Practical introduction to GC-MS analysis with quadrupoles:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
Heidelberg
Hüthig
1998
|
| Schriftenreihe: | Desk library of chemistry
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben. - Dt. Ausg. u.d.T.: Oehme, Michael: Praktische Einführung in die GC-MS-Analytik mit Quadrupolen |
| Beschreibung: | 195 S. graph. Darst. |
| ISBN: | 3778526022 |
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| 100 | 1 | |a Oehme, Michael |d 1950- |e Verfasser |0 (DE-588)109960599 |4 aut | |
| 245 | 1 | 0 | |a Practical introduction to GC-MS analysis with quadrupoles |c by Michael Oehme |
| 264 | 1 | |a Heidelberg |b Hüthig |c 1998 | |
| 300 | |a 195 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Desk library of chemistry | |
| 500 | |a Literaturangaben. - Dt. Ausg. u.d.T.: Oehme, Michael: Praktische Einführung in die GC-MS-Analytik mit Quadrupolen | ||
| 650 | 4 | |a Gas chromatography | |
| 650 | 4 | |a Gas chromatography |x Instruments |x Calibration | |
| 650 | 4 | |a Gas chromatography |x Instruments |x Maintenance and repair | |
| 650 | 4 | |a Mass spectrometers |x Calibration | |
| 650 | 4 | |a Mass spectrometers |x Maintenance and repair | |
| 650 | 4 | |a Mass spectrometry | |
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-008208677 | |
Datensatz im Suchindex
| _version_ | 1807773331067240448 |
|---|---|
| adam_text |
7
CONTENTS
PREFACE
1.
POTENTIAL,
RANGE
OF
APPLICATION
AND
METHODOLOGICAL
LIMITATIONS
OF
GAS
CHROMATOGRAPHY
-
MASS
SPECTROMETRY
1.1
THE
DEVELOPMENT
OF
GC-MS
TOWARDS
A
ROUTINE
METHOD
11
1.2
FIELD
OF
APPLICATION
OF
GC-MS
15
1.3
A
UNIQUE
METHOD
FOR
ULTRA-TRACE
ANALYSIS
16
1.4
LITERATURE
ABOUT
HISTORICAL
DEVELOPMENT
18
2.
CONSTRUCTION
AND
PRINCIPLES
OF
OPERATION
OF
QUADRUPOLE
MASS
SPECTROMETERS
2.1
CONSTRUCTION
OF
QUADRUPOLE
MASS
SPECTROMETERS
19
2.2
THE
ION
SOURCE
22
2.2.1
ION
SOURCES
FOR
CHEMICAL
IONIZATION
(CI)
24
2.3
THE
QUADRUPOLE
MASS-FILTER
26
2.3.1
MASS
RESOLUTION
31
2.3.2
ADJUSTMENT
OF
THE
RESOLUTION
OF
A
QUADRUPOLE
31
2.4
THE
ELECTRON
MULTIPLIER
34
2.5
THE
HIGH-VACUUM
SYSTEM
37
2.5.1
WHY
IS
HIGH
VACUUM
NEEDED?
37
2.5.2
DIFFUSION
PUMPS
37
2.5.3
TURBOMOLECULAR
PUMPS
39
2.5.4
ROTARY
PUMPS
41
2.5.5
DESIGN
OF
VACUUM
SYSTEMS
42
2.5.6
VACUUM
GAUGES
43
2.5.6.1
INSTRUMENTATION
FOR
ROUGH
VACUUM
MEASUREMENT
44
2.5.6.2
HIGH-VACUUM
INSTRUMENTATION
45
2.6
LITERATURE
47
3.
IONIZATION
TECHNIQUES
3.1
THE
MOST
IMPORTANT
IONIZATION
TECHNIQUES
48
8
CONTENTS
3.2
ELECTRON
IONIZATION
(EI)
49
3.2.1
WHAT
INFORMATION
DOES
THE
EL
MASS
SPECTRUM
CONTAIN?
