Basic one- and two-dimensional NMR spectroscopy:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English German |
| Veröffentlicht: |
Weinheim [u.a.]
Wiley-VCH
1998
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| Ausgabe: | 3., rev. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXIV, 386 S.: Ill., graph. Darst. |
| ISBN: | 3527295135 |
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MARC
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| 245 | 1 | 0 | |a Basic one- and two-dimensional NMR spectroscopy |c Horst Friebolin |
| 250 | |a 3., rev. ed. | ||
| 264 | 1 | |a Weinheim [u.a.] |b Wiley-VCH |c 1998 | |
| 300 | |a XXIV, 386 S.: Ill., graph. Darst. | ||
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Datensatz im Suchindex
| _version_ | 1804126895130804224 |
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| adam_text | HORST FRIEBOLIN BASIC ONE- AND TWO-DIMENSIONAL NMR SPECTROSCOPY THIRD
REVISED EDITION TRANSLATED BY JACK K. BECCONSALL WILEY-VCH WEINHEIM *
NEW YORK * CHICHESTER * BRISBANE * SINGAPORE * TORONTO CONTENTS 1 THE
PHYSICAL BASIS OF NMR SPECTROSCOPY 1 1.1 INTRODUCTION 1 1.2 NUCLEAR
ANGULAR MOMENTUM AND MAGNETIC MOMENT 2 1.3 NUCLEI IN A STATIC MAGNETIC
FIELD 4 1.3.1 DIRECTIONAL QUANTIZATION 4 1.3.2 ENERGY OF THE NUCLEI IN
THE MAGNETIC FIELD .... 4 1.3.3 POPULATIONS OF THE ENERGY LEVELS 6 1.3.4
MACROSCOPIC MAGNETIZATION 6 1.4 BASIC PRINCIPLES OF THE NMR EXPERIMENT 7
1.4.1 THE RESONANCE CONDITION 7 1.4.2 BASIC PRINCIPLE OF THE NMR
MEASUREMENT .... 8 1.5 THE PULSED NMR METHOD 9 1.5.1 THE PULSE 9 1.5.2
THE PULSE ANGLE 10 1.5.3 RELAXATION 13 1.5.4 THE TIME AND FREQUENCY
DOMAINS; THE FOURIER TRANSFORMATION 14 1.5.5 SPECTRUM ACCUMULATION 16
1.5.6 THE PULSED NMR SPECTROMETER 18 1.6 SPECTRAL PARAMETERS: A BRIEF
SURVEY 22 1.6.1 THE CHEMICAL SHIFT 22 1.6.1.1 NUCLEAR SHIELDING 22
1.6.1.2 REFERENCE COMPOUNDS AND THE 5-SCALE 24 1.6.2 SPIN-SPIN COUPLING
26 1.6.2.1 THE INDIRECT SPIN-SPIN COUPLING 26 1.6.2.2 COUPLING TO ONE
NEIGHBORING NUCLEUS (AX SPIN SYSTEM) 27 1.6.2.3 COUPLING TO TWO
EQUIVALENT NEIGHBORING NUCLEI (AX 2 SPIN SYSTEM) 28 1.6.2.4 COUPLING TO
THREE OR MORE EQUIVALENT NEIGHBORING NUCLEI (AX N SPIN SYSTEM) 30
1.6.2.5 MULTIPLICITY RULES 30 1.6.2.6 COUPLINGS BETWEEN THREE
