Polymer synthesis and characterization: a laboratory manual
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
San Diego [u.a.]
Acad. Press
1998
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVII, 212 S. Ill., graph. Darst. |
| ISBN: | 012618240X |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804126717257711616 |
|---|---|
| adam_text | : . . . : * M M - : * * : * ; * * * * ; : * - . * : : : : OLYMER
SYNTHESIS AND CHARACTERIZATION I ** %|;F * *. ** : * *0 * : ;IS. * HI
: 9 ! M ** * * STANLEY R. SANDLER ELF ATOCHEM NORTH AMERICA, INC. KING
OF PRUSSIA, PENNSYLVANIA WOLF KARO CONSULTANT TO THE CHEMICAL INDUSTRY
HUNTINGTON VALLEY, PENNSYLVANIA JO-ANNE BONESTEEL ELF ATOCHEM NORTH
AMERICA, INC. KING OF PRUSSIA, PENNSYLVANIA ELI M. PEARCE POLYTECHNIC
UNIVERSITY BROOKLYN, NEW YORK ACADEMIC PRESS SAN DIEGO LONDON BOSTON NEW
YORK SYDNEY TOKYO TORONTO CONTENTS PREFACE XVII INTRODUCTION 1 SCALE OF
OPERATIONS AND MONITORING OF REACTIONS 1 SAFETY 2 WASTE DISPOSAL 2
LABORATORY RECORDS/NOTEBOOKS 2 SECTION I POLYMER SYNTHESIS A:
POLYMERIZATION OF STYRENE INTRODUCTION 7 EXPERIMENT 1 PREPARATION OF
POLYSTYRENE BY A FREE RADICAL POLYMERIZATION PROCESS 9 INTRODUCTION 9
APPLICABILITY 9 BULK POLYMERIZATION 10 SAFETY PRECAUTIONS 11 APPARATUS
11 REAGENTS AND MATERIALS 11 PROCEDURE 11 V NOTES 12 REFERENCES 12
EXPERIMENT 2 PREPARATION OF POLYSTYRENE BY AN EMULSION POLYMERIZATION
PROCESS 14 INTRODUCTION 14 APPARATUS 14 REAGENTS AND MATERIALS 15 SAFETY
PRECAUTIONS 15 PROCEDURE 15 NOTE 15 REFERENCES 15 EXPERIMENT 3
PREPARATION OF POLYSTYRENE BY AN ANIONIC POLYMERIZATION METHOD 17
INTRODUCTION 17 APPLICABILITY 19 SAFETY PRECAUTIONS 19 APPARATUS 19
REAGENTS AND MATERIALS 20 PROCEDURE 20 REFERENCES 20 EXPERIMENT 4
PREPARATION OF POLYSTYRENE BY A CATIONIC POLYMERIZATION PROCESS 22
INTRODUCTION 22 APPLICABILITY 22 SAFETY PRECAUTIONS 23 APPARATUS 23
REAGENTS AND MATERIALS 24 PROCEDURE 24 NOTES 24 REFERENCES 25 B:
POLYMERIZATION OF ACRYLIC ESTERS INTRODUCTION 27 REACTANTS AND REACTION
CONDITIONS 27 INHIBITORS AND THEIR REMOVAL 27 REACTION TEMPERATURE 28
CONTENTS VII CHAIN-TRANSFER AGENTS 28 INITIATORS 28 PROCEDURES 29 BULK
POLYMERIZATION 29 SUSPENSION POLYMERIZATION 30 EMULSION POLYMERIZATION
31 REFERENCES 32 EXPERIMENT 5 BULK POLYMERIZATION OF METHYL
METHACRYLATE: A TEST TUBE DEMONSTRATION 35 INTRODUCTION 35 SAFETY
PRECAUTIONS 35 APPARATUS 36 REAGENTS AND MATERIALS 36 PROCEDURE 36 NOTES
36 REFERENCES 37 EXPERIMENT 6 SUSPENSION POLYMERIZATION OF METHYL
METHACRYLATE 38 INTRODUCTION 38 SAFETY PRECAUTIONS 38 APPARATUS 38
