Modern techniques in applied molecular spectroscopy:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
Wiley
1998
|
| Schriftenreihe: | Techniques in analytical chemistry
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVI, 410 S. zahlr. Ill., graph. Darst. |
| ISBN: | 0471123595 |
Internformat
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| 245 | 1 | 0 | |a Modern techniques in applied molecular spectroscopy |c ed. by Francis M. Mirabella |
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Datensatz im Suchindex
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| adam_text | MODERN TECHNIQUES IN APPLIED MOLECULAR SPECTROSCOPY EDITED BY FRANCIS M.
MIRABELLA EQUISTAR CHEMICALS, LP A WILEY-INTERSCIENCE PUBLICATION JOHN
WILEY & SONS, INC. NEW YORK * CHICHESTER * WEINHEIM * BRISBANE *
SINGAPORE * TORONTO CONTENTS PREFACE XIII LIST OF CONTRIBUTORS XV 1
INTRODUCTION 1 FRANCIS M. MIRABELLA 1.1. TRANSMISSION SPECTROSCOPY 4
1.2. SPECULAR REFLECTANCE SPECTROSCOPY 5 1.3. ATTENUATED TOTAL
REFLECTANCE SPECTROSCOPY 5 1.4. DIFFUSE REFLECTANCE SPECTROSCOPY 6 1.5.
PHOTOACOUSTIC SPECTROSCOPY 7 1.6. INFRARED MICROSPECTROSCOPY 7 1.7.
RAMAN MICROSPECTROSCOPY 8 1.8. FIBER OPTICS TECHNIQUES 9 1.9. EMISSION
SPECTROSCOPY 9 REFERENCES 10 VI CONTENTS 2 TRANSMISSION INFRARED
SPECTROSCOPY 11 RICHARD W DUERST, MARILYN D. DUERST, AND WILLIAM L.
STEBBINGS 2.1. HISTORY 11 DISCOVERY OF INFRARED RADIATION 11 EVOLUTION
OF INSTRUMENTATION FOR TRANSMISSION INFRARED SPECTROSCOPY 13 NICHE
APPLICATIONS 14 2.2. PRINCIPLES AND THEORY 15 MOLECULAR INTERACTIONS
WITH ELECTROMAGNETIC RADIATION 15 MOLECULAR VIBRATION-ROTATION THEORY 19
2.3. INSTRUMENTATION 30 INFRARED SOURCES 30 OPTICAL COMPONENTS 34
DETECTORS 36 ELECTRONICS ^ 38 MOUNTS 38 NOISE SOURCES 38 FFT ALGORITHMS
FOR FT-IR SPECTROMETERS 39 ADVANTAGES AND DISADVANTAGES OF THE DIFFERENT
INSTRUMENT SYSTEMS 40 2.4. EXPERIMENTAL CONSIDERATIONS 41 INSTRUMENT
PERFORMANCE EVALUATION*HOW DO YOU KNOW IF THE INSTRUMENT IS FUNCTIONING
PROPERLY? 41 TYPES OF SAMPLES, SAMPLE PREPARATION METHODS 42 ACCESSORY
AND METHODOLOGY CHOICES 51 SETTING UP THE INSTRUMENT FOR SAMPLE SPECTRUM
COLLECTION 51 IDENTIFYING ACCEPTABLE SPECTRA WITHOUT ARTIFACTS 52 DATA
MANIPULATIONS 54 2.5. INTERPRETATION 56 QUALITATIVE ANALYSIS 56
QUANTITATIVE ANALYSIS 59 CALCULATED SPECTRA 63 2.6. EXPERIMENTAL RESULTS
AND CASE STUDIES 64 WATER IN THE GASEOUS STATE 64 QUANTITATIVE ANALYSIS
OF XYLENE MIXTURES 67 MOLECULAR ORIENTATION STUDIES 68 2.7. COURSES,
USERS GROUPS, AND MEETINGS 70 CONTENTS VLL REFERENCES 71 GLOSSARY 80 3
SPECULAR REFLECTION SPECTROSCOPY 83 ROBERT J. LIPPERT, BRIAN D. LAMP,
AND MARC D. PORTER 3.1. INTRODUCTION 83 3.2. THEORETICAL CONSIDERATIONS
84 PROPAGATION OF ELECTROMAGNETIC RADIATION THROUGH A NONCONDUCTING
HOMOGENEOUS MEDIUM 85 REFLECTION OF ELECTROMAGNETIC RADIATION AT A
BOUNDARY BETWEEN HOMOGENEOUS MEDIA OF DIFFERENT OPTICAL PROPERTIES 89
BAND DISTORTIONS 95 ORIENTATION ANALYSIS 102 3.3. EXPERIMENTAL
CONSIDERATIONS 104 3.4. APPLICATIONS 110 ORGANIZED THIN FILMS 110 REDOX
TRANSFORMATIONS AT ELECTROCHEMICAL INTERFACES 114 ALUMINUM NITRIDE
THIN-FILM CHARACTERIZATION 122 3.5. CONCLUSIONS AND PROSPECTUS 124
REFERENCES 124 4 ATTENUATED TOTAL REFLECTION SPECTROSCOPY 127 FRANCIS M.
