Verfügbarkeit: Crystallographic instrumentation

Crystallographic instrumentation:

Gespeichert in:

Bibliographische Detailangaben
Hauptverfasser:	Aslanov, L. A. (VerfasserIn), Fetisov, G. V. (VerfasserIn), Howard, J. A. K. (VerfasserIn)
Format:	Buch
Sprache:	English
Veröffentlicht:	Oxford [u.a.] Oxford Univ. Press 1998
Schriftenreihe:	International Union of Crystallography: International Union of Crystallography monographs on crystallography 7
Schlagworte:	Kristallstruktur Röntgendiffraktometrie Röntgenstreuung
Online-Zugang:	Inhaltsverzeichnis
Beschreibung:	XI, 309 S. Ill., graph. Darst.
ISBN:	0198559275

Internformat

MARC


LEADER	00000nam a2200000 cb4500
001	BV012080398
003	DE-604
005	19991122
007	t
008	980730s1998 ad\|\| \|\|\|\| 00\|\|\| eng d
020			\|a 0198559275 \|9 0-19-855927-5
035			\|a (OCoLC)845029399
035			\|a (DE-599)BVBBV012080398
040			\|a DE-604 \|b ger \|e rakddb
041	0		\|a eng
049			\|a DE-703 \|a DE-20 \|a DE-91G \|a DE-29T \|a DE-188
082	0		\|a 548.83
084			\|a UQ 5100 \|0 (DE-625)146522: \|2 rvk
084			\|a UQ 5600 \|0 (DE-625)146528: \|2 rvk
084			\|a CHE 312f \|2 stub
084			\|a GEO 425f \|2 stub
084			\|a CHE 220f \|2 stub
100	1		\|a Aslanov, L. A. \|e Verfasser \|4 aut
245	1	0	\|a Crystallographic instrumentation \|c L. A. Aslanov and G. V. Fetisov and J. A. K. Howard
264		1	\|a Oxford [u.a.] \|b Oxford Univ. Press \|c 1998
300			\|a XI, 309 S. \|b Ill., graph. Darst.
336			\|b txt \|2 rdacontent
337			\|b n \|2 rdamedia
338			\|b nc \|2 rdacarrier
490	1		\|a International Union of Crystallography: International Union of Crystallography monographs on crystallography \|v 7
650	0	7	\|a Kristallstruktur \|0 (DE-588)4136176-3 \|2 gnd \|9 rswk-swf
650	0	7	\|a Röntgendiffraktometrie \|0 (DE-588)4336833-5 \|2 gnd \|9 rswk-swf
650	0	7	\|a Röntgenstreuung \|0 (DE-588)4178324-4 \|2 gnd \|9 rswk-swf
689	0	0	\|a Kristallstruktur \|0 (DE-588)4136176-3 \|D s
689	0	1	\|a Röntgenstreuung \|0 (DE-588)4178324-4 \|D s
689	0		\|5 DE-604
689	1	0	\|a Röntgendiffraktometrie \|0 (DE-588)4336833-5 \|D s
689	1		\|5 DE-604
700	1		\|a Fetisov, G. V. \|e Verfasser \|4 aut
700	1		\|a Howard, J. A. K. \|e Verfasser \|4 aut
830		0	\|a International Union of Crystallography: International Union of Crystallography monographs on crystallography \|v 7 \|w (DE-604)BV005455767 \|9 7
856	4	2	\|m GBV Datenaustausch \|q application/pdf \|u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008179014&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA \|3 Inhaltsverzeichnis
999			\|a oai:aleph.bib-bvb.de:BVB01-008179014

