Macrocyclic compounds in analytical chemistry:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | Undetermined |
| Veröffentlicht: |
New York [u.a.]
Wiley
1997
|
| Schriftenreihe: | Chemical analysis
143 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XXIV, 424 S. graph. Darst. |
| ISBN: | 0471172626 |
Internformat
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Datensatz im Suchindex
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| adam_text | MACROCYCLIC COMPOUNDS IN ANALYTICAL CHEMISTRY EDITED BY YU. A. ZOLOTOV
N. S. KUMAKOV INSTITUTE OF GENERAL AND INORGANIC CHEMISTRY MOSCOW,
RUSSIA A WILEY-INTERSCIENCE PUBLICATION JOHN WILEY & SONS, INC. NEW YORK
/ CHICHESTER / WEINHEIM / BRISBANE / SINGAPORE / TORONTO CONTENTS
CONTRIBUTORS XI PREFACE TO THE ENGLISH EDITION XIII PREFACE TO THE
RUSSIAN EDITION XV NOMENCLATURE OF MACROCYCLIC COMPOUNDS XVII
INTRODUCTION 1 YU. A. ZOLOTOV CHAPTER 1 SYNTHESIS OF MACROCYCLIC
COMPOUNDS 5 A. A. FORMANOVSKII AND I. V. MIKHURA 1.1. GENERAL PRINCIPLES
5 1.1.1. GENERAL APPROACHES AND METHODS 5 1.1,2JHE METHOD OF HIGH
DILUTION 7 1.1.3. THE METHOD OF TEMPLATE REACTIONS 7 1.1.4. THE METHOD
OF CONFORMATIONAL CONTROL 8 1.2. OXYGEN MACROCYCLES 8 1.2.1.
POLYOXACYCLOALKANES (CROWN ETHERS) 8 1.2.2. BENZOCROWN ETHERS 10 1.2.3.
CROWN ETHERS WITH PENDENT GROUPS 11 1.3. AZACROWNS 14 1.3.1. MACROCYCLIC
POLYAMINES 14 1.3.2. OXAZACROWN COMPOUNDS 16 1.3.2.1. ALIPHATIC
OXAZACROWN COMPOUNDS 16 1.3.2.2. BENZOOXAZACROWN COMPOUNDS 16 1.3.2.3.
OXAZACROWN COMPOUNDS WITH PYRIDINE UNITS 18 1.3.2.4. CRYPTANDS AND
RELATED COMPOUNDS 19 1.3.3. MACROCYCLIC SCHIFF BASES 21 1.3.3.1.
NITROGEN-CONTAINING SCHIFF BASES 21 V VI CONTENTS 1.3.3.2. SCHIFF BASES
CONTAINING NITROGEN AND OXYGEN 26 1.3.3.3. SCHIFF BASES WITH A PYRIDINE
UNIT 27 1.4. THIACROWNS 27 1.4.1. MACROCYCLIC POLYTHIA-ETHERS 28 1.4.2.
OXATHIACROWNS 29 1.4.3. THIAZACROWNS 30 1.4.4. OXATHIAZACROWNS 32
REFERENCES 34 CHAPTER 2 COMPLEXATION AND SELECTIVITY 41 /. V. PLETNEV
2.1. COMPLEXATION EFFICIENCY: THE MACROCYCLIC EFFECT AND PREORGANIZATION
41 2.2. COMPLEXATION SELECTIVITY: THE CAVITY DIAMETER-CATION SIZE
RELATIONSHIP 51 REFERENCES 58 CHAPTER 3 SOLVENT EXTRACTION OF METALS
WITH MACROCYCLIC REAGENTS AND ITS ANALYTICAL APPLICATIONS 63 M. K.