53
3.2.2
FACTORS
INFLUENCING
FRAGMENTATION
REACTIONS
55
3.3
CHEMICAL
IONIZATION
57
3.3.1
FORMATION
OF
POSITIVE
IONS
57
3.3.1.1
CHARGE-TRANSFER
REACTIONS
57
3.3.1.2
PROTON
TRANSFER
58
3.3.2
FORMATION
OF
NEGATIVE
IONS
60
3.4
LITERATURE
65
4.
METHODS
AND
OPTIMIZATION
OF
ION
DETECTION
4.1
MASS
SCAN
AND
TOTAL
ION
CURRENT
CHROMATOGRAM
66
4.1.1
ACQUISITION
TECHNIQUE
66
4.1.2
OPTIMIZATION
OF
THE
MASS
SCAN
TECHNIQUE
67
4.1.2.1
MASS
RANGE,
MS
BACKGROUND
AND
MASS
THRESHOLD
68
4.1.2.2
SCAN
SPEED
FOR
FULL-SCAN
MASS
SPECTROMETRY
71
4.2
SELECTIVE
ION
DETECTION
(SID)
73
4.2.1
RANGE
OF
APPLICATION
OF
THE
SID
TECHNIQUE
74
4.2.2
OPTIMIZATION
OF
THE
SID
TECHNIQUE
76
4.2.2.1
CALIBRATION
OF
MASS
SCALE
AND
MEASUREMENT
TIME
PER
ION
76
4.2.2.2
OPTIMIZATION
OF
THE
ION
SOURCE
FOR
SID
ANALYSIS
80
4.2.2.3
QUADRUPOLE
AND
ELECTRON
MULTIPLIER
83
4.3
MS-MS
COUPLING
83
4.4 LITERATURE
87
5.
THE
GC-MS
INTERFACE
5.1
REQUIREMENTS
OF
A
GC-MS
INTERFACE
89
5.2
GC-MS
INTERFACES
FOR
CAPILLARY
GC
91
5.2.1
DIRECT
COUPLING
91
5.2.1.1
LIMITATIONS
OF
THE
DIRECT
COUPLING
91
5.2.1.2
POSSIBLE
PROBLEMS
94
5.2.1.3
ADAPTATION
OF
CARRIER-GAS
FLOW
TO
PUMPING
CAPACITY
95
5.2.1.4
PRACTICAL
RECOMMENDATIONS
98
5.2.2
OPEN-SPLIT
INTERFACE
101
5.2.2.1
A
SIMPLE
OPEN-SPLIT
COUPLING
103
5.2.2.2
OPTIMIZATION
OF
THE
CARRIER-GAS
FLOW
103
CONTENTS
9
5.2.3
THE
CLASSICAL
JET-SEPARATOR
104
5.3
METHODS
FOR
TESTING
GC-MS
INTERFACES
106
5.3.1
TEST
FOR
UNIFORM
HEATING
106
5.3.2
TESTS
FOR
REACTIVE
OR
ADSORPTIVE
SURFACES
107
5.4
LITERATURE
109
6.
QUANTITATIVE
ANALYSIS
AND
QUALITY
CONTROL
6.1
MASS
SPECTROMETRY
AND
QUANTITATIVE
ANALYSIS
111
6.2
PREPARATION
FOR
QUANTITATIVE
ANALYSIS
113
6.2.1
MONITORING
THE
LINEAR
RANGE
113
6.2.2
SELECTION
CRITERIA
FOR
INTERNAL
REFERENCE
STANDARDS
115
6.2.3
ISOTOPE-LABELLED
COMPOUNDS
AS
CLEAN-UP
STANDARDS
118
6.2.4
ADAPTATION
OF
THE
GAS
CHROMATOGRAPHIC
SEPARATION
118
6.2.5
SAMPLE
PURITY
121
6.2.6
DERIVATIZATION
122
6.2.6.1
DERIVATIZATION
WITH
DIAZOMETHANE
123
6.2.6.2
TRIMETHYLSILYLETHER
DERIVATIVES
123
6.2.6.3
EXTRACTIVE
ACYLATION
124
6.3
PERFORMING
QUANTITATIVE
ANALYSIS
125
6.3.1
IDENTIFICATION
CRITERIA
126
6.3.2
QUANTIFICATION
CRITERIA
128
6.3.3
INTEGRATION
PROBLEMS
129
6.3.4
PRINCIPLES
OF
QUANTIFICATION
CALCULATIONS
131
6.4
ANALYSIS
REPORT
AND
DATA
STORAGE
134
6.5
LITERATURE
137
7.
