Characterization techniques of glasses and ceramics:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | German |
| Veröffentlicht: |
Berlin ; Heidelberg ; New York ; Barcelona ; Hong Kong ; London
Springer
1999
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XII, 239 S. Ill., graph. Darst. |
| ISBN: | 3540636579 |
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| 245 | 1 | 0 | |a Characterization techniques of glasses and ceramics |c J. M. Rincon ; M. Romero (ed.) |
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Datensatz im Suchindex
| _version_ | 1805083634755960832 |
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| adam_text |
Table of Contents
Part I. Chemical Analysis
1. Rare Earth Elements:
Applications and Determination
F.J. Valle Fuentes.
1.1 Introduction.
1.1.1 Metallurgy.
1.1.2 Catalysis.
1.1.3 Glasses.
1.1.4 Cathode Ray Tubes.
1.1.5 Lasers.
1.1.6 Electric and Electronic Ceramics .
1.1.7 Electro-Optical Ceramics.
1.1.8 Decorated Tableware and Porcelain.
1.1.9 Refractory Materials.
1.1.10 Miscellaneous Applications.
1.2 Determination of Rar e Earths.
1.2.1 Nuclear Neutron Activation.
1.2.2 Atomic Absorption Spectrometry.
1.2.3 Plasma Spectrometries.
1.2.4 X Ray Fluorescence Spectrometry.
1.3 Determination of REE in Advanced Ceramic Materials
3
3
3
4
4
5
5
5
5
5
6
C
6
7
8
8
10
II
Part II. Microscopies: Including Scanning Tunneling and Electron
Microscopies
2. Scanning Tunneling Microscopy: Applications to the Study
of Ordered and Disordered Conducting Solid Surfaces
L. Vazquez. R.C. Salvarezza and A.J. Arvi a . 17
2.1 Introduction. 17
2.1.1 Basic Operating Principles. 18
2.1.2 Experimental Mounting. 20
VIII
2.2 Theoretical Outline. 21
2.3 Applications. 22
2.3.1 Imaging Weakly Disordered Surfaces by STM. 22
2.3.2 Surface Reactions. 26
2.3.3 Imaging Disordered Systems by STM . 29
2.4 Conclusions . 38
3. Basis and Applications of Convergent Beam Electron
Diffraction (CBED) for the Investigation of Phases in Ceramics
and Glass-Ceramics
J. Ma. Rincón and M. Romrro. 41
3.1 introduction. 41
3.1.1 Fundamentals of Electron Diffraction by CBED:
Basic Principles. 41
3.1.2 Possibilities and Limitations
of CBED for characterising ceramic powders. 46
3.2 Practical Aspects of CBED: Specimen Preparation
and Operation in the TEM. 52
3.3 Applications of CBED for solving Problems in Ceramics:
Some Examples and Application to Zirconia/Mullite Materials. 54
3.1 Future of the CBED Method . 59
3.5 Conclusion. 60
4. Basis and Applications of High Resolution Electron
Microscopy (HREM) for the Characterization of Ceramics and
Glass-Ceramics
J. Ma. Rtxcón and M. Romero. 64
4.1 Introduction: Fundamentals of the HREM Methods. 64
4.2 Operating Procedures and Instrumental Requirements. 65
4.3 Key Examples of HREM Applications
on Ceramics and Glassy Materials. 68
4.3.1 Monophase Ceramics. 68
4.3.2 Polyphase Ceramics. 69
4.3.3 Interfaces and Grain Boundaries in Oxide
and Non-Oxide Ceramics. 69
1.3.4 Phase Transformations. 72
4.3.5 G lass-Ceramics and Glasses Studied by HREM. 74
4.4 Computation. 76
4.5 Future Prospects on HREM:
Combination with Spectroscopy, CBED and Holographic Methods . 76
4.6 Conclusions . 80
Table of Contents
IX
Part III. Thermal Methods
5. Applications of Differential Scanning Calorimetry for the
Study of Transformation Processes in Quenched Alloys
A. Varschavsky and J. SiiSTAK. 85
Part I: Theoretical Basis
5.1 Introduction. 85
5.2 Characterization of TA Curves. 86
5.3 Information Content. 88
5.4 Determination of Stable
and Metastable Phase Diagram Boundary. 89
5.5 Study of Equilibrium and Nonequilibrium Processes. 91
5.6 Glass Transition
as an Example of Highly Nonequilibrium Changes. 92
5.7 Crystallization and Transformation
of Me Las table Phases. 91
5.8 The Study of Reaction Kinetics. 94
Part II: Experimental Results
of Short-Range Ordering in q-Cu-A1 Alloys
5.1 Introduction and Experimental. 96
5.2 DSC Thermograms for Quenched Alloys. 97
5.3 Kinetic Parameters and Kinetic Laws. 99
5.4 Overall Kinetics for Ordering.100
5.5 Effect of Quenching Conditions .101
5.6 Vacancy Behavior.104
