High performance capillary electrophoresis: theory, techniques and applications
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
Wiley
1998
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| Schriftenreihe: | Chemical analysis
146 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXXII, 1047 S. graph. Darst. |
| ISBN: | 0471148512 |
Internformat
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| adam_text | HIGH-PERFORMANCE CAPILLARY ELECTROPHORESIS THEORY, TECHNIQUES, AND
APPLICATIONS EDITED BY MORTEZA G. KHALEDI DEPARTMENT OF CHEMISTRY NORTH
CAROLINA STATE UNIVERSITY RALEIGH, NORTH CAROLINA A WILEY-INTERSCIENCE
PUBLICATION JOHN WILEY & SONS, INC. NEW YORK / CHICHESTER / WEINHEIM /
BRISBANE / SINGAPORE / TORONTO CONTENTS CONTRIBUTORS XIX PREFACE XXIII
CUMULATIVE LISTING OF VOLUMES IN SERIES XXVII PART I THEORY AND MODES OF
HPCE CHAPTER 1 CAPILLARY ELECTROPHORESIS: OVERVIEW AND PERSPECTIVE 3
BARRY L. KARGER 1.1. INTRODUCTION 3 1.2. MODES OF OPERATION 5 1.3.
CAPILLARY ELECTROPHORESIS-MASS SPECTROMETRY 16 1.4. ELECTRIC FIELD
MANIPULATION OF BULK LIQUID FLOW 18 1.5. CONCLUSIONS 22 LIST OF ACRONYMS
AND ABBREVIATIONS 22 REFERENCES 23 CHAPTER 2 THEORY OF CAPILLARY ZONE
ELECTROPHORESIS 25 ERNST KENNDLER 2.1. CAPILLARY ZONE ELECTROPHORESIS IN
THE ABSENCE OF ELECTROOSMOTIC FLOW 27 2.2. CAPILLARY ZONE
ELECTROPHORESIS IN THE PRESENCE OF ELECTROOSMOTIC FLOW 58 LIST OF
SYMBOLS 70 LIST OF ACRONYMS 73 REFERENCES 73 V VI CONTENTS CHAPTER 3
MICELLAR ELECTROKINETIC CHROMATOGRAPHY 77 MORTEZA G. KHALEDI 3.1.
