Chemistry and technology of isocyanates:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester [u.a.]
Wiley
1996
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIII, 489 S. graph. Darst. |
| ISBN: | 0471963712 |
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| 100 | 1 | |a Ulrich, Henri |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chemistry and technology of isocyanates |c Henri Ulrich |
| 264 | 1 | |a Chichester [u.a.] |b Wiley |c 1996 | |
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Datensatz im Suchindex
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| adam_text | CHEMISTRY AND TECHNOLOGY OF ISOCYANATES HENRI ULRICH CHEMICAL CONSULTANT
GUILFORD, CT, USA JOHN WILEY & SONS CHICHESTER * NEW YORK * BRISBANE *
TORONTO * SINGAPORE CONTENTS PREFACE XI ACKNOWLEDGMENTS XUEI 1
MONOISOCYANATES 1 1.1 ALKYL AND ARYL ISOCYANATES 1 1.1.1 INTRODUCTION 1
1.1.2 SYNTHESIS OF ALKYL AND ARYL ISOCYANATES 3 1.1.2.1 SYNTHESIS BY
PHOSGENATION REACTIONS 3 1.1.2.2 FORMATION OF ALKYL AND ARYL ISOCYANATES
VIA NITRENE INTERMEDIATES 11 1.1.2.3 FORMATION OF ALKYL AND ARYL
ISOCYANATES BY THERMAL PROCESSES 19 1.1.2.4 REARRANGEMENTS OF NITRILE
OXIDES AND CYANATES 26 1.1.2.5 REACTIONS OF ORGANIC HALIDES WITH SALTS
OF CYANIC ACID 27 1.1.2.6 REACTION OF OLEFINS AND ALDEHYDES WITH
ISOCYANIC ACID 28 1.1.2.7 ISOCYANATES FROM OTHER HETEROCUMULENES 29
1.1.2.8 FROM IMINES AND PHOSPHINEIMINES 30 1.1.2.9 MISCELLANEOUS
SYNTHETIC METHODS 31 1.1.3 REFERENCES 36 1.1.4 REACTIONS OF ALKYL AND
ARYL ISOCYANATES 42 1.1.4.1 INTRODUCTION 42 1.1.4.2 ROLIGOMERIZATION AND
POLYMERIZATION 45 1.1.4.3 CYCLOADDITION REACTIONS 54 1.1.4.4
NUCLEOPHILIC REACTIONS 98 1.1.4.5 INSERTION REACTIONS 106 1.1.4.6
MISCELLANEOUS REACTIONS 124 1.1.5 REFERENCES 133 VI CONTENTS 1.2
UNSATURATED ISOCYANATES 149 1.2.1 INTRODUCTION 149 1.2.2 SYNTHESIS OF
UNSATURATED ISOCYANATES 149 1.2.2.1 ELIMINATION OF HYDROGEN HALIDE FROM
HALOGENATED ISOCYANATES 149 1.2.2.2 SYNTHESIS VIA NITRENE INTERMEDIATES
150 1.2.2.3 FROM AMINES, IMINES OR NITRILES AND PHOSGENE 152 1.2.2.4
MISCELLANEOUS SYNTHETIC METHODS 154 1.2.3 REACTIONS OF UNSATURATED
ISOCYANATES 157 1.2.3.1 HOMOPOLYMERIZATION 157 1.2.3.2 COPOLYMERIZATION
157 1.2.3.3 NUCLEOPHILIC REACTIONS 157 1.2.3.4 CYCLOADDITION REACTIONS
157 1.2.3.5 MISCELLANEOUS REACTIONS 160 1.2.4 REFERENCES 161 1.3
