Food and environmental analysis in capillary gas chromatography: hints for practical use
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | German English |
| Veröffentlicht: |
Heidelberg
Hüthig
1997
|
| Schriftenreihe: | Chromatographic methods
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XII, 178 S. graph. Darst. |
| ISBN: | 3778524194 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV011376331 | ||
| 003 | DE-604 | ||
| 005 | 19970825 | ||
| 007 | t | ||
| 008 | 970603s1997 gw d||| |||| 00||| ger d | ||
| 016 | 7 | |a 950510718 |2 DE-101 | |
| 020 | |a 3778524194 |c Gb. : DM 98.00, S 715.00, sfr 89.00 |9 3-7785-2419-4 | ||
| 035 | |a (OCoLC)37854326 | ||
| 035 | |a (DE-599)BVBBV011376331 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 1 | |a ger |a eng |h ger | |
| 044 | |a gw |c DE | ||
| 049 | |a DE-703 | ||
| 050 | 0 | |a TX548.2.G36 | |
| 082 | 0 | |a 664/.07 |2 21 | |
| 084 | |a VG 7400 |0 (DE-625)147205:253 |2 rvk | ||
| 130 | 0 | |a Lebensmittel- und Umweltanalytik mit der Kapillar-GC | |
| 245 | 1 | 0 | |a Food and environmental analysis in capillary gas chromatography |b hints for practical use |c ed. by Lothar Matter |
| 264 | 1 | |a Heidelberg |b Hüthig |c 1997 | |
| 300 | |a XII, 178 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Chromatographic methods | |
| 650 | 7 | |a Cromatografia gasosa |2 larpcal | |
| 650 | 4 | |a Environmental monitoring | |
| 650 | 4 | |a Food |x Analysis | |
| 650 | 4 | |a Gas chromatography | |
| 650 | 0 | 7 | |a Glaskapillargaschromatographie |0 (DE-588)4157443-6 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Glaskapillargaschromatographie |0 (DE-588)4157443-6 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Matter, Lothar |e Sonstige |4 oth | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007645328&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-007645328 | |
Datensatz im Suchindex
| _version_ | 1807681892351213568 |
|---|---|
| adam_text |
CONTENTS
1
APPLICATION
OF
THE
RULES
OF
CHROMATOGRAPHY
TO
CAPILLARY
GAS
CHROMATOGRAPHY
LOTHAR
MATTER
.
1
1.1
INTRODUCTION
.
1
1.2
RULES
OF
CHROMATOGRAPHY
.
2
1.2.1
SAMPLE
INTRODUCTION
.
2
1.2.2
CHOICE
OF
THE
"
RIGHT
"
STATIONARY
PHASE
.
5
1.2.3
COLUMN
LENGTH
.
5
1.2.4
COLUMN
DIAMETER
.
5
1.2.5
FILM
THICKNESS
.
6
1.2.6
CARRIER
GAS
.
6
1.3
APPLICATIONS
.
7
1.3.1
DETERMINATION
OF
PENTACHLOROPHENOL
IN
WOOD
.
7
1.3.2
SUBJECTIVITY
OF
THE
SENSES
-
OBJECTIVITY
OF
CAPILLARY
GC
.
8
1.3.3
DETERMINATION
OF
BROMOCYCLENE
AND
MUSK
XYLENE
IN
FISH
.
10
1.3.4
SEPARATION
OF
33
ORGANOCHLOROPESTICIDES
.
11
1.3.5
SENSE
AND
NONSENSE
OF
ANALYZING
PAH-CONTAMINATED
SOILS
.
12
1.3.6
DETECTION
OF
IRRADIATED
FAT-CONTAINING
FOODS
.
16
1.3.7
DISTINCTION
BETWEEN
ANIMAL
SPECIES
IN
HEATED
PRODUCTS
.
18
1.3.7.1
DETECTION
OF
THE
ADDITION
OF
PORK
DRIPPING
TO
GOOSE
DRIPPING
.
18
1.3.7.2
DETECTION
OF
THE
ADDITION
OF
COW
'
S
MILK
TO
SHEEP
AND
.
19
GOAT
'
S
MILK
PRODUCTS
1.3.7.3
DISTINCTION
BETWEEN
BEEF
AND
PORK
PRODUCTS
.
21
1.3.7.4
DISTINCTION
BETWEEN
HUTCH
RABBIT
AND
WILD
HARE
.