NON-EQUIVALENT NUCLEI (AMX SPIN SYSTEM) 31 1.6.2.7 COUPLINGS BETWEEN
EQUIVALENT NUCLEI (A N SPIN SYSTEMS) 32 1.6.2.8 THE ORDER OF A SPECTRUM
33 XV 1.6.2.9 COUPLINGS BETWEEN PROTONS AND OTHER NUCLEI; 13 C SATELLITE
SPECTRA 33 1.6.3 THE INTENSITIES OF THE RESONANCE SIGNALS 34 1.6.3.1 J H
SIGNAL INTENSITIES 34 1.6.3.2 13 C SIGNAL INTENSITIES 35 1.6.4 SUMMARY
37 1.7 OTHER NUCLIDES 38 1.7.1 NUCLIDES WITH I=YI 39 1.7.2 NUCLIDES
WITH I VI 40 1.8 BIBLIOGRAPHY FOR CHAPTER 1 41 2 THE CHEMICAL SHIFT 43
2.1 INTRODUCTION 43 2.1.1 INFLUENCE OF THE CHARGE DENSITY ON THE
SHIELDING 44 2.1.2 EFFECTS OF NEIGHBORING GROUPS 47 2.1.2.1 MAGNETIC
ANISOTROPY OF NEIGHBORING GROUPS. . 47 2.1.2.2 RING CURRENT EFFECTS 49
2.1.2.3 ELECTRIC FIELD EFFECTS 51 2.1.2.4 INTERMOLECULAR INTERACTIONS -
HYDROGEN BONDING AND SOLVENT EFFECTS 51 2.1.2.5 ISOTOPE EFFECTS 51 2.1.3
SUMMARY 52 2.2 H CHEMICAL SHIFTS OF ORGANIC COMPOUNDS ... 53 2.2.1
ALKANES AND CYCLOALKANES 54 2.2.2 ALKENES 56 2.2.3 ARENES 56 2.2.4
ALKYNES 57 2.2.5 ALDEHYDES 58 2.2.6 OH, SH, NH 59 2.3 I3 C CHEMICAL
SHIFTS OF ORGANIC COMPOUNDS ... 60 2.3.1 ALKANES AND CYCLOALKANES 61
2.3.2 ALKENES 63 2.3.3 ARENES . 64 2.3.4 ALKYNES 66 2.3.5 ALLENES 66
2.3.6 CARBONYL AND CARBOXY COMPOUNDS 66 2.3.6.1 ALDEHYDES AND KETONES 67
2.3.6.2 CARBOXYLIC ACIDS AND DERIVATIVES 68 2.4 RELATIONSHIPS BETWEEN
THE SPECTRUM AND THE MOLECULAR STRUCTURE 70 2.4.1 EQUIVALENCE, SYMMETRY
AND CHIRALITY 70 2.4.2 HOMOTOPIC, ENANTIOTOPIC AND DIASTEREOTOPIC GROUPS
74 2.4.3 SUMMARY 77 2.5 CHEMICAL SHIFTS OF OTHER NUCLIDESS 78 2.6
BIBLIOGRAPHY FOR CHAPTER 2 83 XVIII 3 INDIRECT SPIN-SPIN COUPLING 85 3.1
INTRODUCTION 85 3.2 H,H COUPLING CONSTANTS AND CHEMICAL STRUCTURE 87
3.2.1 GEMINAL COUPLINGS 2 /(H,H) 87 3.2.1.1 DEPENDENCE ON BOND ANGLE 87
3.2.1.2 SUBSTITUENT EFFECTS 87 3.2.1.3 EFFECTS OF NEIGHBORING
7T-ELECTRONS 87 3.2.2 VICINAL COUPLINGS 3 /(H,H) 89 3.2.2.1 DEPENDENCE
ON THE DIHEDRAL ANGLE 90 3.2.2.2 SUBSTITUENT EFFECTS 93 3.2.3 H,H
COUPLINGS IN AROMATIC COMPOUNDS 95 3.2.4 LONG-RANGE COUPLINGS 96 3.3 C,H
COUPLING CONSTANTS AND CHEMICAL STRUCTURE 97 3.3.1 C,H COUPLINGS THROUGH
ONE BOND V(C,H) ... 97 3.3.1.1 DEPENDENCE ON THE S-FRACTION 97 3.3.1.2
SUBSTITUENT EFFECTS 97 3.3.2 C,H COUPLINGS THROUGH TWO OR MORE BONDS ...
