Modern infrared spectroscopy:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
1996
|
| Schriftenreihe: | Analytical chemistry by open learning
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XX, 180 S. zahlr. Ill. und graph. Darst. |
| ISBN: | 0471959162 0471959170 |
Internformat
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Datensatz im Suchindex
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| adam_text |
MODERN INFRARED SPECTROSCOPY ANALYTICAL CHEMISTRY BY OPEN LEARNING
AUTHOR: BARBARA STUART UNIVERSITY OF GREENWICH EDITOR: DAVID J. ANDO
UNIVERSITY OF GREENWICH PUBLISHED ON BEHALF OF ACOT (UNIVERSITY OF
GREENWICH) BY JOHN WILEY & SONS CHICHESTER * NEW YORK * BRISBANE *
TORONTO * SINGAPORE CONTENTS STUDY GUIDE XIII SUPPORTING PRACTICAL WORK
XV BIBLIOGRAPHY XVII ACKNOWLEDGEMENTS XIX 1. INTRODUCTION . . . 1 1.1.
GENERAL INTRODUCTION 1 1.2. ELECTROMAGNETIC RADIATION 2 1.3. VIBRATIONS
OF MOLECULES 6 1.3.1. NORMAL MODES OF VIBRATION 7 1.3.2. INTENSITY OF
INFRARED BANDS 13 2. INSTRUMENTATION 19 2.1. INTRODUCTION 19 2.2.
REPRESENTATION OF SPECTRA 19 2.3. DISPERSIVE SPECTROMETERS 20 2.3.1.
MONOCHROMATORS 21 2.3.2. DOUBLE-BEAM INSTRUMENTS 22 2.3.3. SOURCES AND
DETECTORS 22 2.3.4. LIMITATIONS 23 - 2.4. FOURIER-TRANSFORM INFRARED
SPECTROMETERS 24 2.4.1. THE MICHELSON INTERFEROMETER 24 2.4.2. FOURIER
TRANSFORMATION 26 2.4.3. ADVANTAGES OF FOURIER-TRANSFORM INFRARED
SPECTROSCOPY . . : 27 2.4.4. SOURCES AND DETECTORS 28 2.4.5. THE MOVING
MIRROR 28 IX ANALYTICAL CHEMISTRY BY OPEN LEARNING 3. SAMPLING 32 3.1.
INTRODUCTION 32 3.2. TRANSMISSION METHODS 32 3.2.1. LIQUIDS AND
SOLUTIONS 32 3.2.2. SOLIDS 37 3.2.3. GASES 42 3.2.4. PATHLENGTH
CALIBRATION 42 3.3. REFLECTANCE METHODS 44 3.3.1. ATTENUATED TOTAL
REFLECTANCE SPECTROSCOPY 45 3.3.2. SPECULAR REFLECTANCE 48 3.3.3.
DIFFUSE REFLECTANCE 49 3.4. OTHER TECHNIQUES 51 3.4.1. PHOTOACOUSTIC
SPECTROSCOPY 51 3.4.2. THE USE OF TEMPERATURE CELLS 52 3.4.3.
MICROSAMPLING 52 3.4.4. COMBINATION TECHNIQUES 52 4. SPECTRUM
INTERPRETATION 55 4.1. INTRODUCTION . 55 4.2. GROUP FREQUENCIES 55
4.2.1. THE X*H STRETCHING REGION (4000-2500 CM' 1 ) . 55 4.2.2. TRIPLE
BOND REGION (2500-2000 CM" 1 ) 60 4.2.3. DOUBLE BOND REGION (2000-1500
CM" 1 ) 61 4.2.4. FINGERPRINT REGION (1500-600 CM" 1 ) 66 4.3.
COMPLICATING FACTORS 67 4.3.1. OVERTONE AND COMBINATION BANDS 67 .--
4.3.2. FERMI RESONANCE 69 4.3.3. HYDROGEN BONDING .70 5. QUANTITATIVE
ANALYSIS -. . . 75 5.1. INTRODUCTION 75 5.2. SPECTRUM MANIPULATION 75
5.2.1. BASELINE CORRECTION 76 5.2.2. SMOOTHING 76 5.2.3. DERIVATIVES 77
5.2.4. DECONVOLUTION 79 5.2.5. CURVE-FITTING. 81 5.3. DETERMINATION OF
CONCENTRATION 81 5.4. SIMPLE ANALYSIS 85 5.4.1. ANALYSIS OF LIQUID
SAMPLES 85 CONTENTS XI 5.4.2. ANALYSIS OF SOLID SAMPLES 91 5.5.