INTRODUCTION 77 3.2. PSEUDOSTATIONARY PHASES 79 3.3. MIGRATION IN
MICELLAR ELECTROKINETIC CHROMATOGRAPHY 83 3.4. MIGRATION PARAMETERS 84
3.5. RESOLUTION 85 3.6. STRUCTURE-RETENTION RELATIONSHIPS IN MICELLAR
ELECTROKINETIC CHROMATOGRAPHY 87 3.7. CHARACTERIZATION OF THE CHEMICAL
SELECTIVITY OF PSEUDOSTATIONARY PHASES 89 3.8. EFFECTS OF CHEMICAL
COMPOSITION OF MICELLAR SOLUTIONS 95 3.9. MULTIPARAMETER OPTIMIZATION
117 3.10. CONCLUSIONS AND FUTURE TRENDS 127 LIST OF ACRONYMS 130
REFERENCES 131 CHAPTER 4 BAND BROADENING IN MICELLAR ELECTROKINETIC
CHROMATOGRAPHY 141 JOE M. DAVIS 4.1. INTRODUCTION 142 4.2. MEASUREMENTS
OF EFFICIENCY 143 4.3. PLUG SIZE 143 4.4. THE DETECTION WINDOW AND TIME
CONSTANTS 144 4.5. MICELLAR OVERLOAD 145 4.6. LONGITUDINAL DIFFUSION 146
4.7. NONEQUILIBRIUM DISPERSION IN MICELLAR SYSTEMS 148 4.8.
ELECTROMIGRATIVE DISPERSION 158 4.9. DEPENDENCE OF N ON CONCENTRATION OF
ORGANIZED MEDIA 158 4.10. DEPENDENCE OF N ON ELECTROLYTE CONCENTRATION
AND COMPOSITION 164 4.11. DEPENDENCE OF N ON ORGANIC SOLVENTS 165
CONTENTS VLL 4.12. EFFICIENCY OF PSEUDOSTATIONARY PHASES OTHER THAN
SIMPLE MICELLES 4.13. GENERAL OBSERVATIONS 4.14. CONCLUSIONS ADDENDUM
LIST OF ACRONYMS AND ABBREVIATIONS REFERENCES 171 174 175 176 178 179
CHAPTER 5 CAPILLARY GEL ELECTROPHORESIS PAUL SHIEH, NELSON COOKE, AND
ANDRAS GUTTMAN 5.1. INTRODUCTION 5.2. THEORY AND OPERATION PARAMETERS
5.3. APPLICATIONS 5.4. CONCLUSION LIST OF ACRONYMS AND ABBREVIATIONS
REFERENCES 185 185 187 196 217 218 218 CHAPTER 6 CAPILLARY ISOELECTRIC
FOCUSING JOHN E. WIKTOROWICZ 6.1. INTRODUCTION 6.2. CAPILLARY
ISOELECTRIC FOCUSING 6.3. MODES OF ISOELECTRIC POINT DETERMINATION 6.4.
FUTURE CONSIDERATIONS AND DIRECTION ADDENDUM LIST OF ACRONYMS REFERENCES
223 223 226 241 245 247 247 248 CHAPTER 7 CAPILLARY ISOTACHOPHORESIS
LUDMILA KFIVAENKOVAE AND PETR BOCEK 7.1. INTRODUCTION 7.2. PRINCIPLES OF
ISOTACHOPHORESIS 7.3. ELECTROLYTE SYSTEMS 7.4. SAMPLE STACKING 7.5. THE
ISOTACHOPHORESIS-CAPILLARY ZONE ELECTROPHORESIS COMBINATION 7.6.
DYNAMICS OF DESTACKING 251 251 252 256 258 260 265 VLLL CONTENTS 7.7.
SAMPLE-INDUCED ISOTACHOPHORESIS (STACKING) 267 7.8. CONCLUSION 273 LIST
OF ACRONYMS AND ABBREVIATIONS 274 REFERENCES 275 CHAPTER 8 CAPILLARY
ELECTROCHROMATOGRAPHY 277 KATHLEEN A. KELLY AND MORTEZA G. KHALEDI 8.1.
INTRODUCTION 277 8.2. COLUMN PREPARATION 279 8.3. DETECTION 283 8.4.
THEORY 285 8.5. STATIONARY PHASE CONSIDERATIONS 287 8.6. MOBILE PHASE
CONSIDERATIONS 289 8.7. APPLICATIONS 290 8.8. CONCLUSIONS AND FUTURE
TRENDS 295 ADDENDUM 296 LIST OF ACRONYMS 297 REFERENCES 297 PART II
DETECTION SYSTEMS IN HPCE CHAPTER 9 CAPILLARY ELECTROPHORETIC DETECTORS
BASED ON LIGHT 303 LOUANN CRUZ, SCOTT A. SHIPPY, AND JONATHAN V.
SWEEDLER 9.1. INTRODUCTION 9.2. REQUIREMENTS OF CAPILLARY
ELECTROPHORETIC DETECTORS 9.3. ABSORBANCE 9.4. FLUORESCENCE 9.5. OTHER
CAPILLARY ELECTROPHORETIC OPTICAL DETECTORS 9.6. RECENT DEVELOPMENTS
9.7. CONCLUSIONS LIST OF ACRONYMS AND ABBREVIATIONS REFERENCES 304 305
308 321 331 341 347 347 348 CONTENTS IX CHAPTER 10 ELECTROCHEMICAL
DETECTION IN HIGH-PERFORMANCE CAPILLARY ELECTROPHORESIS BARBARA RHODEN
BRYANT, FRANKLIN D. SWANEK, AND ANDREW G. EWING 10.1. INTRODUCTION 10.2.
METHODS USED TO ELECTRICALLY ISOLATE THE ELECTROCHEMICAL DETECTOR 10.3.