HALOGENATED ALKYL AND ARYL ISOCYANATES 163 1.3.1 INTRODUCTION 163 1.3.2
SYNTHESIS OF HALOGENATED ALKYL AND ARYL ISOCYANATES 163 1.3.2.1
HALOGENATION OF ALKYL AND ARYL ISOCYANATES 163 1.3.2.2 HALOGENATION OF
ACYL AND THIOACYL ISOCYANATES 167 1.3.2.3 ADDITION OF HALOGEN TO
UNSATURATED ISOCYANATES 168 1.3.2.4 REACTION OF AMINES, IMINES AND
NITRILES WITH PHOSGENE AND ANALOGUES 168 1.3.2.5 SYNTHESIS OF
HALOGENATED ISOCYANATES VIA NITRENE INTERMEDIATES 172 1.3.2.6
MISCELLANEOUS SYNTHETIC METHODS 174 1.3.3 REACTIONS OF HALOGENATED
ISOCYANATES 179 1.3.3.1 NUCLEOPHILIC REACTIONS 179 1.3.3.2 ELIMINATION
OF HYDROGEN HALIDES AND ACIDS 188 1.3.3.3 EXCHANGE REACTIONS WITH
SILYLATED HETEROCUMULENES 188 1.3.3.4 REACTIONS WITH OXIRANES AND
AZIRIDINES 188 1.3.3.5 REACTIONS WITH MULTIPLE BOND SYSTEMS 189 1.3.3.6
CYCLOADDITION REACTIONS 190 1.3.3.7 INSERTION REACTIONS 190 1.3.3.8
MISCELLANEOUS REACTIONS 190 1.3.4 REFERENCES 192 1.4 CARBONYL,
THIOCARBONYL AND IMIDOYL ISOCYANATES 197 1.4.1 INTRODUCTION 197 1.4.2
SYNTHESIS 197 1.4.2.1 SYNTHESIS OF CARBONYL ISOCYANATES 197 1.4.2.2
SYNTHESIS OF THIOCARBONYL ISOCYANATES 212 1.4.2.3 SYNTHESIS OF IMIDOYL
ISOCYANATES 213 CONTENTS VII 1.4.3 REACTIONS 216 1.4.3.1 REACTIONS OF
CARBONYL ISOCYANATES 216 1.4.3.2 REACTIONS OF THIOCARBONYL ISOCYANATES
231 1.4.3.3 REACTIONS OF IMIDOYL ISOCYANATES 235 1.4.4 REFERENCES 235
1.5 SULFUR ISOCYANATES 241 1.5.1 INTRODUCTION 241 1.5.2 SYNTHESIS 241
1.5.2.1 SYNTHESIS OF DIVALENT SULFUR ISOCYANATES 241 1.5.2.2 SYNTHESIS
OF TETRAVALENT SULFUR ISOCYANATES 242 1.5.2.3 SYNTHESIS OF HEXAVALENT
SULFUR ISOCYANATES 242 1.5.3 REACTIONS OF SULFUR ISOCYANATES 248 1.5.3.1
NUCLEOPHILIC REACTIONS 248 1.5.3.2 CYCLOADDITION REACTIONS 252 1.5.3.3
MISCELLANEOUS REACTIONS 269 1.5.4 REFERENCES 274 1.6 PHOSPHORUS
ISOCYANATES 279 1.6.1 INTRODUCTION 279 1.6.2 SYNTHESIS OF PHOSPHORUS
ISOCYANATES 280 1.6.2.1 FROM PHOSPHORUS HALIDES AND CYANIC ACID AND ITS
SALTS 280 1.6.2.2 FROM CARBAMATES 281 1.6.2.3 FROM PHOSPHORYL AMIDES AND
OXALYL CHLORIDE 282 1.6.2.4 MISCELLANEOUS SYNTHETIC METHODS 282 1.6.3
REACTIONS OF PHOSPHORUS ISOCYANATES 284 1.6.3.1 REACTION WITH *OH
COMPOUNDS 284 1.6.3.2 REACTION WITH AMINES AND HYDRAZINES 284 1.6.3.3
CYCLOADDITION REACTIONS 284 1.6.3.4 MISCELLANEOUS REACTIONS 286 1.6.4
REFERENCES 287 1.7 INORGANIC ISOCYANATES 290 1.7.1 INTRODUCTION 290