MULTICOMPONENT ANALYSIS 92 6. APPLICATIONS 97 6.1. INTRODUCTION 97 6.2.
ORGANIC COMPOUNDS 97 6.2.1. ALKANES 97 6.2.2. ALKENES 99 6.2.3. ALKYNES
100 6.2.4. AROMATIC COMPOUNDS 101 6.2.5. ALCOHOLS, PHENOLS AND ETHERS
104 6.2.6. AMINES 104 6.2.7. ALDEHYDES AND KETONES 105 6.2.8. OTHER
CARBONYL CONTAINING COMPOUNDS 106 6.2.9. OTHER NITROGEN CONTAINING
COMPOUNDS 107 6.2.10. SULPHUR CONTAINING COMPOUNDS 107 6.2.11. HALOGEN
CONTAINING COMPOUNDS 108 6.3. INORGANIC COMPOUNDS 109 6.3.1. BORON
COMPOUNDS 109 6.3.2. SILICON COMPOUNDS 109 6.3.3. PHOSPHORUS COMPOUNDS
110 6.4. POLYMERS 113 6.4.1. SAMPLE PREPARATION 113 6.4.2. POLYPROPYLENE
113 6.5. BIOLOGICAL SYSTEMS 117 6.5.1. SAMPLE PREPARATION 117 6.5.2.
PROTEINS 117 6.5.3. LIPIDS 119 6.6. DRUG ANALYSIS 121 6.7. POLLUTION
MONITORING 121 6.8. COAL 123 6.9. MINERALS 123 6.10. CATALYSTS 123 7.
IDENTIFICATION OF UNKNOWN SAMPLES 126 7.1. INTRODUCTION. . . .' 126
7.2. STRATEGY , 126 7.3. EXAMPLES 128 7.4. EXAMPLES FOR FURTHER PRACTICE
132 XII ANALYTICAL CHEMISTRY BY OPEN LEARNING APPENDIX 1. CORRELATION
TABLE FOR ORGANIC MOLECULES 136 2. CORRELATION TABLE FOR THE
OUT-OF-PLANE BENDING VIBRATIONS OF BENZENOID COMPOUNDS 137 3.
CORRELATION TABLE FOR CARBONYL STRETCHING FREQUENCIES . . 138 4.
CORRELATION TABLE FOR THE OUT-OF-PLANE BENDING VIBRATIONS OF ALKENES 139
SELF-ASSESSMENT QUESTIONS AND RESPONSES 140 UNITS OF MEASUREMENT 171
INDEX 177 |
| any_adam_object | 1 |
| author | Stuart, Barbara H. |
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| author_sort | Stuart, Barbara H. |
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| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543/.08583/077 |
| dewey-search | 543/.08583/077 |
| dewey-sort | 3543 48583 277 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-08-05T08:36:01Z |
| institution | BVB |
| isbn | 0471959162 0471959170 |
| language | Undetermined |
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| oclc_num | 246847608 |
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| physical | XX, 180 S. zahlr. Ill. und graph. Darst. |
| publishDate | 1996 |
| publishDateSearch | 1996 |
| publishDateSort | 1996 |
| publisher | Wiley |
| record_format | marc |
| series2 | Analytical chemistry by open learning |
| spellingShingle | Stuart, Barbara H. Modern infrared spectroscopy Chemistry, Analytic Programmed instruction Infrared spectroscopy Programmed instruction Infrarotspektroskopie (DE-588)4135411-4 gnd |
| subject_GND | (DE-588)4135411-4 |
| title | Modern infrared spectroscopy |
| title_auth | Modern infrared spectroscopy |
| title_exact_search | Modern infrared spectroscopy |
| title_full | Modern infrared spectroscopy author: Barbara Stuart |
| title_fullStr | Modern infrared spectroscopy author: Barbara Stuart |
| title_full_unstemmed | Modern infrared spectroscopy author: Barbara Stuart |
| title_short | Modern infrared spectroscopy |
| title_sort | modern infrared spectroscopy |
| topic | Chemistry, Analytic Programmed instruction Infrared spectroscopy Programmed instruction Infrarotspektroskopie (DE-588)4135411-4 gnd |
| topic_facet | Chemistry, Analytic Programmed instruction Infrared spectroscopy Programmed instruction Infrarotspektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007539954&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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Inhaltsverzeichnis
THWS Schweinfurt Magazin
| Signatur: |
2801 2014:0026 |
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| Exemplar 1 | ausleihbar Verfügbar Bestellen |