BEKLEMISHEV, S. G. DMITRIENKO, AND N. V. ISAKOVA 3.1. INTERPHASE
PARTITION OF MACROCYCLIC COMPOUNDS 64 3.2. EXTRACTION EQUILIBRIA 67
3.2.1. EXTRACTION OF THE COMPLEX 68 3.2.2. DISSOCIATION OF THE COMPLEX
INTO IONS IN THE ORGANIC PHASE 69 3.2.3. COMPLEX FORMATION IN THE
AQUEOUS PHASE 73 3.2.4. PARTITION OF MACROCYCLES BETWEEN PHASES 77
3.2.5. PROTONATION OF MACROCYCLES IN THE AQUEOUS PHASE 77 3.2.6.
EXTRACTION OF ACIDS 79 3.2.7. EXTRACTION OF ACIDS IN THE ABSENCE OF A
MACROCYCLE 82 3.2.8. ASSOCIATION OF MACROCYCLES IN THE ORGANIC PHASE 82
3.2.9. RARE AND LESS IMPORTANT EQUILIBRIA 83 CONTENTS VLL 3.2.10.
EXTRACTION OF COMPLEXES OF UNUSUAL COMPOSITION 83 3.3. CROWN ETHERS AS
EXTRACTANTS 88 3.3.1. GENERAL REMARKS 88 3.3.2. EXTRACTION OF ALKALI AND
ALKALINE-EARTH METALS WITH CROWN ETHERS 89 3.3.2.1. METAL RECOVERY AND
STABILITY OF THE COMPLEXES 89 3.3.2.2. EFFECT OFTHE CROWN ETHER
STRUCTURE 92 3.3.2.3. THE COUNTERION TYPE 103 3.3.2.4. EFFECT OFTHE
SOLVENT 109 3.3.2.5. THE SYNERGISTIC EFFECT 114 3.3.3. LANTHANIDE AND
ACTINIDES 117 3.3.4. TRANSITION METALS AND THE ELEMENTS OF THE HIA-VIA
GROUPS 124 3.3.5. EXTRACTION OF ANIONIC COMPLEXES 126 3.4. EXTRACTION
WITH MACROCYCLES CONTAINING NITROGEN, SULFUR, AND OTHER HETEROATOMS 129
3.4.1. MACROCYCLES CONTAINING NITROGEN AND OXYGEN 130 3.4.2. CRYPTANDS
139 3.4.3. NITROGEN-CONTAINING MACROCYCLES 141 3.4.4. PORPHYRINS AND
PHTHALOCYANINES 149 3.4.5. SULFUR-, SELENIUM-, AND PHOSPHORUS-
CONTAINING MACROCYCLES 151 3.4.6. MACROCYCLES CONTAINING NITROGEN,
SULFUR, AND OXYGEN IN VARIOUS COMBINATIONS 158 3.5. APPLICATIONS OF
METAL EXTRACTION WITH MACROCYCLES IN ANALYTICAL CHEMISTRY 162 3.5.1.
CROWN ETHERS 163 3.5.1.1. PRECONCENTRATION AND SEPARATION 163 3.5.1.2.
PHOTOMETRY 166 3.5.1.3. FLUOROMETRY 172 3.5.1.4. ATOMIC ABSORPTION
SPECTROMETRY 172 3.5.2. MACROCYCLES CONTAINING NITROGEN, SULFUR, AND
OTHER HETEROATOMS 173 3.5.2.1. PHOTOMETRY 173 3.5.2.2. FLUOROMETRY 176
VLLL CONTENTS 3.5.2.3. ATOMIC ABSORPTION SPECTROMETRY 178 3.5.2.4. OTHER
METHODS OF DETERMINATION 179 3.6. ION TRANSPORT ACROSS LIQUID MEMBRANES
180 3.7. EXTRACTION WITH MACROCYCLES ATTACHED TO POLYMERS 186 REFERENCES
188 CHAPTER 4 SORPTION AND CHROMATOGRAPHY 209 N. A. PASEKOVA AND E. I.
MOROSANOVA 4.1. GENERAL COMMENTS 209 4.2. METHODS OF SORBENT PREPARATION
210 4.3. SORPTION UNDER BATCH CONDITIONS 214 4.4. SORPTION UNDER DYNAMIC
CONDITIONS 234 4.5. APPLICATION OF MACROCYCLIC SORBENTS IN
CHROMATOGRAPHY 240 4.5.1. LIQUID CHROMATOGRAPHY 241 4.5.1.1. THIN-LAYER
CHROMATOGRAPHY 241 4.5.1.2. EXTRACTION CHROMATOGRAPHY 248 4.5.1.3.
LIQUID CHROMATOGRAPHY ON COLUMNS 252 4.5.2. GAS CHROMATOGRAPHY 271
REFERENCES 274 CHAPTER 5 ION-SELECTIVE ELECTRODES 285 L. K. SHPIGUN AND
R. D. TSINGARELLI 5.1. HISTORICAL BACKGROUND 285 5.2. GENERAL PRINCIPLES
299 5.2.1. ELECTRODE CONSTRUCTION AND MEMBRANE COMPOSITION 299 5.2.2.