1.7.2 SYNTHESIS OF INORGANIC ISOCYANATES 290 1.7.2.1 MAIN GROUP LILA
ISOCYANATES 290 1.7.2.2 MAIN GROUP IVA ISOCYANATES 291 1.7.2.3 MAIN
GROUP VA ISOCYANATES 293 1.7.2.4 MAIN GROUP VIA ISOCYANATES 296 1.7.2.5
MAIN GROUP VLLA ISOCYANATES 297 1.7.2.6 LIGANDED TRANSITION METAL
ISOCYANATES 297 1.7.3 REACTIONS OF INORGANIC ISOCYANATES 299 1.7.4
REFERENCES 300 1.8 APPLICATIONS OF MONOISOCYANATES 303 1.8.1
AGRICULTURAL AND PHARMACEUTICAL PRODUCTS 303 1.8.2 MONOISOCYANATES IN
POLYMER MODIFICATION 305 VIII CONTENTS 1.8.3 AS REAGENTS IN ORGANIC
SYNTHESIS 308 1.8.4 MISCELLANEOUS APPLICATIONS 311 1.8.5 REFERENCES 312
DIISOCYANATES 315 2.1 ALIPHATIC DIISOCYANATES 315 2.1.1 INTRODUCTION 315
2.1.2 SYNTHESIS OF ALIPHATIC DIISOCYANATES 328 2.1.2.1 PHOSGENATION OF
AMINES 328 2.1.2.2 NONPHOSGENE PROCESSES 333 2.1.2.3 FORMATION VIA
NITRENE INTERMEDIATES 334 2.1.2.4 FROM OLEFINS AND ISOCYANIC ACID OR
ETHYL CARBAMATE 337 2.1.2.5 FROM ORGANIC DIHALIDES AND SALTS OF
ISOCYANIC ACID 338 2.1.2.6 MISCELLANEOUS SYNTHETIC METHODS 338 2.1.3
MANUFACTURE OF MAJOR ALIPHATIC DIISOCYANATES 342 2.1.3.1 HEXAMETHYLENE
DIISOCYANATE (HDI) 342 2.1.3.2 ISOPHORONE (IPDI) AND
TNMETHYLHEXAMETHYLENE DIISOCYANATES (TMHDI) 343 2.1.3.3 HMDI 344 2.1.3.4
TRANS-CYCLOHEXANE DIISOCYANATE (CHDI) 345 2.1.3.5 TETRAMETHYLXYLYLENE
DIISOCYANATE (TMXDI) 346 2.1.4 REACTIONS OF ALIPHATIC DIISOCYANATES 347
2.1.4.1 HOMOPOLYMERIZATION 347 2.1.4.2 COPOLYMERIZATION 348 2.1.4.3
ADDITION POLYMERIZATION 349 2.1.4.4 CONDENSATION POLYMERIZATION 350
2.1.4.5 OTHER REACTIONS OF ALIPHATIC DIISOCYANATES 351 2.1.5
APPLICATIONS OF ALIPHATIC DIISOCYANATES 356 2.1.5.1 POLYURETHANES 356
2.1.6 REFERENCES 361 2.2 AROMATIC DIISOCYANATES 368 2.2.1 INTRODUCTION
368 2.2.2 SYNTHESIS 372 2.2.2.1 PHOSGENATION OF AMINES 372 2.2.2.2
NONPHOSGENE PROCESSES 375 2.2.2.3 AROMATIC DIISOCYANATES VIA NITRENE
INTERMEDIATES 379 2.2.2.4 AROMATIC DIISOCYANATES BY COUPLING OF
MONOISOCYANATES OR ISOCYANATE PRECURSORS 380 2.2.2.5 MISCELLANEOUS
SYNTHESES OF AROMATIC DIISOCYANATES 384 2.2.3 MANUFACTURE OF AROMATIC
DIISOCYANATES 385 CONTENTS IX 2.2.3.1 MDI AND POLYMERIE ISOCYANATES
(PMDI) 385 2.2.3.2 TOLYLENE DIISOCYANATE (TDI) 392 2.2.3.3 P-PHENYLENE
DIISOCYANATE (PPDI) 394 2.2.3.4 NAPHTHALENE DIISOCYANATE (NDI) 394 2.2.4
REACTIONS OF AROMATIC DIISOCYANATES 395 2.2.4.1 HOMOPOLYMERIZATION