MODES OF ELECTROCHEMICAL DETECTION 10.4. APPLICATIONS OF
HIGH-PERFORMANCE CAPILLARY ELECTROPHORESIS WITH ELECTROCHEMICAL
DETECTION 10.5. FUTURE DIRECTIONS LIST OF ACRONYMS REFERENCES 355 355
356 359 363 369 371 371 CHAPTER 11 INDIRECT DETECTION IN CAPILLARY
ELECTROPHORESIS 375 HANS POPPE AND XIAOMA XU 11.1. INTRODUCTION 375
11.2. MEASUREMENT CONSIDERATIONS 377 11.3. THE TRANSFER RATIO AND SYSTEM
ZONES 383 11.4. OVERLOAD: ELECTROMIGRATION DISPERSION 390 11.5. NOISE
INDUCED BY THE ELECTROPHORETIC PROCESS AND SYSTEM PEAKS 393 11.6. CHOICE
OF THE BACKGROUND ELECTROLYTE 395 11.7. INSTRUMENTAL IMPROVEMENTS 397
11.8. APPLICATIONS AND SOME SPECIAL ASPECTS 398 11.9. SUMMARY 400 LIST
OF ACRONYMS 401 REFERENCES 401 CHAPTER 12 HIGH-PERFORMANCE CAPILLARY
ELECTROPHORESIS-MASS SPECTROMETRY KENNETH B. TOMER, LEESA J. DETERDING,
AND CAROL E. PARKER 405 12.1. INTRODUCTION 406 X CONTENTS 12.2.
ADVANTAGES OF MASS SPECTROMETRIC DETECTION 407 12.3. INSTRUMENTATION 407
12.4. DISADVANTAGES OF MASS SPECTROMETRIC DETECTION 414 12.5. POTENTIAL
SOLUTIONS TO DISADVANTAGES OF MASS SPECTROMETRIC DETECTION 415 12.6.
APPLICATIONS 429 12.7. SUMMARY 435 ADDENDUM NO. 1 436 ADDENDUM NO. 2 438
LIST OF ACRONYMS 440 REFERENCES 441 PART III OPERATIONAL ASPECTS AND
SPECIAL TECHNIQUES IN HPCE CHAPTER 13 SAMPLE INTRODUCTION AND STACKING
449 RING-LING CHIEN 13.1. INTRODUCTION 449 13.2. SAMPLE INTRODUCTION IN
CAPILLARY ZONE ELECTROPHORESIS 451 13.3. ON-COLUMN SAMPLE STACKING 456
13.4. STACKING IN SAMPLE INTRODUCTION 464 13.5. APPLICATIONS OF SAMPLE
STACKING 471 13.6. CONCLUSIONS 477 ADDENDUM 477 LIST OF ACRONYMS AND
ABBREVIATIONS 478 REFERENCES 478 CHAPTER 14 COATED CAPILLARIES IN HIGH-
PERFORMANCE CAPILLARY ELECTRO- PHORESIS 481 GERHARD SCHOMBURG 14.1.
INTRODUCTION 481 14.2. THE STATUS OF CAPILLARY SURFACES IN CAPILLARY
ELECTROPHORESIS: INFLUENCE ON ELECTROOSMOTIC FLOW 483 CONTENTS XI 14.3.
INFLUENCE OF ELECTROOSMOTIC FLOW ON EFFICIENCY AND RESOLUTION OF
CAPILLARY ELECTROPHORETIC SEPARATIONS 484 14.4. ANALYTE-WALL INTERACTION
AND THE PERFORMANCE OF ANALYTICAL CAPILLARY ELECTROPHORETIC SEPARATIONS
486 14.5. SURFACE-MODIFICATION PROCEDURES BY COATING IN FUSED-SILICA
CAPILLARIES 488 14.6. METHODS AND APPLICATIONS OF DYNAMIC SURFACE
MODIFICATIONS 492 14.7. METHODS AND APPLICATIONS OF PERMANENT SURFACE
MODIFICATIONS 507 14.8. RECENT DEVELOPMENTS IN THE DYNAMIC AND PERMANENT
MODIFICATION OF CAPILLARY SURFACES 516 LIST OF ACRONYMS AND
ABBREVIATIONS 519 REFERENCES 520 CHAPTER 15 NONAQUEOUS CAPILLARY
ELECTROPHORESIS JOSEPH L. MILLER AND MORTEZA G. KHALEDI 15.1.