22
1.3.7.5
DISTINCTION
BETWEEN
DOMESTICATED
PIG
AND
WILD
BOAR,
AND.
22
BETWEEN
VEAL
AND
BEEF
1.3.7.6
DISTINCTION
BETWEEN
GAME
SPECIES
.
24
1.3.8
DETERMINATION
OF
GERMINATION
INHIBITORS
(IPC/CIPC)
.
24
IN
POTATOES
1.3.9
INTERPRETATION
OF
CHROMATOGRAMS
-
AN
EXAMPLE
.
26
1.4
SUMMARY
.
27
1.5
REFERENCES
.
28
X
CONTENTS
2
GC/MS
DETERMINATION
OF
RESIDUES
AND
CONTAMINANTS
PETER
FURST
.
29
2.1
INTRODUCTION
.
29
2.2
RECORDING
MASS
SPECTRA
.
30
2.2.1
FULL
SCAN
.
.'
.
30
2.2.2
MASS
FRAGMENTOGRAPHY
.
32
2.3
APPLICATIONS
OF
GC/MS
TO
THE
ANALYSIS
OF
RESIDUES
.
33
AND
CONTAMINANTS
IN
FOODS.
2.3.1
IDENTIFICATION
OF
UNKNOWN
SUBSTANCES
AND
CONFIRMATION
.
33
OF
ANALYTICAL
DATA
BY
RECORDING
COMPLETE
MASS
SPECTRA
2.3.1.1
DETERMINATION
OF
TRIAZINE
HERBICIDES
IN
DRINKING
WATER
.
33
2.3.1.2
CONFIRMATION
OF
CHLORPYRIPHOS-ETHYL
IN
ORANGES
.
36
2.3.1.3
DETECTION
OF
DICHLORAN
IN
NUTRITION
.
37
2.3.1.4
IDENTIFICATION
OF
PROPENOPHOS
IN
TOMATOES
.
38
2.3.1.5
DETERMINATION
OF
HORMONE
DERIVATIVES
IN
VEAL
.
40
2.3.1.6
DETECTION
OF
NEUROLEPTICS
IN
PORK
.
41
2.3.2
DETECTION
AND
DETERMINATION
OF
RESIDUES
AND
CONTAMINANTS
.
43
WITH
THE
AID
OF
MASS
FRAGMENTOGRAPHY
2.3.2.1
DETERMINATION
OF
POLYCHLORINATED
DIBENZODIOXINS
.
44
AND
DIBENZOFURANS
2.3.2.2
DETERMINATION
OF
PCB
AND
PCB
SUBSTITUTES
.
52
2.3.2.3
DETERMINATION
OF
POLYBROMINATED
FLAME
RETARDANTS
.
55
2.3.2.4
DETERMINATION
OF
POLYCHLORINATED
TERPENES
.
57
2.3.2.5
DETERMINATION
OF
BENZO[A]PYRENE
IN
SMOKED
MEAT
.
60
AND
MEAT
PRODUCTS
2.3.2.6
DETERMINATION
OF
CHLORAMPHENICOL
IN
FOODS
OF
ANIMAL
.
63
ORIGIN
2.3.2.7
DETERMINATION
OF
B-SYMPATHOMIMETICS
IN
MEAT
AND
URINE
.
66
2.3.2.8
DETERMINATION
OF
DIETHYLSILBESTROL
IN
MEAT
BY
.
69
GC/LRMS
AND
GC/HRMS
2.4
SUMMARY
.
72
2.5
REFERENCES
.
72
3
DETERMINATION
OF
PAH
IN
FOODS
KARL
SPEER
.
75
3.1
INTRODUCTION
.
75
CONTENTS
XI
3.2
PAH
IN
OILS
AND
FATS
.
78
3.2.1
ANALYSIS
OF
FATS
AND
OILS
.
79
3.2.2
INJECTION
SYSTEMS
.
84
3.2.3
RESULTS
.
85
3.3
PAH
IN
VEGETABLES
.
89
3.3.1
ANALYSIS
.
89
3.3.2
RESULTS
.
93
3.4
PAH
IN
FISH
PRODUCTS
AND
MOLLUSKS
.
95
3.4.1
ANALYSIS
.
95
3.4.2
RESULTS
.
96
3.5
PAH
IN
COFFEE
.
98
3.5.1
ANALYSIS
.
100
3.5.2
RESULTS
.
100
3.6
PAH
IN
TEA
.
100
3.6.1
ANALYSIS
.
101
3.6.2
RESULTS
.