98 3.3.2.1 GEMINAL COUPLINGS (I. E. 2 7(C,H) IN H-C- 13 C) . . 98
3.3.2.2 VICINAL COUPLINGS (I. E. 3 7(C,H) IN H-C-C- 13 C) . 99 3.3.2.3
LONG-RANGE COUPLINGS 3+ /(C,H) 99 3.3.3 C,H COUPLINGS IN BENZENE
DERIVATIVES . 99 3.4 C,C COUPLING CONSTANTS AND CHEMICAL STRUCTURE 100
3.5 CORRELATIONS BETWEEN C,H AND H,H COUPLING CONSTANTS 101 3.6 COUPLING
MECHANISMS 102 3.6.1 THE ELECTRON-NUCLEAR INTERACTION 102 3.6.2 H,D
COUPLINGS 104 3.6.3 RELATIONSHIP BETWEEN THE COUPLING AND THE LIFETIME
OF A SPIN STATE 105 3.6.4 COUPLINGS THROUGH SPACE 106 3.7 COUPLINGS OF
OTHER NUCLIDES (HETERONUCLEAR COUPLINGS) 106 3.8 BIBLIOGRAPHY FOR
CHAPTER 3 109 4 SPECTRUM ANALYSIS AND CALCULATIONS ILL 4.1 INTRODUCTION
ILL 4.2 NOMENCLATURE 113 4.2.1 SYSTEMATIC NOTATION FOR SPIN SYSTEMS 113
4.2.2 CHEMICAL AND MAGNETIC EQUIVALENCE 114 4.3 TWO-SPIN SYSTEMS 116
4.3.1 THE AX SPIN SYSTEM 116 4.3.2 THE AB SPIN SYSTEM 118 4.4 THREE-SPIN
SYSTEMS 120 4.4.1 THE AX 2 , AK 2 , AB 2 , AND A 3 SPIN SYSTEMS ... 120
4.4.2 THE AMX AND ABX SPIN SYSTEMS 121 4.5 FOUR-SPIN SYSTEMS 123 4.5.1 A
2 X 2 AND A 2 B 2 SPIN SYSTEMS 123 4.5.2 THE AA XX AND AA BB SPIN
SYSTEMS 124 4.6 SPECTRUM SIMULATION AND ITERATION 125 4.7 ANALYSIS OF C
NMR SPECTRA 126 4.8 BIBLIOGRAPHY FOR CHAPTER 4 127 5 DOUBLE RESONANCE
EXPERIMENTS 129 5.1 INTRODUCTION 129 5.2 SPIN DECOUPLING IN H NMR
SPECTROSCOPY ... . 130 5.2.1 SIMPLIFICATION OF SPECTRA BY SELECTIVE SPIN
DECOUPLING 130 5.2.2 SUPPRESSION OF A SOLVENT SIGNAL 132 5.3 SPIN
DECOUPLING IN C NMR SPECTROSCOPY ... 133 5.3.1 !H BROAD-BAND DECOUPLING
133 5.3.2 THE GATED DECOUPLING EXPERIMENT 135 5.3.3 X H OFF-RESONANCE
DECOUPLING 136 5.3.4 SELECTIVE DECOUPLING IN 13 C NMR SPECTROSCOPY 137
5.4 BIBLIOGRAPHY FOR CHAPTER 5 138 6 ASSIGNMENT OF L H AND 13 C SIGNALS
139 6.1 INTRODUCTION 139 6.2 M NMR SPECTROSCOPY 140 6.2.1 DEFINING THE
PROBLEM 140 6.2.2 EMPIRICAL CORRELATIONS FOR PREDICTING CHEMICAL SHIFTS
. . * 141 6.2.2.1 ALKANES (SHOOLERY S RULE) 141 6.2.2.2 ALKENES 142
6.2.2.3 BENZENE DERIVATIVES 143 6.2.3 DECOUPLING EXPERIMENTS 145 6.2.4
EFFECTS OF SOLVENT AND TEMPERATURE . 145 6.2.5 ALTERING THE CHEMICAL
STRUCTURE OF THE SAMPLE . 146 6.3 D C NMR SPECTROSCOPY 147 6.3.1
DEFINING THE PROBLEM . 147 6.3.2 EMPIRICAL CORRELATIONS FOR PREDICTING
APPROXIMATE CHEMICAL SHIFTS 148 6.3.2.1 ALKANES 148 6.3.2.2 ALKENES X
151 6.3.2.3 BENZENE DERIVATIVES . 153 6.3.3 DECOUPLING EXPERIMENTS 154
6.3.4 T MEASUREMENTS 154 6.3.5 SOLVENT AND TEMPERATURE EFFECTS AND