5.7 Concentration Dependence of the Relative Increase
of the SRO Parameter.107
5.8 Acknowledgements.110
6. Use of Thermal Analysis in Zeolite
Research and Application
C. Coll'lla.112
6.1 Introduction.112
6.2 Zeolite Properties and Applications.113
6.3 Thermal Behavior of Zeolites.116
6.3.1 Water Loss.116
6.3.2 Decomposition and Gas Evolution.123
6.3.3 Order-Disorder 'IVansformation and Phase Transition .126
6.3.4 Structure Collapse. Recrystallization and Melting.127
6.3.5 Changes in Electrical Properties.129
6.4 Evaluation of Zeolite Content
in Multicomponent Mixtures.129
X
6.5 Thermal Characterization of Zeolite Catalysts .132
6.5.1 Adsorbate/Framework Interactions .133
6.5.2 Estimation of Acidity Distribution in a Zeolite Catalyst.134
6.5.3 Modification of, and Reactant Conversion on,
a Zeolite Catalyst .134
7. Viscous Flow of Glass Forming Liquids:
Experimental Techniques for the High Viscosity Range
E.D. Zanotto and A.R. Mtcjliore Jr.138
7.1 Introduction.138
7.2 The Physics of Viscous Flow.138
7.3 Rheological Models.142
7.4 Measurement Techniques.144
7.4.1 Fiber Extension and Cylinder Compression.147
7.4.2 The Beam-Bending Method.'147
7.4.3 Indentation Techniques.148
7.4.4 Parallel Plates .149
7.5 Final Comments.149
8. Diffusion Structural Analysis in the Characterization of
Inorganic Materials
V. Balek.151
8.1 Basic Principles of the Method.151
8.2 Sample Preparation for DSA Measurements .151
8.2.1 Diffusion Technique.151
8.2.2 Sample Preparation in the Inert Gas Atmosphere.152
8.2.3 Implantation of Accelerated Ions of Inert Gases .152
8.2.4 Inert- Gases Produced from Nuclear Reactions.152
8.2.5 Introduction of Parent Radionuclides
as a Source of Inert Gas Atoms.152
8.3 Mechanisms and Theories
for Release of the Inert Gases from Solids.153
8.3.1 Cases when the Inert Gas has been Incorporated
into a, Solid without its Parent Nuclide(s).154
8.3.2 Cases when the Parent Nueliclc(s) of the Inert Gas are used
for Sample Labelling.154
8.4 Measurement of Inert Gas Release.155
8.5 Potential Use of Diffusion Structural Analysis.157
8.6 Examples of DSA Applications.158
8.6.1 Diagnostics of the Defect State.158
8.6.2 Assessment of Inorganic Materials Prepared
by Heat Treatment.158
8.6.3 Characterization of Geleous Materials.159
Tablo of Contents XL
Part IV. X-ray, Resonance and Nuclear Methods
9. Texture Determination by Using X ray Diffraction
F. Wagnf.r.1G9
9.1 Introduction.169
9.2 Experimental Information: The Pole Figures.170
9.2.1 Principle of a Pole Figure Measure.170
9.2.2 Corrections of the Data .172
9.2.3 Pole Figure Representation - Examples.175
9.3 Orientation Density Function (ODF) Determination.176
9.3.1 Orientation of a Grain .176
9.3.2 The ODF (Orientation Density Function).179
9.3.3 Fundamental Equation of the Texture Analysis.179
9.3.1 Principles of the Harmonic Method for Texture Analysis.180
9.3.5 Ambiguity in ODF Determination.181
9.3.6 ODF Representation and Examples.182
9.4 Conclusion.184
10. Recent Advances in X-Ray Fluorescence (XRF) Analysis
S. Uht.tg.187
10.1 Analytical Capability of XRF Analysis.187
10.2 Simple and Rapid Sample Preparation .188
10.3 High-Tech Instrumentation .190
10.4 Flexible Sample Handling.191
10.5 Unlimited Areas of Application.192
10.6 Optimized Light Element Analysis.193
10.7 Effective and Comfortable Data Evaluation.193
10.8 Precalibrated Analytical Programs.194
10.9 Conclusion.198
11. Mossbauer Spectroscopy Applied to Inorganic Materials
V. Kozhukiiarov and S. Vasilev.199
11.1 Introduction.199
11.2 Fundamental Equations.200
11.3 Mossbauer Isotopes and Transitions.201
11.4 Instrumentation.202
11.5 Basic Characteristics of Mossbauer Spectra.203
11.5.1 Isomer Shift.203
11.5.2 Quadrupole Splitting.206
11.5.3 Magnetic Ilyperfine Splitting.206
11.6 Interpretation of Mossbauer Spectra.207
11.7 Bonding and Structure Interpretation.208
XII
11.8 Conclusion.218
12. Neutron Diffraction in Amorphous Structures
S. Neov and V. Kozhukiiarov.220
12.1 Introduction.220
12.2 Diffraction Methods Review.220
12.3 Neutron Scattering in Amorphous Solids.223
12.4 Nuclear Reactor as Neutron Source.225
12.5 Neutron Detectors.226