Datensatz im Suchindex

_version_	1804126682636877824
adam_text	CRYSTALLOGRAPHIC INSTRUMENTATION L. A. ASLANOV AND G. V. FETISOV DEPARTMENT OF CHEMISTRY MOSCOW STATE UNIVERSITY, RUSSIAN FEDERATION AND J. A. K. HOWARD DEPARTMENT OF CHEMISTRY UNIVERSITY OF DURHAM, GREAT BRITAIN EDITED BY J. A. K. HOWARD INTERNATIONAL UNION OF CRYSTALLOGRAPHY OXFORD UNIVERSITY PRESS 1998 CONTENTS INTRODUCTION XIII ABBREVIATIONS XV 1 RADIATION USED IN CRYSTALLOGRAPHY 1 1.1 CONVENTIONAL X-RAYS 1 1.1.1 WHITE RADIATION 1 1.1.2 CHARACTERISTIC RADIATION 2 1.1.3 FLUORESCENT RADIATION 6 1.2 SYNCHROTRON RADIATION 7 1.3 GENERAL PROPERTIES OF X-RAYS 11 1.3.1 ABSORPTION OF X-RAYS 12 1.3.2 SCATTERING OF X-RAYS 15 2 PRINCIPLE OF DIFFRACTION EXPERIMENT 20 2.1 CONCEPT OF THE EWALD CONSTRUCTION 20 2.2 GEOMETRIES FOR DIFFRACTION MEASUREMENTS 23 2.2.1 SINGLE CRYSTAL DIFFRACTOMETER 29 2.2.2 METHODS FOR MEASUREMENT OF REFLECTION-INTEGRATED INTENSITY IN SINGLE-CRYSTAL DIFFRACTOMETRY 43 2.2.3 LAUE METHOD.GEOMETRY 52 2.2.4 POWDER DIFFRACTION GEOMETRY 56 2.2.5 THE DEBYE-SCHERRER METHOD (PARALLEL BEAM GEOMETRY) 59 2.2.6 FOCUSING TECHNIQUES 60 3 FUNDAMENTAL TECHNIQUES FOR X-RAY DIFFRACTOMETRY 68 3.1 TOOLS FOR X-RAY GENERATION 68 3.1.1 X-RAY TUBE 68 3.1.2 SYNCHROTRON. INSERTION DEVICES . 76 3.2 CONDITIONING OF X-RAY BEAMS 86 3.3 RADIATION MONOCHROMATIZATION 88 3.3.1 BETA-FILTERS 88 3.3.2 CRYSTAL-MONOCHROMATORS 90 3.4 DETECTION OF X-RAYS 95 3.4.1 X-RAY DETECTORS 99 3.5 X-RAY DIFFRACTOMETERS 113 3.5.1 FOUR-CIRCLE SINGLE-CRYSTAL DIFFRACTOMETERS 114 X CONTENTS 4 SINGLE-CRYSTAL X-RAY DIFFRACTOMETRY 121 4.1 INSTRUMENT PREPARATION FOR X-RAY CRYSTAL STRUCTURE ANALYSIS 123 4.1.1 ADJUSTMENT OF FOUR-CIRCLE X-RAY GONIOMETER 123 4.1.2 ADJUSTMENT OF THE RADIATION DETECTION CHAIN 127 4.1.3 CHECKING OF THE DIFFRACTOMETER STABILITY 129 4.2 REFLECTION SCAN PARAMETERS 135 4.2.1 SCAN-PARAMETER ESTIMATION FROM 2-DIMENSIONAL REFLECTION INTENSITY MAPS 136 4.3 RADIATION CHOICE 142 5 SINGLE-CRYSTAL DIFFRACTION DATA COLLECTION AND PRIMARY PROCESSING 144 5.1 THE FOUR-CIRCLE DIFFRACTOMETER METHOD 144 5.1.1 STARTING THE REFLECTION SEARCH 144 5.1.2 REFLECTION CENTRING 147 5.1.3 ORIENTATION MATRIX 148 5.1.4 INDEXING OF REFLECTIONS 154 5.1.5 MEASUREMENT OF INTEGRATED INTENSITIES 158 5.1.6 BACKGROUND SUBTRACTION 160 5.1.7 DIFFRACTION DATA COLLECTION 169 5.2 LAUE METHOD 173 5.2.1 DETERMINATION OF THE CRYSTAL ORIENTATION 173 5.2.2 INTENSITY MEASUREMENTS . 176 6 PRIMARY DATA REDUCTION AND ERROR CORRECTION IN SINGLE-CRYSTAL DIFFRACTOMETRY 183 6.1 ABSORPTION CORRECTION 184 6.1.1 SEMI-EMPIRICAL ABSORPTION CORRECTION 187 6.1.2 INTEGRATION METHODS 193 6.2 SIMULTANEOUS REFLECTIONS 2LL 6.2.1 MODELLING OF THE SIMULTANEOUS REFLECTION EFFECT 220 6.3 THERMAL DIFFUSE SCATTERING 224 6.3.1 CALCULATION OF TDS CORRECTION USING THE CRYSTAL ELASTICITY CONSTANTS 226 6.4 MATHEMATICAL MODELLING FOR TDS CORRECTION 228 6.4.1 ALLOWANCE FOR CRYSTAL MOSAICITY IN THE MODEL 235 6.4.2 ALLOWANCE FOR TDS IN THE MODEL 238 6.4.3 MATHEMATICAL REDUCTION METHOD 241 7 DEFECTS IN CRYSTAL AND THEIR INFLUENCE ON X-RAY STRUCTURE ANALYSIS 250 7.1 DEFECTS IN CRYSTALS 251 CONTENTS XI 7.1.1 X-RAY DIFFRACTION FROM CRYSTALS WITH DEFECTS 252 7.2 PREPARATION OF A SINGLE-CRYSTAL SAMPLE FOR DIFFRACTION DATA COLLECTION . 257 7.2.1 CRYSTAL LATTICE DEFECTS GENERATED BY SAMPLE PREPARATION AND THEIR INFLUENCE UPON X-RAY DIFFRACTION 260 7.3 EXTINCTION EFFECTS AND THE EXTINCTION CORRECTION PROBLEM 266 7.4 SAMPLES FOR X-RAY POWDER DIFFRACTION 272 8 AUXILIARY METHODS 273 8.1 LOW-TEMPERATURE DEVICES 273 8.2 HIGH-TEMPERATURE DEVICES 279 8.3 HIGH-PRESSURE DEVICES 282 8.4 LASER ACTION ON THE CRYSTAL 290 REFERENCES 295 SUBJECT INDEX 305