REAGENTS AND MATERIALS 39 PROCEDURE 39 NOTES 39 REFERENCES 40 EXPERIMENT
7 REDOX EMULSION POLYMERIZATION OF ETHYL ACRYLATE 41 INTRODUCTION 41
SAFETY PRECAUTIONS 41 APPARATUS 41 REAGENTS AND MATERIALS 42 PROCEDURE
42 NOTES 43 REFERENCES 43 C: POLYAMIDES INTRODUCTION 45 REFERENCES 47
VIII CONTENTS EXPERIMENT 8 PREPARATION OF POLY(HEXAMETHYLENESEBACAMIDE)
(NYLON 6-10) BY AN INTERFACIAL POLYMERIZATION TECHNIQUE 49 INTRODUCTION
49 BACKGROUND 49 SAFETY PRECAUTIONS 49 APPARATUS 50 REAGENTS AND
MATERIALS 50 PROCEDURE 50 NOTES 50 REFERENCES 51 D: POLYESTERS
INTRODUCTION 53 REFERENCES 56 EXPERIMENT 9 PREPARATION OF
POIY(L,4-BUTYLENE ISOPHTHALATE) 59 INTRODUCTION 59 SAFETY PRECAUTIONS 59
APPARATUS 59 REAGENTS AND MATERIALS 59 PROCEDURE 60 NOTE 60 REFERENCE 60
E: EPOXY RESINS INTRODUCTION 61 SAFETY PRECAUTIONS 62 ANALYSIS OF EPOXY
RESINS 63 CONDENSATION-ELIMINATION REACTIONS 63 EPOXY COMPOUNDS VIA
EPICHLOROHYDRIN 63 CURING-POLYMERIZATION REACTIONS OF EPOXY COMPOUNDS
AND RESINS 64 REFERENCES 66 EXPERIMENT 10 PREPARATION OF A CURED EPOXY
RESIN BY THE ROOM TEMPERATURE REACTION OF BISPHENOL A DIGLYCIDYL ETHER
WITH POLYAMINES 69 SAFETY PRECAUTIONS 69 CONTENTS IX APPARATUS 69
REAGENTS AND MATERIALS 69 PROCEDURE 70 REPORT 70 NOTES 70 F:
POLYMERIZATION OF VINYL ACETATE INTRODUCTION 71 EXPERIMENT 11 SEEDED
EMULSION TERPOLYMERIZATION OF VINYL ACETATE, BUTYL ACRYLATE, AND VINYL
NEODECANOATE WITH GRADUAL MONOMER AND INITIATOR ADDITIONS 73 PRINCIPLE
73 COMPOSITION 74 SAFETY PRECAUTIONS 74 APPARATUS 74 REAGENTS AND
MATERIALS 75 PROCEDURE 75 REPORT 76 REFERENCE 76 EXPERIMENT 12
PREPARATION OF POLYVINYL ALCOHOL) BY THE ALCOHOLYSIS OF POLYVINYL
ACETATE) 77 INTRODUCTION 77 BACKGROUND 77 APPLICABILITY 78 SAFETY
PRECAUTIONS 78 APPARATUS 78 REAGENTS AND MATERIALS 79 PROCEDURE 79 NOTE
79 REFERENCES 80 SECTION II POLYMER CHARACTERIZATION EXPERIMENT 13
NUCLEAR MAGNETIC RESONANCE 83 INTRODUCTION 83 PRINCIPLES 83 THEORY 83
POLYMER CHARACTERIZATION 86 X CONTENTS ACCURACY AND PRECISION 91 SAFETY
PRECAUTIONS 92 APPARATUS 92 REAGENTS AND MATERIALS 92 PROCEDURE 92 EPOXY
KINETICS: CONDENSATION REACTION 93 POLYMER TACTICITY 93 CALCULATIONS 95
EPOXY KINETICS 95 POLYMER TACTICITY 95 REPORT 95 NOTES 95 REFERENCES 96
EXPERIMENT 14 INFRARED SPECTROSCOPY 98 INTRODUCTION 98 BACKGROUND 98
ELECTROMAGNETIC RADIATION SPECTRUM 98 THEORY 100 POLYMER
CHARACTERIZATION 100 SAMPLE PREPARATION TECHNIQUES APPLIED TO POLYMERS
103 APPLICABILITY 104 ACCURACY AND PRECISION 104 SAFETY PRECAUTIONS 104
APPARATUS 104 REAGENTS AND MATERIALS 105 PROCEDURE 105 FUNDAMENTAL