COMPUTER-BASED
LIBRARY
SEARCH
AND
INTERPRETATION
OF
MASS
SPECTRA
7.1
WHY
ARE
LIBRARY
SEARCH
PROGRAMS
IMPORTANT?
138
7.2
PRINCIPLES
OF
SEARCH
PROGRAMS
139
7.2.1
SELECTION
OF
SIGNIFICANT
MASSES
139
7.2.2
SEARCH
ALGORITHMS
142
7.2.3
IMPORTANT
FACTORS
FOR
A
SUCCESSFUL
LIBRARY
SEARCH
145
7.2.3.1
QUALITY
OF
SPECTRA
IN
THE
LIBRARY
145
7.2.3.2
ACQUISITION
CONDITIONS
FOR
SAMPLE
SPECTRA
145
7.2.4
INTERPRETATION
OF
SEARCH
RESULTS
147
7.2.5
EXAMPLES
OF
LIBRARY
SEARCH
RESULTS
148
7.3
COMPUTER
PROGRAMS
FOR
THE
ELUCIDATION
OF
PARTIAL
STRUCTURES
153
7.3.1
EXAMPLE
OF
A
SPECTRUM
SEARCH
OF
A
COMPOUND
NOT
IN
THE
LIBRARY
155
7.4
LITERATURE
158
10
CONTENTS
8.
TROUBLESHOOTING
AND
MAINTENANCE
8.1
THE
COMPLEXITY
COMPLICATES
TROUBLESHOOTING
161
8.2
GAS
CHROMATOGRAPH
162
8.2.1
MAINTENANCE
162
8.2.2
TROUBLESHOOTING
163
8.3
VACUUM
SYSTEM
166
8.3.1
MAINTENANCE
166
8.3.1.1
ROUGH-VACUUM
PUMPS
166
8.3.1.2
DIFFUSION
PUMPS
167
8.2.1.3
TURBOMOLECULAR
PUMPS
168
8.3.2
TROUBLESHOOTING
168
8.3.2.1
INSUFFICIENT
VACUUM
169
8.3.2.2
CONTAMINATED
BACKGROUND
171
8.3.2.2.1
PUMP
OILS
173
83.2.2.2
VALVES
174
8.3.2.23
PLASTICIZERS
AND
CALIBRATION
COMPOUND
176
83.2.2.4
HIGH
AND
UNCHARACTERISTIC
BACKGROUND
176
8.3.3
CLEANING
OF
SURFACES
AND
VALVES
177
8.4
ION
SOURCE
179
8.4.1
MAINTENANCE
179
8.4.1.1
VENTING
A
MASS
SPECTROMETER
179
8.4.1.2
DISMANTLING
THE
ION
SOURCE
180
8.4.13
CLEANING
OF
METAL
PARTS
181
8.4.1.4
CLEANING
OF
INSULATORS
182
8.4.2
TROUBLESHOOTING
183
8.5
QUADRUPOLE
184
8.5.1
MAINTENANCE
184
8.5.2
TROUBLESHOOTING
185
8.6
SENSITIVITY
TESTS
187
8.6.1
WHAT
IS
IMPORTANT?