any_adam_object	1
author	Aslanov, L. A. Fetisov, G. V. Howard, J. A. K.
author_facet	Aslanov, L. A. Fetisov, G. V. Howard, J. A. K.
author_role	aut aut aut
author_sort	Aslanov, L. A.
author_variant	l a a la laa g v f gv gvf j a k h jak jakh
building	Verbundindex
bvnumber	BV012080398
classification_rvk	UQ 5100 UQ 5600
classification_tum	CHE 312f GEO 425f CHE 220f
ctrlnum	(OCoLC)845029399 (DE-599)BVBBV012080398
dewey-full	548.83
dewey-hundreds	500 - Natural sciences and mathematics
dewey-ones	548 - Crystallography
dewey-raw	548.83
dewey-search	548.83
dewey-sort	3548.83
dewey-tens	540 - Chemistry and allied sciences
discipline	Chemie / Pharmazie Geowissenschaften Physik Chemie
format	Book
fullrecord	<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>02041nam a2200481 cb4500</leader><controlfield tag="001">BV012080398</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">19991122 </controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">980730s1998 ad\|\| \|\|\|\| 00\|\|\| eng d</controlfield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">0198559275</subfield><subfield code="9">0-19-855927-5</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)845029399</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV012080398</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-703</subfield><subfield code="a">DE-20</subfield><subfield code="a">DE-91G</subfield><subfield code="a">DE-29T</subfield><subfield code="a">DE-188</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">548.83</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">UQ 5100</subfield><subfield code="0">(DE-625)146522:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">UQ 5600</subfield><subfield code="0">(DE-625)146528:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">CHE 312f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">GEO 425f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">CHE 220f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Aslanov, L. A.</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Crystallographic instrumentation</subfield><subfield code="c">L. A. Aslanov and G. V. Fetisov and J. A. K. Howard</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Oxford [u.a.]</subfield><subfield code="b">Oxford Univ. Press</subfield><subfield code="c">1998</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XI, 309 S.</subfield><subfield code="b">Ill., graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="490" ind1="1" ind2=" "><subfield code="a">International Union of Crystallography: International Union of Crystallography monographs on crystallography</subfield><subfield code="v">7</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kristallstruktur</subfield><subfield code="0">(DE-588)4136176-3</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Röntgendiffraktometrie</subfield><subfield code="0">(DE-588)4336833-5</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Röntgenstreuung</subfield><subfield code="0">(DE-588)4178324-4</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Kristallstruktur</subfield><subfield code="0">(DE-588)4136176-3</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Röntgenstreuung</subfield><subfield code="0">(DE-588)4178324-4</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Röntgendiffraktometrie</subfield><subfield code="0">(DE-588)4336833-5</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Fetisov, G. V.</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Howard, J. A. K.</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="830" ind1=" " ind2="0"><subfield code="a">International Union of Crystallography: International Union of Crystallography monographs on crystallography</subfield><subfield code="v">7</subfield><subfield code="w">(DE-604)BV005455767</subfield><subfield code="9">7</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">GBV Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008179014&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="999" ind1=" " ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-008179014</subfield></datafield></record></collection>