INTRODUCTION 15.2. INFLUENCE OF NONAQUEOUS SOLVENTS IN CAPILLARY
ELECTROPHORESIS 15.3. APPLICATIONS 15.4. CONCLUSIONS AND FUTURE TRENDS
LIST OF ACRONYMS AND ABBREVIATIONS REFERENCES 525 525 527 540 553 553
554 CHAPTER 16 METHOD VALIDATION IN CAPILLARY ELECTROPHORESIS 557 K. D.
ALTRIA 16.1. INTRODUCTION 557 16.2. SPECIFIC VALIDATION ASPECTS 559
16.3. CONCLUSIONS 577 LIST OF ACRONYMS 577 REFERENCES 578 XII CONTENTS
CHAPTER 17 TWO-DIMENSIONAL SEPARATIONS IN HIGH-PERFORMANCE CAPILLARY
ELECTROPHORESIS 581 THOMAS F. HOOKER, DOROTHEA J. JEFFREY, AND JAMES W.
JORGENSON 17.1. INTRODUCTION 582 17.2. TWO-DIMENSIONAL SEPARATION THEORY
583 17.3. COMPREHENSIVE TWO-DIMENSIONAL LIQUID CHROMATOGRAPHY-CAPILLARY
ELECTROPHORESIS 588 17.4. THREE-DIMENSIONAL SIZE EXCLUSION
CHROMATOGRAPHY-REVERSED-PHASE LIQUID CHROMATOGRAPHY-HIGH-SPEED CAPILLARY
ZONE ELECTROPHORESIS 605 17.5. FUTURE DIRECTIONS 607 LIST OF ACRONYMS
610 REFERENCES 610 CHAPTER 18 MICROFABRICATED CHEMICAL SEPARATION
DEVICES 613 STEPHEN C. JACOBSON AND J. MICHAEL RAMSEY 18.1. INTRODUCTION
18.2. MODULAR SYSTEM DESIGN 18.3. FABRICATION TECHNIQUES 18.4. FLUID
MANIPULATION AND INJECTION 18.5. MICROCHIP ELECTROPHORESIS 18.6. DNA
SEPARATIONS 18.7. CHROMATOGRAPHIE SEPARATIONS 18.8. INTEGRATED
STRUCTURES FOR CHEMICAL AND BIOCHEMICAL REACTIONS AND ANALYSIS 18.9. THE
FUTURE ADDENDUM LIST OF ACRONYMS REFERENCES 613 614 615 617 620 623 626
627 629 631 631 632 CONTENTS XLLL PART IV APPLICATIONS OF HPCE CHAPTER
19 PEPTIDE ANALYSIS BY CAPILLARY ELECTROPHORESIS: METHODS DEVELOPMENT
AND OPTIMIZATION, SENSITIVITY ENHANCEMENT STRATEGIES, AND APPLICATIONS
637 GREGORY M. MCLAUGHLIN, KENNETH W. ANDERSON, AND DIETRICH K. HAUFFE
19.1. INTRODUCTION 638 19.2. EFFECTS OF CAPILLARY DIMENSIONS, APPLIED
VOLTAGE, AND TEMPERATURE 639 19.3. EFFECTS OF PH AND IONIC STRENGTH 643
19.4. BUFFER ADDITIVES 647 19.5. USE OF ION-PAIRING REAGENTS 650 19.6.
USE OF MICELLAR ELECTROKINETIC CHROMATOGRAPHY FOR HYDROPHOBIE AND
NEUTRAL SPECIES 651 19.7. CHIRAL SELECTORS 653 19.8.
SENSITIVITY-ENHANCEMENT STRATEGIES 654 19.9. USE OF COATED CAPILLARIES
AND WALL COATINGS 656 19.10. METHODS DEVELOPMENT STRATEGY 657 19.11. USE
OF CAPILLARY ELECTROPHORESIS AND HIGH- PERFORMANCE LIQUID CHROMATOGRAPHY
AS COMPLEMENTARY TECHNIQUES 659 19.12. ENHANCED DETECTION METHODS 662
19.13. PHYSICOCHEMICAL MEASUREMENTS 663 19.14. CONCLUDING REMARKS AND
FUTURE TRENDS 666 ADDENDA 666 LIST OF ACRONYMS, ABBREVIATIONS, AND
SYMBOLS 670 REFERENCES 671 CHAPTER 20 CAPILLARY ELECTROPHORESIS OF
PROTEINS FRED E. REGNIER AND SHEN HIN 20.1. CONVENTIONAL ELECTROPHORESIS
OF PROTEINS 683 684 XIV CONTENTS 20.2. ELECTROPHORESIS OF PROTEINS IN
FUSED- SILICA CAPILLARIES 685 20.3. SURFACE MODIFIKATION OF CAPILLARIES
686 20.4. ZONE ELECTROPHORESIS IN OPEN-TUBULAR CAPILLARIES 703 20.5.