SHIFT REAGENTS 154 6.3.6 CHEMICAL CHANGES TO THE SAMPLE 154 6.4
COMPUTER-AIDED ASSIGNMENT OF U C NMR SPECTRA 156 6.4.1 SEARCHING FOR
IDENTICAL OR RELATED COMPOUNDS . 156 6.4.2 SPECTRUM PREDICTION 157 6.5
BIBLIOGRAPHY FOR CHAPTER 6 159 7 RELAXATION 161 7.1 INTRODUCTION 161 7.2
SPIN-LATTICE RELAXATION OF 13 C NUCLEI (7 ) .... 162 7.2.1 RELAXATION
MECHANISMS 162 7.2.2 EXPERIMENTAL DETERMINATION OF 7 ; THE INVERSION
RECOVERY EXPERIMENT 164 7.2.3 RELATIONSHIPS BETWEEN T AND CHEMICAL
STRUCTURE 168 7.2.3.1 INFLUENCE OF PROTONS IN CH, CH 2 AND CH 3 GROUPS
168 7.2.3.2 INFLUENCE OF MOLECULAR SIZE 169 7.2.3.3 SEGMENTAL MOBILITIES
170 7.2.3.4 ANISOTROPY OF THE MOLECULAR MOBILITY 170 7.2.4 SUPPRESSION
OF THE WATER SIGNAL 171 7.3 SPIN-SPIN RELAXATION (T 2 ) 171 7.3.1
RELAXATION MECHANISMS 171 7.3.2 EXPERIMENTAL DETERMINATION OF T2; THE
SPIN-ECHO EXPERIMENT 173 7.3.3 LINE-WIDTHS OF NMR SIGNALS 177 7.4
BIBLIOGRAPHY FOR CHAPTER 7 178 8 ONE-DIMENSIONAL NMR EXPERIMENTS USING
COMPLEX PULSE SEQUENCES 181 8.1 INTRODUCTION 181 8.2 BASIC TECHNIQUES
USING PULSE SEQUENCES AND PULSED FIELD GRADIENTS 182 8.2.1 THE EFFECT OF
THE PULSE ON THE LONGITUDINAL MAGNETIZATION (M Z ) 183 8.2.2 THE EFFECT
OF THE PULSE ON THE TRANSVERSE MAGNETIZATION COMPONENTS (M X - MY) 184
8.2.3 THE EFFECT OF PULSED FIELD GRADIENTS ON THE TRANSVERSE
MAGNETIZATION 187 8.3 THE /-MODULATED SPIN-ECHO EXPERIMENT 192 8.4 THE
PULSED GRADIENT SPIN-ECHO EXPERIMENT . . 200 8.5 SIGNAL ENHANCEMENT BY
POLARIZATION TRANSFER . . 202 8.5.1 THE SPI EXPERIMENT 202 8.5.2 THE
INEPT EXPERIMENT 205 8.5.3 THE REVERSE INEPT EXPERIMENT WITH PROTON
DETECTION 213 8.6 THE DEPT EXPERIMENT 218 8.7 THE SELECTIVE TOCSY
EXPERIMENT 223 8.8 THE ONE-DIMENSIONAL INADEQUATE EXPERIMENT 225 8.9
BIBLIOGRAPHY FOR CHAPTER 8 22 9 9 TWO-DIMENSIONAL NMR SPECTROSCOPY 231
9.1 INTRODUCTION 231 9.2 THE TWO-DIMENSIONAL NMR EXPERIMENT 232 9.2.1
PREPARATION, EVOLUTION AND MIXING, DATA ACQUISITION 232 9.2.2 GRAPHICAL
REPRESENTATION 236 9.3 TWO-DIMENSIONAL /-RESOLVED NMR SPECTROSCOPY 237
9.3.1 HETERONUCLEAR TWO-DIMENSIONAL /-RESOLVED NMR SPECTROSCOPY 237
9.3.2 HOMONUCLEAR TWO-DIMENSIONAL /-RESOLVED NMR SPECTROSCOPY 241 9.4
TWO-DIMENSIONAL CORRELATED NMR SPECTROSCOPY 246 9.4.1 TWO-DIMENSIONAL
HETERONUCLEAR (C,H)-CORRELATED NMR SPECTROSCOPY (HETCOR OR C,H-COSY) 247
9.4.2 TWO-DIMENSIONAL HOMONUCLEAR (H,H)-CORRELATED NMR SPECTROSCOPY
(H,H-COSY; LONG-RANGE COSY) 255 9.4.3 REVERSE TWO-DIMENSIONAL