id	DE-604.BV012080398
illustrated	Illustrated
indexdate	2024-07-09T18:21:20Z
institution	BVB
isbn	0198559275
language	English
oai_aleph_id	oai:aleph.bib-bvb.de:BVB01-008179014
oclc_num	845029399
open_access_boolean
owner	DE-703 DE-20 DE-91G DE-BY-TUM DE-29T DE-188
owner_facet	DE-703 DE-20 DE-91G DE-BY-TUM DE-29T DE-188
physical	XI, 309 S. Ill., graph. Darst.
publishDate	1998
publishDateSearch	1998
publishDateSort	1998
publisher	Oxford Univ. Press
record_format	marc
series	International Union of Crystallography: International Union of Crystallography monographs on crystallography
series2	International Union of Crystallography: International Union of Crystallography monographs on crystallography
spelling	Aslanov, L. A. Verfasser aut Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard Oxford [u.a.] Oxford Univ. Press 1998 XI, 309 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier International Union of Crystallography: International Union of Crystallography monographs on crystallography 7 Kristallstruktur (DE-588)4136176-3 gnd rswk-swf Röntgendiffraktometrie (DE-588)4336833-5 gnd rswk-swf Röntgenstreuung (DE-588)4178324-4 gnd rswk-swf Kristallstruktur (DE-588)4136176-3 s Röntgenstreuung (DE-588)4178324-4 s DE-604 Röntgendiffraktometrie (DE-588)4336833-5 s Fetisov, G. V. Verfasser aut Howard, J. A. K. Verfasser aut International Union of Crystallography: International Union of Crystallography monographs on crystallography 7 (DE-604)BV005455767 7 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008179014&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Aslanov, L. A. Fetisov, G. V. Howard, J. A. K. Crystallographic instrumentation International Union of Crystallography: International Union of Crystallography monographs on crystallography Kristallstruktur (DE-588)4136176-3 gnd Röntgendiffraktometrie (DE-588)4336833-5 gnd Röntgenstreuung (DE-588)4178324-4 gnd
subject_GND	(DE-588)4136176-3 (DE-588)4336833-5 (DE-588)4178324-4
title	Crystallographic instrumentation
title_auth	Crystallographic instrumentation
title_exact_search	Crystallographic instrumentation
title_full	Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard
title_fullStr	Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard
title_full_unstemmed	Crystallographic instrumentation L. A. Aslanov and G. V. Fetisov and J. A. K. Howard
title_short	Crystallographic instrumentation
title_sort	crystallographic instrumentation
topic	Kristallstruktur (DE-588)4136176-3 gnd Röntgendiffraktometrie (DE-588)4336833-5 gnd Röntgenstreuung (DE-588)4178324-4 gnd
topic_facet	Kristallstruktur Röntgendiffraktometrie Röntgenstreuung
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008179014&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
volume_link	(DE-604)BV005455767
work_keys_str_mv	AT aslanovla crystallographicinstrumentation AT fetisovgv crystallographicinstrumentation AT howardjak crystallographicinstrumentation

Verfügbarkeit

Es ist kein Print-Exemplar vorhanden.

Fernleihe Bestellen Achtung: Nicht im THWS-Bestand! Inhaltsverzeichnis

MARC

Datensatz im Suchindex

Es ist kein Print-Exemplar vorhanden.

Ähnliche Einträge