EQUATION 105 CALCULATIONS 105 REPORT 106 REFERENCES 106 EXPERIMENT 15
THERMOGRAVIMETRIC ANALYSIS 108 INTRODUCTION 108 PRINCIPLE 108
QUALITATIVE IDENTIFICATION 109 COMPOSITIONAL ANALYSIS 109 APPLICABILITY
112 ACCURACY AND PRECISION 112 SAFETY PRECAUTIONS 112 APPARATUS 112
REAGENTS AND MATERIALS 112 PROCEDURE 113 CONTENTS XI EXPERIMENT 15A:
POLYMER FINGERPRINTING 114 PURPOSE 114 EXPERIMENT 15B: POLYMER
DEGRADATION IN DIFFERENT ATMOSPHERES 115 FUNDAMENTAL EQUATIONS 116
CALCULATIONS 116 REPORT 117 NOTES 117 REFERENCES 118 EXPERIMENT 16
DIFFERENTIAL SCANNING CALORIMETRY 120 INTRODUCTION BACKGROUND THEORY 120
120 120 HEAT CAPACITY 122 ENTHALPY 122 GLASS TRANSITION 122 MELTING AND
CRYSTALLIZATION 123 POLYMERIZATION AND HEATS OF REACTION 124
APPLICATIONS 124 ACCURACY AND PRECISION 124 SAFETY PRECAUTIONS 125
APPARATUS 125 REAGENTS AND MATERIALS 125 PREPARATION 125 PROCEDURE 125
FIRST-ORDER TRANSITION OF POLY(AMIDE) 126 FUNDAMENTAL EQUATIONS 127
CALCULATIONS 127 REPORT 128 NOTES 128 REFERENCES 128 EXPERIMENT 17
DILUTE SOLUTION VISCOSITY OF POLYMERS 131 INTRODUCTION 131 PRINCIPLE 131
FLEXIBLE CHAINS 133 EVALUATION OF MOLECULAR WEIGHT 133 BRANCHED POLYMERS
134 COPOLYMERS 134 POLYELECTROLYTES 134 APPLICABILITY 134 ACCURACY AND
PRECISION 134 SAFETY PRECAUTIONS 134 APPARATUS 135 REAGENTS AND
MATERIALS 135 PREPARATION 135 PROCEDURE 136 FUNDAMENTAL EQUATIONS 137
CALCULATIONS 137 REPORT 138 NOTES 138 REFERENCES 138 EXPERIMENT 18 GEL
PERMEATION CHROMATOGRAPHY 140 INTRODUCTION 140 THEORY 140 BACKGROUND 140
SIZE EXCLUSION 141 COLUMN EFFICIENCY 143 COLUMN PACKINGS 143 ELUENTS 144
DETECTORS 144 APPLICABILITY 145 ACCURACY AND PRECISION 146 SAFETY
PRECAUTIONS 146 APPARATUS 146 REAGENTS AND MATERIALS 146 PREPARATION 147
PROCEDURE 148 INSTRUMENT SETUP 148 FUNDAMENTAL EQUATIONS 148
CALCULATIONS 149 REPORT 149 NOTES 150 REFERENCES 151 EXPERIMENT 19 LIGHT
SCATTERING 152 INTRODUCTION 152 THEORY 152 BACKGROUND 152 LIGHT
SCATTERING FROM A LIQUID 15 3 SCATTERING FROM A SOLUTION OF SMALL
PARTICLES 153 SCATTERING FROM A SOLUTION OF LARGER PARTICLES 154
TREATMENT OF DATA: GENERAL EQUATION AND ZIMM PLOT INSTRUMENTATION 155
CONTENTS XIII APPLICABILITY 156 ACCURACY AND PRECISION 156 SAFETY
PRECAUTIONS 156 APPARATUS 157 REAGENTS AND MATERIALS 157 PREPARATION 157
PROCEDURE 158 CALIBRATION OF LIGHT SCATTERING PHOTOMETER 159 MEASURING
THE SCATTERING OF THE PURE SOLVENT 159 MEASURING THE SCATTERING OF THE
REFERENCE MATERIAL 159 MEASURING THE SCATTERING OF THE POLYMER SOLUTIONS
