, it is the only text that emphasizes strategies, interpretation, modern techniques, and problem solving. The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements." "Organic Structure Analysis adopts a practical approach to the subject which emphasizes building experience; the authors recognize that a combination of problem solving, access to data from models, and understanding the rules of spectral interpretation helps students to build expertise in structure determination from spectra. It outlines elements of theory, but with an emphasis on those directly relevant to spectral interpretation. The text is divided into three major sections: the first section provides extensive coverage of each of the individual methods, the second section illustrates how the strategies of organic structure analysis are actually applied in ten problems whose solutions are provided, and the third section consists of fifty unsolved problems which range from simple monofunctional compounds to complex natural products."--BOOK JACKET. |
| Beschreibung: | XXIV, 552 S. Ill., zahlr. graph. Darst. |
| ISBN: | 0195101022 |
Internformat
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| 490 | 0 | |a Topics in organic chemistry | |
| 520 | 1 | |a "Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage, it is the only text that emphasizes strategies, interpretation, modern techniques, and problem solving. The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements." "Organic Structure Analysis adopts a practical approach to the subject which emphasizes building experience; the authors recognize that a combination of problem solving, access to data from models, and understanding the rules of spectral interpretation helps students to build expertise in structure determination from spectra. It outlines elements of theory, but with an emphasis on those directly relevant to spectral interpretation. The text is divided into three major sections: the first section provides extensive coverage of each of the individual methods, the second section illustrates how the strategies of organic structure analysis are actually applied in ten problems whose solutions are provided, and the third section consists of fifty unsolved problems which range from simple monofunctional compounds to complex natural products."--BOOK JACKET. | |
| 650 | 7 | |a Espectroscopia de massa |2 larpcal | |
| 650 | 7 | |a Espectroscopia ressonancia magnetica nuclear |2 larpcal | |
| 650 | 7 | |a Espectroscopia |2 larpcal | |
| 650 | 7 | |a Estrutura molecular (quimica teorica) |2 larpcal | |
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Datensatz im Suchindex
| _version_ | 1804127065604096000 |
|---|---|
| adam_text | ORGANIC STRUCTURE ANALYSIS PHILLIP CREWS JAIME RODRIGUEZ MARCEL JASPARS
UNIVERSITY OF CALIFORNIA, SANTA CRUZ NEW YORK OXFORD OXFORD UNIVERSITY
PRESS 1998 CONTENTS SCHEINES, FIGURES, CHARTS, AND TABLES XI PREFACE XXI
C H A P T E R I USING SPECTROSCOPIC DATA IN ORGANIC STRUCTURE ANALYSIS I
1.1 A GLIMPSE OF THE SPECTROMETRIC METHODS IN COMMON USE 1 1.2
CHARACTERISTICS OF THE IMPORTANT METHODS 4 1.3 STEPS IN ESTABLISHING A
MOLECULAR STRUCTURE 8 1.4 MOLECULAR FORMULA (MF) AND UNSATURATION NUMBER
(UN) 10 1.5 SUBSTRUCTURES, WORKING STRUCTURES, AND COUNTING RINGS 11 1.6
LIMITATIONS OF SPECTROSCOPIC DATA IN STRUCTURE ANALYSIS 14 SOURCES FOR
FURTHER READING 17 PROBLEMS 17 MORE CHALLENGING PROBLEMS 21 C H A P T E
R 2 INTRODUCTION TO NUCLEAR MAGNETIC RESONANCE 23 2.1 A GLIMPSE OF THE