HETERONUCLEAR (H.C)-CORRELATED NMR SPECTROSCOPY (HSQC; HMQC) 263 9.4.4
THE GRADIENT-SELECTED (GS-)HMBC EXPERIMENT 269 9.4.5 THE TOCSY
EXPERIMENT 273 9.4.6 TWO-DIMENSIONAL EXCHANGE NMR SPECTRO- SCOPY: THE
NOESY AND EXSY EXPERIMENTS ... 276 9.5 THE TWO-DIMENSIONAL INADEQUATE
EXPERIMENT 279 9.6 SUMMARY OF CHAPTERS 8 AND 9 284 9.7 BIBLIOGRAPHY FOR
CHAPTER 9 285 10 THE NUCLEAR OVERHAUSER EFFECT 287 10.1 INTRODUCTION 287
10.2 THEORETICAL BACKGROUND 288 10.2.1 THE TWO-SPIN SYSTEM 288 10.2.2
ENHANCEMENT FACTORS 291 10.2.3 MULTI-SPIN SYSTEMS 292 10.2.4 FROM THE
ONE-DIMENSIONAL TO THE TWO-DIMENSIONAL EXPERIMENT 293 10.3 EXPERIMENTAL
ASPECTS 294 10.4 APPLICATIONS 295 10.5 BIBLIOGRAPHY FOR CHAPTER 10 300
11 DYNAMIC NMR SPECTROSCOPY (DNMR) .301 11.1 INTRODUCTION 301 11.2
QUANTITATIVE CALCULATIONS 305 11.2.1 COMPLETE LINE-SHAPE ANALYSIS 305
11.2.2 THE COALESCENCE TEMPERATURE 7C AND THE CORRESPONDING RATE
CONSTANT KC 307 11.2.3 ACTIVATION PARAMETERS 308 11.2.3.1 THE ARRHENIUS
ACTIVATION ENERGY E A 308 11.2.3.2 THE FREE ENTHALPY OF ACTIVATION AG X
309 11.2.3.3 ESTIMATING THE LIMITS OF ERROR 310 11.2.4 RATE CONSTANTS IN
REACTIONS WITH INTERMEDIATE STAGES 311 11.2.5 INTERMOLECULAR EXCHANGE
PROCESSES 312 11.3 APPLICATIONS 313 11.3.1 ROTATION ABOUT CC SINGLE
BONDS 313 11.3.1.1 C(SP 3 )-C(SP 3 ) BONDS 314 11.3.1.2 C(SP 2 )-C(SP 3
) BONDS 314 11.3.1.3 C(SP 2 )-C(SP 2 ) BONDS 315 11.3.2 ROTATION ABOUT A
PARTIAL DOUBLE BOND 315 11.3.3 INVERSION AT NITROGEN AND PHOSPHORUS
ATOMS .. 317 11.3.4 RING INVERSION 318 11.3.5 VALENCE TAUTOMERISM 321
11.3.6 KETO-ENOL TAUTOMERISM 322 11.3.7 INTERMOLECULAR PROTON EXCHANGE
323 11.3.8 REACTIONS AND EQUILIBRATION PROCESSES 325 11.4 BIBLIOGRAPHY
FOR CHAPTER 11 328 12 SHIFT REAGENTS 331 12.1 LANTHANIDE SHIFT REAGENTS
(LSRS) 331 12.1.1 FUNDAMENTALS 331 12.1.2 APPLICATIONS AND QUANTITATIVE
INTERPRETATION . . 333 12.2 CHIRAL LANTHANIDE SHIFT REAGENTS 336 12.3
CHIRAL SOLVENTS 338 12.4 BIBLIOGRAPHY FOR CHAPTER 12 341 13
MACROMOLECULES 343 13.1 INTRODUCTION 343 13.2 SYNTHETIC POLYMERS 343
13.2.1 THE TACTICITY OF POLYMERS * 343 13.2.2 POLYMERIZATION OF DIENES
347 13.2.3 COPOLYMERS 348 13.3 BIBLIOGRAPHY FOR CHAPTER 13 350 14 NMR
SPECTROSCOPY IN BIOCHEMISTRY AND MEDICINE 351 14.1 INTRODUCTION 35 1
14.2 ELUCIDATING REACTION PATHWAYS IN BIOCHEMISTRY 352 14.2.1 SYNTHESES
USING SINGLY 13 C-LABELED PRECURSORS . 352 14.2.1.1 LOW LEVELS OF 13 C
ENRICHMENT 352 14.2.1.2 HIGH LEVELS OF 13 C ENRICHMENT 354 14.2.2