159 FUNDAMENTAL EQUATIONS 159 CALCULATIONS 160 REPORT 160 NOTES 160
REFERENCES 161 EXPERIMENT 20 END GROUP ANALYSIS 163 INTRODUCTION 163
THEORY 163 MOLECULAR WEIGHT DETERMINATION 163 LINEAR POLYMERS 164
CONDENSATION POLYMERS 164 VINYL POLYMERS 164 OTHER FUNCTIONAL GROUPS 165
METHODOLOGY 166 APPLICABILITY 166 ACCURACY AND PRECISION 166 SAFETY
PRECAUTIONS 166 APPARATUS 166 PROCEDURE I: AMINE END GROUPS 166
PROCEDURE II: HYDROXYL END GROUPS 167 REAGENTS AND MATERIALS 167
PROCEDURE I: AMINE END GROUPS 167 PROCEDURE II: HYDROXYL END GROUPS 167
SAMPLE PREPARATION 167 PROCEDURE I: AMINE END GROUPS 167 PROCEDURE II:
HYDROXYL END GROUPS 168 PROCEDURE 168 PROCEDURE I: AMINE END GROUPS 168
PROCEDURE II: HYDROXYL END GROUPS 169 FUNDAMENTAL EQUATIONS 170
PROCEDURE I: AMINE END GROUPS 170 PROCEDURE II: HYDROXYL END GROUPS 170
XIV CONTENTS CALCULATIONS 170 PROCEDURE I: AMINE END GROUPS 170
PROCEDURE II: HYDROXYL END GROUPS 170 REPORT 170 PROCEDURE I: AMINE END
GROUPS 170 PROCEDURE II: HYDROXYL END GROUPS 171 NOTE 171 REFERENCES 171
EXPERIMENT 21 X-RAY DIFFRACTION 173 INTRODUCTION 173 PRINCIPLE 173
THEORY 173 AMORPHOUS SAMPLES 175 DEGREE OF ORIENTATION 175 CRYSTALLINE
SAMPLES 176 EXPERIMENTAL METHODS 177 APPLICABILITY 178 ACCURACY AND
PRECISION 178 SAFETY PRECAUTIONS 178 APPARATUS 179 REAGENTS AND
MATERIALS 179 PREPARATION 180 SAMPLE MOUNTING 180 FIBER PREPARATION 180
PROCEDURE 180 START-UP 180 WIDE ANGLE EXPERIMENTS 180 SMALL ANGLE
EXPERIMENTS 181 FUNDAMENTAL EQUATIONS 181 CALCULATIONS 181 REPORT 182
NOTES 183 REFERENCES 183 EXPERIMENT 22 OPTICAL MICROSCOPY 185
INTRODUCTION 185 BACKGROUND 185 POLYMER MORPHOLOGY: SINGLE CRYSTALS 185
THEORY 186 IMAGING MODES 188 POLARIZED LIGHT 188 MEASUREMENT OF
REFRACTIVE INDEX 190 CONTENTS XV DYNAMIC MICROSCOPY 191 SAMPLE
PREPARATION 191 APPLICABILITY 192 ACCURACY AND PRECISION 192 SAFETY
PRECAUTIONS 192 APPARATUS 192 REAGENTS AND MATERIALS 193 PREPARATION 193
PROCEDURE 193 MICROSCOPE SETUP 193 CRYSTALLIZATION AND MELTING OF LINEAR
POLY(ETHYLENE) 193 BIREFRINGENCE 194 FUNDAMENTAL EQUATIONS 195
CALCULATIONS 195 REPORT 196 NOTES 196 REFERENCES 196 EXPERIMENT 23
DYNAMIC MECHANICAL ANALYSIS 198 INTRODUCTION 198 PRINCIPLE 198 THE
MODULUS CURVE 198 THEORY 199 AMORPHOUS POLYMERS 201 CRYSTALLINE POLYMERS
202 ELASTOMERS 203 APPLICABLILITY 203 ACCURACY AND PRECISION 203 SAFETY
PRECAUTIONS 203 APPARATUS 203 REAGENTS AND MATERIALS 204 PREPARATION 204
PROCEDURE 204 CALIBRATION 204 MEASUREMENT 204 FUNDAMENTAL EQUATIONS 205
CALCULATIONS 205 REPORT 205 NOTES 205 REFERENCES 206 INDEX 207