THE ELECTRODE RESPONSE MECHANISM AND THE ESSENCE OF CATIONIC SELECTIVITY
300 5.2.3. EFFECT OF MACROCYCLE STRUCTURE ON POTENTIOMETRIE SELECTIVITY
306 5.2.4. DEPENDENCE OF THE PROPERTIES OF AN ION- SELECTIVE ELECTRODE
ON THE COMPOSITION OF ITS MEMBRANE 313 5.3. PROPERTIES AND APPLICATIONS
OF MACROCYCLIC- COMPOUND-BASE^ ION-SELECTIVE ELECTRODES 318 CONTENTS IX
5.3.1. LITHIUM ISES 318 5.3.2. SODIUM ISES 321 5.3.3. POTASSIUM ISES 326
5.3.4. RUBIDIUM AND CESIUM ISES 329 5.3.5. ALKALINE-EARTH METAL ISES 330
5.3.6. TRANSITION AND HEAVY METAL ISES 333 5.4. APPLICATIONS IN
FLOW-INJECTION ANALYSIS 337 REFERENCES 348 CHAPTER 6 SEPARATION AND
DETERMINATION OF ORGANIC COMPOUNDS 359 /. V. PLETNEV AND 1.1.
TOROCHESHNIKOVA 6.1. GENERAL COMMENTS 359 6.2. HOST-GUEST COMPLEXES:
GENERAL REVIEW 362 6.2.1. THE ALKYLAMMONIUM-CROWN ETHER COMPLEXES 362
6.2.2. COMPLEXES OF PROTONATED AMINES WITH OXAZA MACROCYCLES 368 6.2.3.
COMPLEXES OF CROWNS AND AZACROWNS WITH OTHER SUBSTRATES 371 6.3.
ION-SELECTIVE ELECTRODES 386 6.4. CHROMATOGRAPHY 390 REFERENCES 398
INDEX 405
|
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| isbn | 0471172626 |
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| physical | XXIV, 424 S. graph. Darst. |
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| series | Chemical analysis |
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| spelling | Macrocyclic compounds in analytical chemistry ed. by Yu. A. Zolotov New York [u.a.] Wiley 1997 XXIV, 424 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 143 A Wiley-Interscience publications Makrocyclische Verbindungen (DE-588)4168678-0 gnd rswk-swf Chemische Analyse (DE-588)4009840-0 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Kronenether (DE-588)4165804-8 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s Kronenether (DE-588)4165804-8 s DE-604 Makrocyclische Verbindungen (DE-588)4168678-0 s Chemische Analyse (DE-588)4009840-0 s Zolotov, Jurij A. 1932- Sonstige (DE-588)11947929X oth Chemical analysis 143 (DE-604)BV000008780 143 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007765880&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Macrocyclic compounds in analytical chemistry Chemical analysis Makrocyclische Verbindungen (DE-588)4168678-0 gnd Chemische Analyse (DE-588)4009840-0 gnd Analytische Chemie (DE-588)4129906-1 gnd Kronenether (DE-588)4165804-8 gnd |
| subject_GND | (DE-588)4168678-0 (DE-588)4009840-0 (DE-588)4129906-1 (DE-588)4165804-8 |
| title | Macrocyclic compounds in analytical chemistry |
| title_auth | Macrocyclic compounds in analytical chemistry |
| title_exact_search | Macrocyclic compounds in analytical chemistry |
| title_full | Macrocyclic compounds in analytical chemistry ed. by Yu. A. Zolotov |
| title_fullStr | Macrocyclic compounds in analytical chemistry ed. by Yu. A. Zolotov |
| title_full_unstemmed | Macrocyclic compounds in analytical chemistry ed. by Yu. A. Zolotov |
| title_short | Macrocyclic compounds in analytical chemistry |
| title_sort | macrocyclic compounds in analytical chemistry |
| topic | Makrocyclische Verbindungen (DE-588)4168678-0 gnd Chemische Analyse (DE-588)4009840-0 gnd Analytische Chemie (DE-588)4129906-1 gnd Kronenether (DE-588)4165804-8 gnd |
| topic_facet | Makrocyclische Verbindungen Chemische Analyse Analytische Chemie Kronenether |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007765880&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000008780 |
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