MIRABELLA 4.1. INTRODUCTION 127 4.2. HISTORY 128 4.3. PRINCIPLES AND
THEORY 132 4.4. PRACTICAL CONSIDERATIONS 142 4.5. ADVANTAGES AND
DISADVANTAGES 153 ADVANTAGES 153 DISADVANTAGES 156 4.6. SPECTRAL REGIONS
AND SPECTRAL TECHNIQUES EMPLOYING ATR 159 4.7. APPLICATIONS OF ATR
SPECTROSCOPY 160 SURFACE CHEMISTRY 160 SURFACE ORIENTATION 175 SPECIFIC
EXPERIMENTAL DETAILS 178 4.8. CONCLUSION 183 REFERENCES 183 VLLL
CONTENTS 5 DIFFUSE REFLECTANCE SPECTROSCOPY 185 JONATHAN P. BLITZ 5.1.
INTRODUCTION 185 5.2. ROLE OF DIFFUSE REFLECTANCE IN MOLECULAR
SPECTROSCOPY 187 5.3. DIFFUSE REFLECTANCE THEORY AND PRACTICE 189
FRESNEL AND KUBELKA-MUNK REFLECTANCE 189 KUBELKA-MUNK THEORY 192 THE
PRACTICE OF DIFFUSE REFLECTANCE SPECTROSCOPY 198 5.4. APPLICATIONS OF
DIFFUSE REFLECTANCE SPECTROSCOPY 208 DIFFUSE REFLECTANCE UV-VISIBLE
SPECTROSCOPY 208 DIFFUSE REFLECTANCE NEAR-INFRARED SPECTROSCOPY 209
DIFFUSE REFLECTANCE MID-INFRARED SPECTROSCOPY 212 5.5. CONCLUSIONS 216
REFERENCES 217 6 PHOTOACOUSTIC SPECTROSCOPY 221 J. F. MCCLELLAND, S. J.
BAJIC, R. W. JONES, AND L. M. SEAVERSON 6.1. INTRODUCTION 221 HISTORY
AND BASIC IDEA OF PAS 222 CONTROLLABLE SAMPLING DEPTH 223 PRACTICAL USES
OF CONTROLLABLE SAMPLING DEPTH 224 6.2. SIGNAL GENERATION THEORY AND
DATA ANALYSIS TREATMENTS 225 MAGNITUDE OF THE PHOTOACOUSTIC SIGNAL 226
PHASE OF.THE PHOTOACOUSTIC SIGNAL 227 PHOTOACOUSTIC SIGNAL SATURATION
228 SAMPLING DEPTH 230 INTERPRETATION OF PHOTOACOUSTIC SIGNAL PHASE DATA
232 6.3. INSTRUMENTATION 236 PHOTOACOUSTIC DETECTOR 236 FTIR
SPECTROMETER 242 PHASE MODULATION 245 6.4. APPLICATIONS 248 RAPID
IDENTIFICATION OF POLYMERS FOR RECYCLING 248 QUANTITATIVE ANALYSIS OF
MAJOR AND MINOR CONCENTRATIONS OF ADDITIVES IN PAPER PRODUCTS 249
ANALYSIS OF AQUEOUS SLUDGES WITH SOLUBLE AND INSOLUBLE SPECIES 251
QUANTITATION OF CAC0 3 RESIDUAL IN LIME 255 CONTENTS IX DETERMINING
SURFACE OR BULK CHARACTER OF POLYMER ADDITIVES 257 FLUORINATION OF
POLYETHYLENE 259 CHEMICALLY TREATED POLYSTYRENE SPHERES 260 ENHANCED
SURFACE SPECIFICITY BY LINEARIZATION OF FTIR-PAS SPECTRA 261
DETERMINATION OF COATING THICKNESS FROM PHASE DATA 262 6.5. CONCLUSION
264 REFERENCES 265 7 INFRARED MICROSPECTROSCOPY 267 JACK E. KATON 7.1.
HISTORICAL BACKGROUND 267 7.2. INFRARED MICROSCOPE 270 7.3. SAMPLING 273
7.4. METHODS OF OBTAINING IR SPECTRAL DATA 282 7.5. QUALITATIVE AND
QUANTITATIVE ANALYSIS OF MIXTURES 283 REFERENCES 289 8 RAMAN
MICROSPECTROSCOPY 291 ANDRE J. SOMMER 8.1. INTRODUCTION 291 8.2. RAMAN
EFFECT 292 8.3. SIGNAL PRODUCTION AND COLLECTION 294 8.4.