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| id | DE-604.BV012112683 |
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| indexdate | 2024-07-09T18:21:53Z |
| institution | BVB |
| isbn | 012618240X |
| language | English |
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| owner_facet | DE-703 DE-29T |
| physical | XVII, 212 S. Ill., graph. Darst. |
| publishDate | 1998 |
| publishDateSearch | 1998 |
| publishDateSort | 1998 |
| publisher | Acad. Press |
| record_format | marc |
| spelling | Polymer synthesis and characterization a laboratory manual Stanley R. Sandler ... San Diego [u.a.] Acad. Press 1998 XVII, 212 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymerization Laboratory manuals Polymers Analysis Laboratory manuals Chemische Synthese (DE-588)4133806-6 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Spektroskopie (DE-588)4056138-0 gnd rswk-swf Polymere (DE-588)4046699-1 s Chemische Synthese (DE-588)4133806-6 s DE-604 Spektroskopie (DE-588)4056138-0 s Sandler, Stanley R. Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008201573&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Polymer synthesis and characterization a laboratory manual Polymerization Laboratory manuals Polymers Analysis Laboratory manuals Chemische Synthese (DE-588)4133806-6 gnd Polymere (DE-588)4046699-1 gnd Spektroskopie (DE-588)4056138-0 gnd |
| subject_GND | (DE-588)4133806-6 (DE-588)4046699-1 (DE-588)4056138-0 |
| title | Polymer synthesis and characterization a laboratory manual |
| title_auth | Polymer synthesis and characterization a laboratory manual |
| title_exact_search | Polymer synthesis and characterization a laboratory manual |
| title_full | Polymer synthesis and characterization a laboratory manual Stanley R. Sandler ... |
| title_fullStr | Polymer synthesis and characterization a laboratory manual Stanley R. Sandler ... |
| title_full_unstemmed | Polymer synthesis and characterization a laboratory manual Stanley R. Sandler ... |
| title_short | Polymer synthesis and characterization |
| title_sort | polymer synthesis and characterization a laboratory manual |
| title_sub | a laboratory manual |
| topic | Polymerization Laboratory manuals Polymers Analysis Laboratory manuals Chemische Synthese (DE-588)4133806-6 gnd Polymere (DE-588)4046699-1 gnd Spektroskopie (DE-588)4056138-0 gnd |
| topic_facet | Polymerization Laboratory manuals Polymers Analysis Laboratory manuals Chemische Synthese Polymere Spektroskopie |
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