101
3.7
ANALYTICAL
PROCEDURES
FOR
DETERMINATION
OF
PAH
IN
FOODS
.
103
3.7.1
CHEMICALS
.
103
3.7.2
GLASS
APPARATUS
AND
AIDS
.
104
3.7.3
PROCEDURE
PL:
FISH
PRODUCTS
AND
MOLLUSKS
.
105
3.7.4
PROCEDURE
P2:
VEGETABLES
.
109
3.7.5
PROCEDURE
P3:
VEGETABLE
OILS
AND
FATS
.
ILL
3.7.6
PROCEDURE
P4:
COFFEE
.
113
3.8
REFERENCES
.
115
4
THE
MASS
SPECTROMETER
AS
DETECTOR
IN
CAPILLARY
GC
HANS-JOACHIM
HILBSCHMANN
.
119
4.1
CLASSICAL
DETECTORS
VERSUS
MASS
SPECTROMETRY
.
119
4.2
MASS
SPECTROMETRY
.
121
4.2.1
HIGH
RESOLUTION
MASS
SPECTROMETERS
.
121
4.2.2
LOW
RESOLUTION
MASS
SPECTROMETERS
.
123
4.3
IONIZATION
PROCESSES
.
124
4.3.1
ELECTRON
IMPACT
IONIZATION
.
124
XII
CONTENTS
4.3.2
CHEMICAL
IONIZATION
.
127
4.3.2.1
PRINCIPLE
OF
CHEMICAL
IONIZATION
.
129
4.3.2.2
REACTANT
GAS
SYSTEMS
.
134
4.3.3
ASPECTS
OF
SWITCHING
BETWEEN
EI
AND
CI
.
137
4.3.3.1
QUADRUPOLE
AND
SECTOR
FIELD
SPECTROMETERS
.
138
4.3.3.2
ION
TRAP
SPECTROMETERS
.
138
4.4
SPECIAL
ASPECTS
OF
GC/MS
COUPLING
.
139
4.4.1
CHOICE
OF
CARRIER
GAS
.
139
4.4.2
CHOICE
OF
CAPILLARY
COLUMN
.
140
4.4.3
GC/MS
COUPLING
TECHNIQUES
.
141
4.4.3.1
OPEN
SPLIT
.
141
4.4.3.2
DIRECT
COUPLING
.
142
4.4.3.3
SEPARATOR
TECHNIQUES
.
143
4.5
EVALUATION
OF
GC/MS
ANALYSES
.
144
4.5.1
PRESENTATION
OF
THE
CHROMATOGRAMS
.
144
4.5.1.1
TOTAL
ION
CURRENT
.
144
4.5.1.2
MASS
CHROMATOGRAMS
.
145
4.5.2
IDENTIFICATION
BY
LIBRARY
SEARCHES
.
145
4.5.2.1
EXTRACTION
OF
SPECTRA
.
146
4.5.2.2
REFERENCE
MASS
SPECTRA
.
146
4.5.2.3
LIBRARY
SEARCH
PROCEDURES
.
148
4.6
APPLICATIONS
.
153
4.6.1
DETERMINATION
OF
SUBSTITUTED
PHENOLS
IN
DRINKING
WATER
.
153
4.6.2
DETERMINATION
OF
PCB,
PAH,
AND
UGILEC
IN
SOIL
.
157
4.6.4
DETERMINATION
OF
CLENBUTEROL
.
168
4.7
SUMMARY
.
171
4.8
REFERENCES
.
171
INDEX
.