CAPILLARY ISOELECTRIC FOCUSING 712 20.6. CAPILLARY GEL ELECTROPHORESIS
713 20.7. MICELLAR ELECTROKINETIC CHROMATOGRAPHY 715 20.8. SELECTIVITY
715 20.9. MASS SPECTROMETRY 716 20.10. THE FUTURE 719 LIST OF ACRONYMS
AND ABBREVIATIONS 720 REFERENCES 722 CHAPTER 21 CAPILLARY
ELECTROPHORESIS OF CARBOHYDRATES MILOS V. NOVOTNY 21.1. INTRODUCTION
21.2. THE GOALS OF ANALYTICAL GLYCOBIOLOGY 21.3. INSTRUMENTAL ASPECTS
21.4. SAMPLE DERIVATIZATION 21.5. ELECTROMIGRATION MECHANISMS 21.6.
SELECTED APPLICATIONS LIST OF ACRONYMS AND ABBREVIATIONS REFERENCES 729
729 730 732 736 744 753 761 761 CHAPTER 22 DNA SEQUENCING BY MULTIPLEXED
CAPILLARY ELECTROPHORESIS EDWARD S. YEUNG AND QINGBO LI 22.1. HIGHLY
MULTIPLEXED DNA SEQUENCING 22.2. ACCELERATION OF ELECTROPHORETIC RUNS
22.3. BASE CALLING AND DATA HANDLING 22.4. SYSTEM INTEGRATION 22.5.
FUTURE PROSPECTS LIST OF ACRONYMS AND SYMBOLS REFERENCES 767 768 774 780
783 785 786 787 CONTENTS XV CHAPTER 23 CHIRAL SEPARATIONS BY CAPILLARY
ELECTROPHORESIS 791 FANG WANG AND MORTEZA G. KHALEDI 23.1. INTRODUCTION
791 23.2. CHIRAL RESOLUTION 793 23.3. TYPESOF CHIRAL SELECTOR 795 23.4.
EFFECT OF THE CHIRAL SELECTOR CONCENTRATION 806 23.5. PH AND IONIC
STRENGTH 807 23.6. ORGANIC SOLVENTS 808 23.7. THE COUNTER-ELECTROOSMOTIC
FLOW SCHEME 811 23.8. CAPILLARY ELECTROCHROMATOGRAPHY 812 23.9.
OTHERMETHODS 813 23.10. CHIRAL SEPARATION EFFICIENCY 814 23.11.
CONCLUSIONS AND FUTURE TRENDS 816 ADDENDUM 817 LIST OF ACRONYMS 818
REFERENCES 819 CHAPTER 24 CAPILLARY ELECTROPHORESIS OF INORGANIC IONS
825 JEFFREY R. MAZZEO 24.1. INTRODUCTION 825 24.2. INDIRECT-ULTRAVIOLET
DETECTION: GENERAL PRINCIPLES 826 24.3. DIRECT-ULTRAVIOLET DETECTION:
ANION DETERMINATIONS 841 24.4. DIRECT-ULTRAVIOLET DETECTION: CATION
DETERMINATIONS 843 24.5. OTHER DETECTION MODES 844 24.6. CONCLUDING
REMARKS 847 LIST OF ACRONYMS AND SYMBOLS 849 REFERENCES 849 CHAPTER 25
THE ANALYSIS OF PHARMACEUTICALS BY CAPILLARY ELECTROPHORESIS K. D.
ALTRIA 853 25.1. INTRODUCTION 853 XVI CONTENTS 25.2. APPLICATION AREAS
OF CAPILLARY ELECTROPHORESIS IN PHARMACEUTICAL ANALYSIS 854 25.3. FUTURE
DIRECTIONS 873 25.4. CONCLUSIONS 875 LIST OF ACRONYMS 875 REFERENCES 875
CHAPTER 26 ON-LINE IMMUNO AFFINITY CAPILLARY ELECTROPHORESIS FOR THE
DETERMINATION OF ANALYTES DERIVED FROM BIOLOGICAL FLUIDS 879 NORBERTO A.
GUZMAN, ANDY J. TOMLINSON, AND STEPHEN NAYLOR 26.1. INTRODUCTION 26.2.
NONSPECIFIC ON-LINE PRECONCENTRATION CAPILLARY ELECTROPHORESIS 26.3.