NMR PHENOMENON 24 2.2 COMMONLY STUDIED NUCLEI 28 2.3 OBTAINING AN NMR
SPECTRUM 31 2.4 MAGNETIC SHIELDING 35 2.5 RELAXATION EFFECTS 36 2.6
EFFECT OF RELAXATION AND NOE ON PEAK INTENSITIES 38 2.7 ELECTRIC
QUADRUPOLE EFFECTS 39 2.8 MEASUREMENT AND PRESENTATION OF DATA 42 2.9
SAMPLE PREPARATION AND SAMPLE SIZE 44 2.10 COMMON IMPURITIES IN NMR
SPECTRA 46 SOURCES FOR FURTHER READING 48 PROBLEMS 49 MORE CHALLENGING
PROBLEMS 51 VI CONTENTS C H A P T E R 3 INTERPRETATION AND USE OF PROTON
AND CARBON CHEMICAL SHIFTS 53 3.1 A GLIMPSE OF CHEMICAL SHIFTS AND PEAK
AREAS 55 3.2 TERMS AND CONVENTIONS 55 3.3 FACTORS THAT DETERMINE
CHEMICAL SHIFTS 58 3.4 CHEMICAL SHIFT POSITIONS OF H/ 13 C ATTACHED TO
COMMON FUNCTIONAL GROUPS 61 3.5 CHEMICAL SHIFT EQUIVALENCE 61 3.6
CHARACTERISTIC CHEMICAL SHIFTS FOR DIFFERENT PROTONS AND CARBONS 68 3.7
A MORE DETAILED VIEW OF USING CHEMICAL SHIFTS AND PEAK AREAS 95 SOURCES
FOR FURTHER READING 97 PROBLEMS 98 MORE CHALLENGING PROBLEMS 101 C H A P
T E R 4 INTERPRETATION AND USE OF PROTON OR CARBON COUPLING CONSTANTS
103 4.1 A GLIMPSE OF COUPLING CONSTANTS 104 4.2 FIRST-ORDER SPECTRA AND
THE N+1 RULE 105 4.3 TERMS AND CONVENTIONS 111 4.4 COMMON COUPLED SPIN
SYSTEMS 111 4.5 MAGNETIC NONEQUIVALENCE 125 4.6 USING COUPLING CONSTANTS
TO MAKE ASSIGNMENTS 128 4.7 COUPLING CONSTANT VALUES FOR DIFFERENT
CARBON AND PROTON TYPES 134 4.8 WAYS TO SIMPLIFY OR ELIMINATE COUPLING
EFFECTS 143 4.9 THE NUCLEAR OVERHAUSER EFFECT 149 4.10 ADDITIONAL WAYS
TO OBTAIN J VALUES 151 SOURCES FOR FURTHER READING 152 PROBLEMS 153 MORE
CHALLENGING PROBLEMS 163 C H A P T E R 5 MULTIPLE-PULSE AND
MULTIDIMENSIONAL NMR TECHNIQUES 167 5.1 A GLIMPSE OF MULTIPLE-PULSE NMR
METHODS 168 5.2 ELEMENTS OF MULTIPLE-PULSE NMR 169 5.3 ONE-DIMENSIONAL
NMR TECHNIQUES 175 5.4 TWO-DIMENSIONAL NMR TECHNIQUES 181 5.5 ASSIGNING
SPECTRA USING TWO-DIMENSIONAL NMR DATA 184 5.6 DETERMINING AN UNKNOWN
STRUCTURE USING TWO-DIMENSIONAL NMR DATA 195 CONTENTS VII 5.7 LONG-RANGE
TWO-DIMENSIONAL NMR METHODS 196 5.8 COMPARISON OF TWO-DIMENSIONAL
STRATEGIES 203 5.9 FUTURE PROSPECTS IN MULTIDIMENSIONAL NMR 204 SOURCES
FOR FURTHER READING 207 PROBLEMS 208 MORE CHALLENGING PROBLEMS 221
CHAPTER 6 CORE TECHNIQUES OF MASS SPECTROMETRY: INTERPRETATION AND USE
OF DATA 229 6.1 A GLIMPSE OF MASS SPECTROMETRY 230 6.2 MEASUREMENT AND
PRESENTATION OF DATA 233 6.3 INTERPRETING A LOW RESOLUTION ELECTRON
IMPACT MASS SPECTRUM 236 6.4 MOLECULAR FORMULAS FROM MOLECULAR ION PEAKS
237 6.5 FRAGMENTATION PROCESSES 242 6.6 IDENTIFICATION OF FUNCTIONALITY
FROM FRAGMENTATION PROCESSES 251 6.7 EVALUATION OF FRAGMENTATION IN THE
[M*1] + TO [M*29] + REGION 269 6.8 OTHER WAYS TO OBTAIN MASS SPECTRA 269
SOURCES FOR FURTHER READING 270 PROBLEMS 271 MORE CHALLENGING PROBLEMS
278 CHAPTER 7 ADDITIONAL TECHNIQUES OF MASS SPECTROMETRY 281 7.1 A
GLIMPSE OF CONTEMPORARY MASS SPECTROMETRY 282 7.2 MOLECULAR FORMULAS AND
MOLECULAR ION PEAKS REVISITED 283 7.3 DIFFERENT IONIZATION TECHNIQUES IN
MASS SPECTROMETRY 286 7.4 DIFFERENT TECHNIQUES FOR ANALYZING IONS IN
MASS SPECTROMETRY 297 7.5 TANDEM MASS SPECTROMETRY 301 7.6 ANALYSIS OF
MIXTURES 304 1.1 DEREPLICATIO N OF KNOWN COMPOUNDS BY MASS SPECTROMETRY
304 7.8 FUTURE PROSPECTS 306 SOURCES FOR FURTHER READING 308 PROBLEMS
309 MORE CHALLENGING PROBLEMS 314 CHAPTER 8 INFRARED SPECTROSCOPY 317
8.1 A GLIMPSE OF INFRARED SPECTROSCOPY 318 8.2 MEASUREMENT AND
PRESENTATION OF DATA 318 VIII CONTENTS 8.3 THE FUNDAMENTALS 320 8.4
IDENTIFYING FUNCTIONAL GROUPS 324 8.5 INTERPRETED INFRARED SPECTRA 334
