Crystallographic instrumentation:
Gespeichert in:
| Hauptverfasser: | , , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Oxford [u.a.]
Oxford Univ. Press
1998
|
| Schriftenreihe: | International Union of Crystallography: International Union of Crystallography monographs on crystallography
7 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XI, 309 S. Ill., graph. Darst. |
| ISBN: | 0198559275 |
Internformat
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| 245 | 1 | 0 | |a Crystallographic instrumentation |c L. A. Aslanov and G. V. Fetisov and J. A. K. Howard |
| 264 | 1 | |a Oxford [u.a.] |b Oxford Univ. Press |c 1998 | |
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| 490 | 1 | |a International Union of Crystallography: International Union of Crystallography monographs on crystallography |v 7 | |
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Datensatz im Suchindex
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| adam_text | CRYSTALLOGRAPHIC INSTRUMENTATION L. A. ASLANOV AND G. V. FETISOV
DEPARTMENT OF CHEMISTRY MOSCOW STATE UNIVERSITY, RUSSIAN FEDERATION AND
J. A. K. HOWARD DEPARTMENT OF CHEMISTRY UNIVERSITY OF DURHAM, GREAT
BRITAIN EDITED BY J. A. K. HOWARD INTERNATIONAL UNION OF CRYSTALLOGRAPHY
OXFORD UNIVERSITY PRESS 1998 CONTENTS INTRODUCTION XIII ABBREVIATIONS XV
1 RADIATION USED IN CRYSTALLOGRAPHY 1 1.1 CONVENTIONAL X-RAYS 1 1.1.1
WHITE RADIATION 1 1.1.2 CHARACTERISTIC RADIATION 2 1.1.3 FLUORESCENT
RADIATION 6 1.2 SYNCHROTRON RADIATION 7 1.3 GENERAL PROPERTIES OF X-RAYS
11 1.3.1 ABSORPTION OF X-RAYS 12 1.3.2 SCATTERING OF X-RAYS 15 2
PRINCIPLE OF DIFFRACTION EXPERIMENT 20 2.1 CONCEPT OF THE EWALD
CONSTRUCTION 20 2.2 GEOMETRIES FOR DIFFRACTION MEASUREMENTS 23 2.2.1
SINGLE CRYSTAL DIFFRACTOMETER 29 2.2.2 METHODS FOR MEASUREMENT OF
REFLECTION-INTEGRATED INTENSITY IN SINGLE-CRYSTAL DIFFRACTOMETRY 43
2.2.3 LAUE METHOD.GEOMETRY 52 2.2.4 POWDER DIFFRACTION GEOMETRY 56 2.2.5
THE DEBYE-SCHERRER METHOD (PARALLEL BEAM GEOMETRY) 59 2.2.6 FOCUSING
TECHNIQUES 60 3 FUNDAMENTAL TECHNIQUES FOR X-RAY DIFFRACTOMETRY 68 3.1
TOOLS FOR X-RAY GENERATION 68 3.1.1 X-RAY TUBE 68 3.1.2 SYNCHROTRON.
INSERTION DEVICES . 76 3.2 CONDITIONING OF X-RAY BEAMS 86 3.3 RADIATION
MONOCHROMATIZATION 88 3.3.1 BETA-FILTERS 88 3.3.2 CRYSTAL-MONOCHROMATORS
90 3.4 DETECTION OF X-RAYS 95 3.4.1 X-RAY DETECTORS 99 3.5 X-RAY
DIFFRACTOMETERS 113 3.5.1 FOUR-CIRCLE SINGLE-CRYSTAL DIFFRACTOMETERS 114
X CONTENTS 4 SINGLE-CRYSTAL X-RAY DIFFRACTOMETRY 121 4.1 INSTRUMENT
PREPARATION FOR X-RAY CRYSTAL STRUCTURE ANALYSIS 123 4.1.1 ADJUSTMENT
OF FOUR-CIRCLE X-RAY GONIOMETER 123 4.1.2 ADJUSTMENT OF THE RADIATION
DETECTION CHAIN 127 4.1.3 CHECKING OF THE DIFFRACTOMETER STABILITY 129
4.2 REFLECTION SCAN PARAMETERS 135 4.2.1 SCAN-PARAMETER ESTIMATION FROM
2-DIMENSIONAL REFLECTION INTENSITY MAPS 136 4.3 RADIATION CHOICE 142 5
SINGLE-CRYSTAL DIFFRACTION DATA COLLECTION AND PRIMARY PROCESSING 144
5.1 THE FOUR-CIRCLE DIFFRACTOMETER METHOD 144 5.1.1 STARTING THE
REFLECTION SEARCH 144 5.1.2 REFLECTION CENTRING 147 5.1.3 ORIENTATION
MATRIX 148 5.1.4 INDEXING OF REFLECTIONS 154 5.1.5 MEASUREMENT OF
INTEGRATED INTENSITIES 158 5.1.6 BACKGROUND SUBTRACTION 160 5.1.7
DIFFRACTION DATA COLLECTION 169 5.2 LAUE METHOD 173 5.2.1 DETERMINATION
OF THE CRYSTAL ORIENTATION 173 5.2.2 INTENSITY MEASUREMENTS . 176 6
PRIMARY DATA REDUCTION AND ERROR CORRECTION IN SINGLE-CRYSTAL
DIFFRACTOMETRY 183 6.1 ABSORPTION CORRECTION 184 6.1.1 SEMI-EMPIRICAL
ABSORPTION CORRECTION 187 6.1.2 INTEGRATION METHODS 193 6.2 SIMULTANEOUS
REFLECTIONS 2LL 6.2.1 MODELLING OF THE SIMULTANEOUS REFLECTION EFFECT
220 6.3 THERMAL DIFFUSE SCATTERING 224 6.3.1 CALCULATION OF TDS
CORRECTION USING THE CRYSTAL ELASTICITY CONSTANTS 226 6.4 MATHEMATICAL
MODELLING FOR TDS CORRECTION 228 6.4.1 ALLOWANCE FOR CRYSTAL MOSAICITY
IN THE MODEL 235 6.4.2 ALLOWANCE FOR TDS IN THE MODEL 238 6.4.3
MATHEMATICAL REDUCTION METHOD 241 7 DEFECTS IN CRYSTAL AND THEIR
INFLUENCE ON X-RAY STRUCTURE ANALYSIS 250 7.1 DEFECTS IN CRYSTALS 251
CONTENTS XI 7.1.1 X-RAY DIFFRACTION FROM CRYSTALS WITH DEFECTS 252 7.2
PREPARATION OF A SINGLE-CRYSTAL SAMPLE FOR DIFFRACTION DATA COLLECTION .