173 |
| any_adam_object | 1 |
| building | Verbundindex |
| bvnumber | BV011376331 |
| callnumber-first | T - Technology |
| callnumber-label | TX548 |
| callnumber-raw | TX548.2.G36 |
| callnumber-search | TX548.2.G36 |
| callnumber-sort | TX 3548.2 G36 |
| callnumber-subject | TX - Home Economics |
| classification_rvk | VG 7400 |
| ctrlnum | (OCoLC)37854326 (DE-599)BVBBV011376331 |
| dewey-full | 664/.07 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 664 - Food technology |
| dewey-raw | 664/.07 |
| dewey-search | 664/.07 |
| dewey-sort | 3664 17 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>00000nam a2200000 c 4500</leader><controlfield tag="001">BV011376331</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">19970825</controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">970603s1997 gw d||| |||| 00||| ger d</controlfield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">950510718</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">3778524194</subfield><subfield code="c">Gb. : DM 98.00, S 715.00, sfr 89.00</subfield><subfield code="9">3-7785-2419-4</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)37854326</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV011376331</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="1" ind2=" "><subfield code="a">ger</subfield><subfield code="a">eng</subfield><subfield code="h">ger</subfield></datafield><datafield tag="044" ind1=" " ind2=" "><subfield code="a">gw</subfield><subfield code="c">DE</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-703</subfield></datafield><datafield tag="050" ind1=" " ind2="0"><subfield code="a">TX548.2.G36</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">664/.07</subfield><subfield code="2">21</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VG 7400</subfield><subfield code="0">(DE-625)147205:253</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="130" ind1="0" ind2=" "><subfield code="a">Lebensmittel- und Umweltanalytik mit der Kapillar-GC</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Food and environmental analysis in capillary gas chromatography</subfield><subfield code="b">hints for practical use</subfield><subfield code="c">ed. by Lothar Matter</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Heidelberg</subfield><subfield code="b">Hüthig</subfield><subfield code="c">1997</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XII, 178 S.</subfield><subfield code="b">graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="490" ind1="0" ind2=" "><subfield code="a">Chromatographic methods</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Cromatografia gasosa</subfield><subfield code="2">larpcal</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Environmental monitoring</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Food</subfield><subfield code="x">Analysis</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Gas chromatography</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Glaskapillargaschromatographie</subfield><subfield code="0">(DE-588)4157443-6</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Glaskapillargaschromatographie</subfield><subfield code="0">(DE-588)4157443-6</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Matter, Lothar</subfield><subfield code="e">Sonstige</subfield><subfield code="4">oth</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007645328&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-007645328</subfield></datafield></record></collection> |
| id | DE-604.BV011376331 |
| illustrated | Illustrated |
| indexdate | 2024-08-18T00:09:52Z |
| institution | BVB |
| isbn | 3778524194 |
| language | German English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007645328 |
| oclc_num | 37854326 |
| open_access_boolean | |
| owner | DE-703 |
| owner_facet | DE-703 |
| physical | XII, 178 S. graph. Darst. |
| publishDate | 1997 |
| publishDateSearch | 1997 |
| publishDateSort | 1997 |
| publisher | Hüthig |
| record_format | marc |
| series2 | Chromatographic methods |
| spelling | Lebensmittel- und Umweltanalytik mit der Kapillar-GC Food and environmental analysis in capillary gas chromatography hints for practical use ed. by Lothar Matter Heidelberg Hüthig 1997 XII, 178 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chromatographic methods Cromatografia gasosa larpcal Environmental monitoring Food Analysis Gas chromatography Glaskapillargaschromatographie (DE-588)4157443-6 gnd rswk-swf Glaskapillargaschromatographie (DE-588)4157443-6 s DE-604 Matter, Lothar Sonstige oth DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007645328&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Food and environmental analysis in capillary gas chromatography hints for practical use Cromatografia gasosa larpcal Environmental monitoring Food Analysis Gas chromatography Glaskapillargaschromatographie (DE-588)4157443-6 gnd |
| subject_GND | (DE-588)4157443-6 |
| title | Food and environmental analysis in capillary gas chromatography hints for practical use |
| title_alt | Lebensmittel- und Umweltanalytik mit der Kapillar-GC |
| title_auth | Food and environmental analysis in capillary gas chromatography hints for practical use |
| title_exact_search | Food and environmental analysis in capillary gas chromatography hints for practical use |
| title_full | Food and environmental analysis in capillary gas chromatography hints for practical use ed. by Lothar Matter |
| title_fullStr | Food and environmental analysis in capillary gas chromatography hints for practical use ed. by Lothar Matter |
| title_full_unstemmed | Food and environmental analysis in capillary gas chromatography hints for practical use ed. by Lothar Matter |
| title_short | Food and environmental analysis in capillary gas chromatography |
| title_sort | food and environmental analysis in capillary gas chromatography hints for practical use |
| title_sub | hints for practical use |
| topic | Cromatografia gasosa larpcal Environmental monitoring Food Analysis Gas chromatography Glaskapillargaschromatographie (DE-588)4157443-6 gnd |
| topic_facet | Cromatografia gasosa Environmental monitoring Food Analysis Gas chromatography Glaskapillargaschromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007645328&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | UT lebensmittelundumweltanalytikmitderkapillargc AT matterlothar foodandenvironmentalanalysisincapillarygaschromatographyhintsforpracticaluse |