SOURCES FOR FURTHER READING 343 PROBLEMS 343 MORE CHALLENGING PROBLEMS
347 C H A P T E R 9 OPTICAL AND CHIROPTICAL TECHNIQUES: ULTRAVIOLET
SPECTROSCOPY 349 9.1 A GLIMPSE OF ULTRAVIOLET SPECTROSCOPY 350 9.2
MEASUREMENT AND PRESENTATION OF DATA 352 9.3 THE FUNDAMENTALS FOR
INTERPRETING SPECTRA 353 9.4 IDENTIFYING FUNCTIONAL GROUPS 355 9.5 THE
BEHAVIOR OF CHIRAL CHROMOPHORES ORD-CD 363 9.6 OTHER WAYS TO EXAMINE
CHIRAL CHROMOPHORES 369 9.7 THE EXCITON CHIRALITY METHOD 370 SOURCES FOR
FURTHER READING 577 PROBLEMS 371 MORE CHALLENGING PROBLEMS 373 C H A P T
E R 10 STRATEGIES OF DETERMINING STRUCTURE AND STEREOCHEMISTRY:
SPECTROSCOPIC DATA TRANSLATED INTO STRUCTURES 375 10.1 A GLIMPSE OF THE
COMBINED USE OF SPECTROSCOPIC DATA 376 10.2 THE STRATEGIES OF
DETERMINING STRUCTURE AND STEREOCHEMISTRY 376 10.3 WORKED EXAMPLES OF
DERIVING STRUCTURES FROM SPECTROSCOPIC DATA 378 USING 13 C NMR DATA TO
CORRECT THE LABEL OF UNKNOWN A, FIGURE 10.1 378 USING !H NMR DATA,
UNKNOWN B, FIGURE 10.2 381 USING 13 C NMR DATA, UNKNOWN C, FIGURE 10.3
384 COMBINING H AND ,3 C NMR DATA, UNKNOWN D, FIGURE 10.4 387 USING UV
DATA, UNKNOWN E, FIGURE 10.5 389 USING NOE H NMR DATA, UNKNOWN F,
FIGURE 10.6 389 COMBINING MS AND NMR DATA, UNKNOWN G, FIGURE 10.7 391
EMPHASIS ON J H- H COSY NMR DATA, UNKNOWN H, FIGURE 10.8 394 EMPHASIS ON
COMBINING 13 C, APT, AND INADEQUATE NMR DATA, UNKNOWN I, FIGURE 10.9 398
EMPHASIS ON H- 13 C COSY NMR DATA, UNKNOWN J, GUAIAZULENE, FIGURE 10.10
402 CONTENTS IX C H A P T E R II PROBLEMS IN ORGANIC STRUCTURE ANALYSIS
407 11.1 A GLIMPSE OF THE SCOPE OF THE FIFTY UNKNOWNS 407 11.2 USING THE
SPECTRA, ACCOMPANYING INFORMATION, AND OTHER RESOURCES 408 SIMPLE
MONOFUNCTIONAL COMPOUNDS 409 MORE CHALLENGING MONO OR HIGHER
FUNCTIONALIZED COMPOUNDS 440 EXTREMELY CHALLENGING POLYFUNCTIONALIZED
COMPOUNDS 476 COMPLEX NATURAL PRODUCTS 486 INDEX OF MOLECULAR FORMULAS
AND STRUCTURES 526 APPENDIX A: COLLECTIONS OF SPECTRA OR DATA TABLES
APPENDIX B: SHAPE OF MS CLUSTERS APPENDIX C: CAS REGISTRY NUMBERS FOR
UNKNOWNS APPENDIX D: GLOSSARY AND ABBREVIATIONS INDEX 531 533 535 539
547
|
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| author | Crews, Phillip 1943- Rodríguez, Jaime 1963- Jaspars, Marcel 1966- |
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| id | DE-604.BV012427836 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:27:25Z |
| institution | BVB |
| isbn | 0195101022 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008433368 |
| oclc_num | 37625549 |
| open_access_boolean | |
| owner | DE-703 DE-29T DE-19 DE-BY-UBM |
| owner_facet | DE-703 DE-29T DE-19 DE-BY-UBM |
| physical | XXIV, 552 S. Ill., zahlr. graph. Darst. |
| publishDate | 1998 |
| publishDateSearch | 1998 |
| publishDateSort | 1998 |
| publisher | Oxford Univ. Press |
| record_format | marc |
| series2 | Topics in organic chemistry |
| spelling | Crews, Phillip 1943- Verfasser (DE-588)140821503 aut Organic structure analysis Phillip Crews ; Jaime Rodríguez ; Marcel Jaspars New York [u.a.] Oxford Univ. Press 1998 XXIV, 552 S. Ill., zahlr. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Topics in organic chemistry "Organic Structure Analysis is an ideal text for upper-level undergraduate and first-year graduate courses in organic spectroscopy. It provides students with the background necessary to effectively apply spectroscopic data in establishing features of molecular structure. Unique in its coverage, it is the only text that emphasizes strategies, interpretation, modern techniques, and problem solving. The text's major aim is to show how spectra can be efficiently examined in order to identify a molecule's major structural elements." "Organic Structure Analysis adopts a practical approach to the subject which emphasizes building experience; the authors recognize that a combination of problem solving, access to data from models, and understanding the rules of spectral interpretation helps students to build expertise in structure determination from spectra. It outlines elements of theory, but with an emphasis on those directly relevant to spectral interpretation. The text is divided into three major sections: the first section provides extensive coverage of each of the individual methods, the second section illustrates how the strategies of organic structure analysis are actually applied in ten problems whose solutions are provided, and the third section consists of fifty unsolved problems which range from simple monofunctional compounds to complex natural products."--BOOK JACKET. Espectroscopia de massa larpcal Espectroscopia ressonancia magnetica nuclear larpcal Espectroscopia larpcal Estrutura molecular (quimica teorica) larpcal Organische chemie gtt Spectrometrie gtt Organic compounds Analysis Spectrum analysis Organische Analyse (DE-588)4172764-2 gnd rswk-swf Spektroskopie (DE-588)4056138-0 gnd rswk-swf Organische Analyse (DE-588)4172764-2 s Spektroskopie (DE-588)4056138-0 s DE-604 Rodríguez, Jaime 1963- Verfasser (DE-588)140821597 aut Jaspars, Marcel 1966- Verfasser (DE-588)140821546 aut GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008433368&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Crews, Phillip 1943- Rodríguez, Jaime 1963- Jaspars, Marcel 1966- Organic structure analysis Espectroscopia de massa larpcal Espectroscopia ressonancia magnetica nuclear larpcal Espectroscopia larpcal Estrutura molecular (quimica teorica) larpcal Organische chemie gtt Spectrometrie gtt Organic compounds Analysis Spectrum analysis Organische Analyse (DE-588)4172764-2 gnd Spektroskopie (DE-588)4056138-0 gnd |
| subject_GND | (DE-588)4172764-2 (DE-588)4056138-0 |
| title | Organic structure analysis |
| title_auth | Organic structure analysis |
| title_exact_search | Organic structure analysis |
| title_full | Organic structure analysis Phillip Crews ; Jaime Rodríguez ; Marcel Jaspars |
| title_fullStr | Organic structure analysis Phillip Crews ; Jaime Rodríguez ; Marcel Jaspars |
| title_full_unstemmed | Organic structure analysis Phillip Crews ; Jaime Rodríguez ; Marcel Jaspars |
| title_short | Organic structure analysis |
| title_sort | organic structure analysis |
| topic | Espectroscopia de massa larpcal Espectroscopia ressonancia magnetica nuclear larpcal Espectroscopia larpcal Estrutura molecular (quimica teorica) larpcal Organische chemie gtt Spectrometrie gtt Organic compounds Analysis Spectrum analysis Organische Analyse (DE-588)4172764-2 gnd Spektroskopie (DE-588)4056138-0 gnd |
| topic_facet | Espectroscopia de massa Espectroscopia ressonancia magnetica nuclear Espectroscopia Estrutura molecular (quimica teorica) Organische chemie Spectrometrie Organic compounds Analysis Spectrum analysis Organische Analyse Spektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008433368&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT crewsphillip organicstructureanalysis AT rodriguezjaime organicstructureanalysis AT jasparsmarcel organicstructureanalysis |