257 7.2.1 CRYSTAL LATTICE DEFECTS GENERATED BY SAMPLE PREPARATION AND
THEIR INFLUENCE UPON X-RAY DIFFRACTION 260 7.3 EXTINCTION EFFECTS AND
THE EXTINCTION CORRECTION PROBLEM 266 7.4 SAMPLES FOR X-RAY POWDER
DIFFRACTION 272 8 AUXILIARY METHODS 273 8.1 LOW-TEMPERATURE DEVICES 273
8.2 HIGH-TEMPERATURE DEVICES 279 8.3 HIGH-PRESSURE DEVICES 282 8.4 LASER
ACTION ON THE CRYSTAL 290 REFERENCES 295 SUBJECT INDEX 305
|
| any_adam_object | 1 |
| author | Aslanov, L. A. Fetisov, G. V. Howard, J. A. K. |
| author_facet | Aslanov, L. A. Fetisov, G. V. Howard, J. A. K. |
| author_role | aut aut aut |
| author_sort | Aslanov, L. A. |
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| building | Verbundindex |
| bvnumber | BV012080398 |
| classification_rvk | UQ 5100 UQ 5600 |
| classification_tum | CHE 312f GEO 425f CHE 220f |
| ctrlnum | (OCoLC)845029399 (DE-599)BVBBV012080398 |
| dewey-full | 548.83 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 548 - Crystallography |
| dewey-raw | 548.83 |
| dewey-search | 548.83 |
| dewey-sort | 3548.83 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Geowissenschaften Physik Chemie |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T18:21:20Z |
| institution | BVB |
| isbn | 0198559275 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008179014 |
| oclc_num | 845029399 |
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| owner_facet | DE-703 DE-20 DE-91G DE-BY-TUM DE-29T DE-188 |
| physical | XI, 309 S. Ill., graph. Darst. |
| publishDate | 1998 |
| publishDateSearch | 1998 |
| publishDateSort | 1998 |
| publisher | Oxford Univ. Press |
| record_format | marc |
| series | International Union of Crystallography: International Union of Crystallography monographs on crystallography |
| series2 | International Union of Crystallography: International Union of Crystallography monographs on crystallography |
| spelling | Aslanov, L. A. Verfasser aut Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard Oxford [u.a.] Oxford Univ. Press 1998 XI, 309 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier International Union of Crystallography: International Union of Crystallography monographs on crystallography 7 Kristallstruktur (DE-588)4136176-3 gnd rswk-swf Röntgendiffraktometrie (DE-588)4336833-5 gnd rswk-swf Röntgenstreuung (DE-588)4178324-4 gnd rswk-swf Kristallstruktur (DE-588)4136176-3 s Röntgenstreuung (DE-588)4178324-4 s DE-604 Röntgendiffraktometrie (DE-588)4336833-5 s Fetisov, G. V. Verfasser aut Howard, J. A. K. Verfasser aut International Union of Crystallography: International Union of Crystallography monographs on crystallography 7 (DE-604)BV005455767 7 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008179014&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Aslanov, L. A. Fetisov, G. V. Howard, J. A. K. Crystallographic instrumentation International Union of Crystallography: International Union of Crystallography monographs on crystallography Kristallstruktur (DE-588)4136176-3 gnd Röntgendiffraktometrie (DE-588)4336833-5 gnd Röntgenstreuung (DE-588)4178324-4 gnd |
| subject_GND | (DE-588)4136176-3 (DE-588)4336833-5 (DE-588)4178324-4 |
| title | Crystallographic instrumentation |
| title_auth | Crystallographic instrumentation |
| title_exact_search | Crystallographic instrumentation |
| title_full | Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard |
| title_fullStr | Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard |
| title_full_unstemmed | Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard |
| title_short | Crystallographic instrumentation |
| title_sort | crystallographic instrumentation |
| topic | Kristallstruktur (DE-588)4136176-3 gnd Röntgendiffraktometrie (DE-588)4336833-5 gnd Röntgenstreuung (DE-588)4178324-4 gnd |
| topic_facet | Kristallstruktur Röntgendiffraktometrie Röntgenstreuung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008179014&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV005455767 |
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