12.6 Time of Flight (TOF) Neutron Diffraction.227
12.7 Small Angle Neutron Scattering (SANS).229
Subject Index .231 |
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| discipline | Physik Werkstoffwissenschaften / Fertigungstechnik |
| format | Book |
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| genre | (DE-588)1071861417 Konferenzschrift 1998 Lanzarote gnd-content (DE-588)1071861417 Konferenzschrift 1998 Yaiza gnd-content |
| genre_facet | Konferenzschrift 1998 Lanzarote Konferenzschrift 1998 Yaiza |
| id | DE-604.BV012240178 |
| illustrated | Illustrated |
| indexdate | 2024-07-20T07:51:40Z |
| institution | BVB |
| isbn | 3540636579 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008294230 |
| oclc_num | 632723473 |
| open_access_boolean | |
| owner | DE-92 DE-703 DE-634 DE-83 DE-11 DE-B16 |
| owner_facet | DE-92 DE-703 DE-634 DE-83 DE-11 DE-B16 |
| physical | XII, 239 S. Ill., graph. Darst. |
| publishDate | 1999 |
| publishDateSearch | 1999 |
| publishDateSort | 1999 |
| publisher | Springer |
| record_format | marc |
| spelling | Characterization techniques of glasses and ceramics J. M. Rincon ; M. Romero (ed.) Berlin ; Heidelberg ; New York ; Barcelona ; Hong Kong ; London Springer 1999 XII, 239 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Céramique industrielle - Analyse Céramique industrielle - Analyse ram Verre - Analyse Verre - Analyse ram Ceramics Analysis Glass Analysis Chemische Analyse (DE-588)4009840-0 gnd rswk-swf Keramischer Werkstoff (DE-588)4030282-9 gnd rswk-swf Glas (DE-588)4021142-3 gnd rswk-swf Werkstoffprüfung (DE-588)4037934-6 gnd rswk-swf Physikalische Analyse (DE-588)4121477-8 gnd rswk-swf (DE-588)1071861417 Konferenzschrift 1998 Lanzarote gnd-content (DE-588)1071861417 Konferenzschrift 1998 Yaiza gnd-content Werkstoffprüfung (DE-588)4037934-6 s Glas (DE-588)4021142-3 s DE-604 Keramischer Werkstoff (DE-588)4030282-9 s Physikalische Analyse (DE-588)4121477-8 s Chemische Analyse (DE-588)4009840-0 s Rincon, J. M. Sonstige oth KOBV Fremddatenuebernahme application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008294230&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Characterization techniques of glasses and ceramics Céramique industrielle - Analyse Céramique industrielle - Analyse ram Verre - Analyse Verre - Analyse ram Ceramics Analysis Glass Analysis Chemische Analyse (DE-588)4009840-0 gnd Keramischer Werkstoff (DE-588)4030282-9 gnd Glas (DE-588)4021142-3 gnd Werkstoffprüfung (DE-588)4037934-6 gnd Physikalische Analyse (DE-588)4121477-8 gnd |
| subject_GND | (DE-588)4009840-0 (DE-588)4030282-9 (DE-588)4021142-3 (DE-588)4037934-6 (DE-588)4121477-8 (DE-588)1071861417 |
| title | Characterization techniques of glasses and ceramics |
| title_auth | Characterization techniques of glasses and ceramics |
| title_exact_search | Characterization techniques of glasses and ceramics |
| title_full | Characterization techniques of glasses and ceramics J. M. Rincon ; M. Romero (ed.) |
| title_fullStr | Characterization techniques of glasses and ceramics J. M. Rincon ; M. Romero (ed.) |
| title_full_unstemmed | Characterization techniques of glasses and ceramics J. M. Rincon ; M. Romero (ed.) |
| title_short | Characterization techniques of glasses and ceramics |
| title_sort | characterization techniques of glasses and ceramics |
| topic | Céramique industrielle - Analyse Céramique industrielle - Analyse ram Verre - Analyse Verre - Analyse ram Ceramics Analysis Glass Analysis Chemische Analyse (DE-588)4009840-0 gnd Keramischer Werkstoff (DE-588)4030282-9 gnd Glas (DE-588)4021142-3 gnd Werkstoffprüfung (DE-588)4037934-6 gnd Physikalische Analyse (DE-588)4121477-8 gnd |
| topic_facet | Céramique industrielle - Analyse Verre - Analyse Ceramics Analysis Glass Analysis Chemische Analyse Keramischer Werkstoff Glas Werkstoffprüfung Physikalische Analyse Konferenzschrift 1998 Lanzarote Konferenzschrift 1998 Yaiza |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008294230&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT rinconjm characterizationtechniquesofglassesandceramics |