SPECIFIC ON-LINE PRECONCENTRATION CAPILLARY ELECTROPHORESIS 26.4.
CONCLUSIONS LIST OF ACRONYMS REFERENCES CHAPTER 27 MICROBIO ANAL YSIS
USING ON-LINE MICROREACTORS-CAPILLARY ELECTROPHORESIS SYSTEMS LARRY
LICKLIDER AND WERNER G. KUHR 27A. INTRODUCTION 27.2. SAMPLING SINGLE
BIOLOGICAL CELLS 27.3. ON-CAPILLARY ASSAYS 27.4. ON-LINE CAPILLARY
MICROREACTORS-CAPILLARY ELECTROPHORESIS SYSTEMS 27.5. CONCLUSIONS LIST
OF ACRONYMS AND SYMBOLS REFERENCES CHAPTER 28 ELECTROPHORETICALLY
MEDIATED MICROANALYSIS BRYAN J. HORMON AND FRED E. REGNIER 28.1.
COUPLING ON-LINE CHEMICAL REACTIONS TO CAPILLARY ELECTROPHORESIS 28.2.
DETERMINATIONS OF ENZYMES BY ELECTROPHORETICALLY MEDIATED MICROANALYSIS
879 881 883 894 894 895 899 899 900 904 909 919 920 920 925 926 928
CONTENTS XV11 28.3. ENZYMATIC DETERMINATIONS OF SUBSTRATES BY
ELECTROPHORETICALLY MEDIATED MICROANALYSIS 28.4. COMPLEXOMETRIC
DETERMINATIONS OF INORGANIC IONS BY ELECTROPHORETICALLY MEDIATED
MICROANALYSIS 28.5. DETERMINATIONS OF SINGLE CELLS BY
ELECTROPHORETICALLY MEDIATED MICROANALYSIS LIST OF ACRONYMS REFERENCES
PART V PHYSICOCHEMICAL STUDIES CHAPTER 29 AFFINITY CAPILLARY
ELECTROPHORESIS: USING CAPILLARY ELECTROPHORESIS TO STUDY THE
INTERACTIONS OF PROTEINS WITH LIGANDS JINMING GAO, MILAN MRKSICH, MATHAI
MAMMEN, AND GEORGE M. WHITESIDES 29 .1. BACKGROUND 29.2. PRINCIPLES OF
AFFINITY CAPIUARY ELECTROPHORESIS 29.3. TECHNICAL ISSUES 29.4. CARBONIC
ANHYDRASE AS A MODEL PROTEIN 29.5. DETERMINATION OF BINDING AFFINITY
29.6. DETERMINATION OF KINETIC PARAMETERS FOR BINDING 29.7. USING
AFFINITY CAPIUARY ELECTROPHORESIS TO MEASURE THE EFFECTIVE CHARGE OF A
PROTEIN 29.8. DETERMINATION OF STOICHIOMETRY OF BINDING 29.9. PROSPECTS
AND LIMITATIONS OF AFFINITY CAPIUARY ELECTROPHORESIS ADDENDUM LIST OF
ACRONYMS OR ABBREVIATIONS REFERENCES CHAPTER 30 DETERMINATION OF
PHYSICOCHEMICAL PARAMETERS BY CAPILLARY ELECTROPHORESIS PIER GIORGIO
RIGHETTI 30.1. INTRODUCTION 938 941 941 942 942 947 948 950 952 953 953
963 963 964 966 968 969 970 973 973 30.2. DETERMINATION OF PK VALUES OF
WEAK ELECTROLYTES 975 XV1U CONTENTS 30.3. DETERMINATION OF PK VALUES OF
AMPHOTERIC COMPOUNDS 980 30.4. ASSESSMENT OF PK VALUE S OF SILANOLS 981
30.5. DETERMINATION OF P/ VALUES OF PROTEINS 982 30.6. DETERMINATION OF
ABSOLUTE MOBILITY AND ITS RELATION TO THE CHARGE/MASS RATIO IN PEPTIDES
(AND PROTEINS) 984 30.7. DETERMINATION OF BINDING CONSTANTS 988 30.8.
DETERMINATION OF DIFFUSION CONSTANTS 991 30.9. VISCOSITY MEASUREMENTS
992 30.10. DETERMINATION OF T M VALUES OF NUCLEIC ACIDS 992 30.11.