SYNTHESES USING DOUBLY 13 C-LABELED PRECURSORS 355 14.3 HIGH RESOLUTION
IN VIVO NMR SPECTROSCOPY . . . 357 14.3.1 THE PROBLEM AND ITS SOLUTION
357 14.3.2 31 P NMR EXPERIMENTS 358 14.3.3 M AND 13 C NMR EXPERIMENTS
361 14.4 MAGNETIC RESONANCE TOMOGRAPHY 362 14.4.1 BASIC PRINCIPLES AND
EXPERIMENTAL CONSIDERATIONS 362 14.4.2 APPLICATIONS 370 14.5
BIBLIOGRAPHY FOR CHAPTER 14 372 SUBJECT INDEX 375 INDEX OF COMPOUNDS 383
|
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| author | Friebolin, Horst |
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| dewey-ones | 543 - Analytical chemistry |
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| dewey-search | 543/.0877 |
| dewey-sort | 3543 3877 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | 3., rev. ed. |
| format | Book |
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| genre | (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV012274250 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T18:24:43Z |
| institution | BVB |
| isbn | 3527295135 |
| language | English German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008319545 |
| oclc_num | 40432527 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-29T DE-703 DE-20 DE-91G DE-BY-TUM DE-M49 DE-BY-TUM DE-858 DE-11 |
| owner_facet | DE-355 DE-BY-UBR DE-29T DE-703 DE-20 DE-91G DE-BY-TUM DE-M49 DE-BY-TUM DE-858 DE-11 |
| physical | XXIV, 386 S.: Ill., graph. Darst. |
| publishDate | 1998 |
| publishDateSearch | 1998 |
| publishDateSort | 1998 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Friebolin, Horst Verfasser (DE-588)106657968 aut Ein- und zweidimensionale NMR-Spektroskopie Basic one- and two-dimensional NMR spectroscopy Horst Friebolin 3., rev. ed. Weinheim [u.a.] Wiley-VCH 1998 XXIV, 386 S.: Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier NMR gtt Résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Medizin (DE-588)4038243-6 gnd rswk-swf Dynamisches System (DE-588)4013396-5 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Methode (DE-588)4038971-6 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Zweidimensionale NMR-Spektroskopie (DE-588)4191219-6 gnd rswk-swf Biochemie (DE-588)4006777-4 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Zweidimensionale NMR-Spektroskopie (DE-588)4191219-6 s DE-604 NMR-Spektroskopie (DE-588)4075421-2 s Analytische Chemie (DE-588)4129906-1 s 1\p DE-604 Medizin (DE-588)4038243-6 s 2\p DE-604 Biochemie (DE-588)4006777-4 