INSTRUMENTATION 295 8.5. DETECTION AND SPECTRAL COLLECTION MODE 305 8.6.
EXCITATION AND COLLECTION OF THE RAMAN SCATTERED RADIATION 305 8.7.
CHOICE OF MICROSCOPE OBJECTIVE 308 8.8. SAMPLING 310 8.9. SAMPLING
PROBLEMS 312 8.10. SPATIAL RESOLUTION 312 8.11. SAMPLE HEATING 316 8.12.
FLUORESCENCE ELIMINATION 318 8.13. POLARIZATION EFFECTS 319 REFERENCES
321 9 EMISSION SPECTROSCOPY 323 S. ZHANG, F. S. FRANKE, AND T. M.
NIEMCZYK 9.1. INTRODUCTION 323 X CONTENTS 9.2. THEORY 325 BLACKBODY
RADIATION 325 REAL-SAMPLE (GRAYBODY) RADIATION 329 INFRARED EMISSION
SPECTROSCOPY OF SEMITRANSPARENT THIN FILMS 330 STRAY LIGHT 333 EMISSION
BAND DISTORTIONS 334 TEMPERATURE DETERMINATION 336 9.3. EXPERIMENTAL
CONSIDERATIONS 338 SPECTROMETERS 338 CONSTANT TEMPERATURE IR EMISSION
ATTACHMENTS 339 TRANSIENT INFRARED EMISSION SPECTROSCOPY 341
MULTIVARIATE CALIBRATION 342 9.4. APPLICATIONS 343 GAS PHASE STUDIES 343
SMALL MOLECULES ON SURFACES 345 CHARACTERIZATION OF SOLID SAMPLES 345
ATMOSPHERIC STUDIES 348 PLANETARY OBSERVATIONS 348 MINERALS AND MINERAL
DEPOSITS 349 ORGANIC THIN FILMS 351 DIELECTRIC THIN FILMS 357 9.5.
CONCLUSION 371 REFERENCES 372 10 FIBER OPTICS IN MOLECULAR SPECTROSCOPY
377 CHRIS W. BROWN 10.1. INTRODUCTION 377 DESCRIPTION OF OPTICAL FIBERS
377 INTERNAL REFLECTION CONSIDERATIONS 378 CORE-CLADDING 379 EVANESCENT
WAVE 379 FIBER THROUGHPUT 380 10.2. SELECTING FIBERS 380 OPTICAL REGIONS
380 SINGLE FIBERS OR BUNDLES AS PROBES 384 10.3. INTERFACING FIBERS 386
SPECTROMETER ACCESSORIES 386 CONTENTS XI COUPLING FIBERS TO SPECTROMETER
ACCESSORIES 387 10.4. SAMPLING CONFIGURATION 387 STRAIGHT-THROUGH
TRANSMISSION PROBES 387 REFLECTION-ABSORPTION PROBES 388 EVANESCENT WAVE
PROBES 388 FIBER OPTIC LENSES 389 10.5. APPLICATIONS 390 DRUG
DISSOLUTION 390 WATER ANALYSIS IN THE NEAR-IR 393 GAS ANALYSIS IN THE
NEAR-IR 396 LAMINATION MONITORING IN THE MID-IR 397 10.6. CONCLUSION 400
REFERENCES 400 INDEX 403 T
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| language | English |
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| spelling | Modern techniques in applied molecular spectroscopy ed. by Francis M. Mirabella New York [u.a.] Wiley 1998 XVI, 410 S. zahlr. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Techniques in analytical chemistry Spectroscopie moléculaire ram Molecular spectroscopy Molekülspektroskopie (DE-588)4128850-6 gnd rswk-swf Molekülspektroskopie (DE-588)4128850-6 s DE-604 Mirabella, Francis M. Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=008152306&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Modern techniques in applied molecular spectroscopy Spectroscopie moléculaire ram Molecular spectroscopy Molekülspektroskopie (DE-588)4128850-6 gnd |
| subject_GND | (DE-588)4128850-6 |
| title | Modern techniques in applied molecular spectroscopy |
| title_auth | Modern techniques in applied molecular spectroscopy |
| title_exact_search | Modern techniques in applied molecular spectroscopy |
| title_full | Modern techniques in applied molecular spectroscopy ed. by Francis M. Mirabella |
| title_fullStr | Modern techniques in applied molecular spectroscopy ed. by Francis M. Mirabella |
| title_full_unstemmed | Modern techniques in applied molecular spectroscopy ed. by Francis M. Mirabella |
| title_short | Modern techniques in applied molecular spectroscopy |
| title_sort | modern techniques in applied molecular spectroscopy |
| topic | Spectroscopie moléculaire ram Molecular spectroscopy Molekülspektroskopie (DE-588)4128850-6 gnd |
| topic_facet | Spectroscopie moléculaire Molecular spectroscopy Molekülspektroskopie |
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