CONCLUSIONS 995 LIST OF ACRONYMS AND SYMBOLS 995 REFERENCES 996 CHAPTER
31 APPLICATIONS OF MICELLAR ELECTROKINETIC CHROMATOGRAPHY IN
QUANTITATIVE STRUCTURE-ACTIVITY RELATIONSHIP STUDIES: ESTIMATION OF LOG
P* AND BIOACTIVITY 999 MORTEZA G. KHALEDI 31.1. INTRODUCTION 999 31.2.
SOLUTE-MICELLE INTERACTIONS AND HYDROPHOBICITY 1001 31.3. RELATIONSHIPS
BETWEEN MICELLAR ELECTRO- KINETIC CHROMATOGRAPHY RETENTION AND LOGP OW
1002 31.4. ROLE OF THE PSEUDOSTATIONARY PHASE 1005 31.5. PREDICTION OF
RETENTION IN MICELLAR ELECTROKINETIC CHROMATOGRAPHY FROM SOLUTE
HYDROPHOBICITY 1011 31.6. QUANTITATIVE RETENTION-ACTIVITY RELATIONSHIPS
IN MICELLAR ELECTROKINETIC CHROMATOGRAPHY 1011 31.7. CONCLUSIONS 1012
LIST OF ACRONYMS 1013 REFERENCES 1014 INDEX 1015
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| id | DE-604.BV012047429 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T18:20:44Z |
| institution | BVB |
| isbn | 0471148512 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-008154065 |
| oclc_num | 37370620 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-20 DE-83 |
| owner_facet | DE-355 DE-BY-UBR DE-20 DE-83 |
| physical | XXXII, 1047 S. graph. Darst. |
| publishDate | 1998 |
| publishDateSearch | 1998 |
| publishDateSort | 1998 |
| publisher | Wiley |
| record_format | marc |
| series | Chemical analysis |
| series2 | Chemical analysis |
| spelling | High performance capillary electrophoresis theory, techniques and applications ed. by Morteza G. Khaledi High-performance capillary electrophoresis New York [u.a.] Wiley 1998 XXXII, 1047 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 146 Biomolécules - Analyse ram Eletroforese capilar de zona larpcal Électrophorèse capillaire ram Électrophorèse ram Capillary electrophoresis Kapillarelektrophorese (DE-588)4290002-5 gnd rswk-swf Kapillarelektrophorese (DE-588)4290002-5 s DE-604 Khaledi, Morteza G. Sonstige oth Chemical analysis 146 (DE-604)BV000008780 146 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008154065&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | High performance capillary electrophoresis theory, techniques and applications Chemical analysis Biomolécules - Analyse ram Eletroforese capilar de zona larpcal Électrophorèse capillaire ram Électrophorèse ram Capillary electrophoresis Kapillarelektrophorese (DE-588)4290002-5 gnd |
| subject_GND | (DE-588)4290002-5 |
| title | High performance capillary electrophoresis theory, techniques and applications |
| title_alt | High-performance capillary electrophoresis |
| title_auth | High performance capillary electrophoresis theory, techniques and applications |
| title_exact_search | High performance capillary electrophoresis theory, techniques and applications |
| title_full | High performance capillary electrophoresis theory, techniques and applications ed. by Morteza G. Khaledi |
| title_fullStr | High performance capillary electrophoresis theory, techniques and applications ed. by Morteza G. Khaledi |
| title_full_unstemmed | High performance capillary electrophoresis theory, techniques and applications ed. by Morteza G. Khaledi |
| title_short | High performance capillary electrophoresis |
| title_sort | high performance capillary electrophoresis theory techniques and applications |
| title_sub | theory, techniques and applications |
| topic | Biomolécules - Analyse ram Eletroforese capilar de zona larpcal Électrophorèse capillaire ram Électrophorèse ram Capillary electrophoresis Kapillarelektrophorese (DE-588)4290002-5 gnd |
| topic_facet | Biomolécules - Analyse Eletroforese capilar de zona Électrophorèse capillaire Électrophorèse Capillary electrophoresis Kapillarelektrophorese |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008154065&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000008780 |
| work_keys_str_mv | AT khaledimortezag highperformancecapillaryelectrophoresistheorytechniquesandapplications AT khaledimortezag highperformancecapillaryelectrophoresis |