s 3\p DE-604 Polymere (DE-588)4046699-1 s 4\p DE-604 Methode (DE-588)4038971-6 s 5\p DE-604 Dynamisches System (DE-588)4013396-5 s 6\p DE-604 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008319545&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 5\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 6\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Friebolin, Horst Basic one- and two-dimensional NMR spectroscopy NMR gtt Résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd Medizin (DE-588)4038243-6 gnd Dynamisches System (DE-588)4013396-5 gnd Polymere (DE-588)4046699-1 gnd Methode (DE-588)4038971-6 gnd Analytische Chemie (DE-588)4129906-1 gnd Zweidimensionale NMR-Spektroskopie (DE-588)4191219-6 gnd Biochemie (DE-588)4006777-4 gnd |
| subject_GND | (DE-588)4075421-2 (DE-588)4038243-6 (DE-588)4013396-5 (DE-588)4046699-1 (DE-588)4038971-6 (DE-588)4129906-1 (DE-588)4191219-6 (DE-588)4006777-4 (DE-588)4123623-3 |
| title | Basic one- and two-dimensional NMR spectroscopy |
| title_alt | Ein- und zweidimensionale NMR-Spektroskopie |
| title_auth | Basic one- and two-dimensional NMR spectroscopy |
| title_exact_search | Basic one- and two-dimensional NMR spectroscopy |
| title_full | Basic one- and two-dimensional NMR spectroscopy Horst Friebolin |
| title_fullStr | Basic one- and two-dimensional NMR spectroscopy Horst Friebolin |
| title_full_unstemmed | Basic one- and two-dimensional NMR spectroscopy Horst Friebolin |
| title_short | Basic one- and two-dimensional NMR spectroscopy |
| title_sort | basic one and two dimensional nmr spectroscopy |
| topic | NMR gtt Résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd Medizin (DE-588)4038243-6 gnd Dynamisches System (DE-588)4013396-5 gnd Polymere (DE-588)4046699-1 gnd Methode (DE-588)4038971-6 gnd Analytische Chemie (DE-588)4129906-1 gnd Zweidimensionale NMR-Spektroskopie (DE-588)4191219-6 gnd Biochemie (DE-588)4006777-4 gnd |
| topic_facet | NMR Résonance magnétique nucléaire Spectroscopie de la résonance magnétique nucléaire Magnetic Resonance Spectroscopy methods Nuclear magnetic resonance spectroscopy NMR-Spektroskopie Medizin Dynamisches System Polymere Methode Analytische Chemie Zweidimensionale NMR-Spektroskopie Biochemie Lehrbuch |
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| work_keys_str_mv | AT friebolinhorst einundzweidimensionalenmrspektroskopie AT friebolinhorst basiconeandtwodimensionalnmrspectroscopy |