187
8.6.2
SUPPLIER
TESTS
188
8.6.3
IN-HOUSE
TESTING
PROCEDURES
188
8.7
LITERATURE
189
INDEX
191 |
| any_adam_object | 1 |
| author | Oehme, Michael 1950- |
| author_GND | (DE-588)109960599 |
| author_facet | Oehme, Michael 1950- |
| author_role | aut |
| author_sort | Oehme, Michael 1950- |
| author_variant | m o mo |
| building | Verbundindex |
| bvnumber | BV012121201 |
| callnumber-first | Q - Science |
| callnumber-label | QD79 |
| callnumber-raw | QD79.C45 |
| callnumber-search | QD79.C45 |
| callnumber-sort | QD 279 C45 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 9800 |
| classification_tum | CHE 247f CHE 234f |
| ctrlnum | (OCoLC)42290036 (DE-599)BVBBV012121201 |
| dewey-full | 543/.0873 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543/.0873 |
| dewey-search | 543/.0873 |
| dewey-sort | 3543 3873 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| format | Book |
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| id | DE-604.BV012121201 |
| illustrated | Illustrated |
| indexdate | 2024-08-19T00:23:15Z |
| institution | BVB |
| isbn | 3778526022 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008208677 |
| oclc_num | 42290036 |
| open_access_boolean | |
| owner | DE-703 DE-M49 DE-BY-TUM DE-1029 DE-1046 |
| owner_facet | DE-703 DE-M49 DE-BY-TUM DE-1029 DE-1046 |
| physical | 195 S. graph. Darst. |
| publishDate | 1998 |
| publishDateSearch | 1998 |
| publishDateSort | 1998 |
| publisher | Hüthig |
| record_format | marc |
| series2 | Desk library of chemistry |
| spelling | Oehme, Michael 1950- Verfasser (DE-588)109960599 aut Practical introduction to GC-MS analysis with quadrupoles by Michael Oehme Heidelberg Hüthig 1998 195 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Desk library of chemistry Literaturangaben. - Dt. Ausg. u.d.T.: Oehme, Michael: Praktische Einführung in die GC-MS-Analytik mit Quadrupolen Gas chromatography Gas chromatography Instruments Calibration Gas chromatography Instruments Maintenance and repair Mass spectrometers Calibration Mass spectrometers Maintenance and repair Mass spectrometry GC-MS (DE-588)4414891-4 gnd rswk-swf Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Quadrupolmassenspektrometrie (DE-588)4176579-5 gnd rswk-swf GC-MS (DE-588)4414891-4 s Quadrupolmassenspektrometrie (DE-588)4176579-5 s DE-604 Gaschromatographie (DE-588)4019330-5 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008208677&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Oehme, Michael 1950- Practical introduction to GC-MS analysis with quadrupoles Gas chromatography Gas chromatography Instruments Calibration Gas chromatography Instruments Maintenance and repair Mass spectrometers Calibration Mass spectrometers Maintenance and repair Mass spectrometry GC-MS (DE-588)4414891-4 gnd Gaschromatographie (DE-588)4019330-5 gnd Quadrupolmassenspektrometrie (DE-588)4176579-5 gnd |
| subject_GND | (DE-588)4414891-4 (DE-588)4019330-5 (DE-588)4176579-5 |
| title | Practical introduction to GC-MS analysis with quadrupoles |
| title_auth | Practical introduction to GC-MS analysis with quadrupoles |
| title_exact_search | Practical introduction to GC-MS analysis with quadrupoles |
| title_full | Practical introduction to GC-MS analysis with quadrupoles by Michael Oehme |
| title_fullStr | Practical introduction to GC-MS analysis with quadrupoles by Michael Oehme |
| title_full_unstemmed | Practical introduction to GC-MS analysis with quadrupoles by Michael Oehme |
| title_short | Practical introduction to GC-MS analysis with quadrupoles |
| title_sort | practical introduction to gc ms analysis with quadrupoles |
| topic | Gas chromatography Gas chromatography Instruments Calibration Gas chromatography Instruments Maintenance and repair Mass spectrometers Calibration Mass spectrometers Maintenance and repair Mass spectrometry GC-MS (DE-588)4414891-4 gnd Gaschromatographie (DE-588)4019330-5 gnd Quadrupolmassenspektrometrie (DE-588)4176579-5 gnd |
| topic_facet | Gas chromatography Gas chromatography Instruments Calibration Gas chromatography Instruments Maintenance and repair Mass spectrometers Calibration Mass spectrometers Maintenance and repair Mass spectrometry GC-MS Gaschromatographie Quadrupolmassenspektrometrie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008208677&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT oehmemichael practicalintroductiontogcmsanalysiswithquadrupoles |