REACTIONS 395 2.2.4.2 COPOLYMERIZATION REACTIONS 395 2.2.4.3
CYCLOPOLYMERIZATION REACTIONS 395 2.2.4.4 ADDITION POLYMERIZATION
REACTIONS 396 2.2.4.5 CONDENSATION POLYMERIZATION REACTIONS 410 2.2.4.6
OTHER REACTIONS OF AROMATIC DIISOCYANATES 416 2.2.5 APPLICATIONS OF
AROMATIC DIISOCYANATES 426 2.2.5.1 POLYURETHANES 426 2.2.5.2
POLY(URETHANE UREAS) AND POLYUREAS 446 2.2.5.3 POLY(URETHANE
ISOEYANURATES) 450 2.2.5.4 BINDER RESINS 452 2.2.5.5 POLYAMIDES 455
2.2.5.6 POLY(AMIDE IMIDES) AND POLYIMIDES 456 2.2.6 REFERENCES 456 3
ENVIRONMENTAL CONSIDERATIONS 469 3.1 TOXICITY 469 3.1.1 TOXICITY OF
ISOCYANATES 469 3.1.2 TOXICITY OF CHEMICALS USED IN ISOCYANATE
MANUFACTURE 472 3.1.3 TOXICITY OF ISOCYANATE DERIVED PRODUCTS 472 3.2
SAFETY ASPECTS 473 3.2.1 STORAGE AND HANDLING OF ISOCYANATES 473 3.2.2
SAFETY OF ISOCYANATE PRODUCTION 474 3.2.3 FIRE SAFETY OF ISOCYANATE
DERIVED PRODUCTS 475 3.3 ENVIRONMENTAL IMPACT 475 3.3.1 DISPOSAL OF
BY-PRODUCTS IN ISOCYANATE MANUFACTURE 475 3.3.2 DISPOSAL OF ISOCYANATE
DERIVED PRODUCTS 476 3.3.3 REPLACEMENT OF CFCS IN CELLULAR PRODUCTS 477
3.4 ISOCYANATES AND POLYURETHANE CHEMICALS BASED ON RENEWABLE RESOURCES
478 3.4.1 ISOCYANATES BASED ON RENEWABLE RESOURCES 478 3.4.2 POLYOLS
BASED ON RENEWABLE RESOURCES 479 3.5 A WORLD WITHOUT ISOCYANATES 479 3.6
REFERENCES 481 INDEX 483
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| isbn | 0471963712 |
| language | English |
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| spelling | Ulrich, Henri Verfasser aut Chemistry and technology of isocyanates Henri Ulrich Chichester [u.a.] Wiley 1996 XIII, 489 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Diisocyanaten gtt Isocyanaten gtt Isocyanates ram Polyuréthanes ram Isocyanates Isocyanate (DE-588)4162492-0 gnd rswk-swf Isocyanate (DE-588)4162492-0 s DE-604 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007467738&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ulrich, Henri Chemistry and technology of isocyanates Diisocyanaten gtt Isocyanaten gtt Isocyanates ram Polyuréthanes ram Isocyanates Isocyanate (DE-588)4162492-0 gnd |
| subject_GND | (DE-588)4162492-0 |
| title | Chemistry and technology of isocyanates |
| title_auth | Chemistry and technology of isocyanates |
| title_exact_search | Chemistry and technology of isocyanates |
| title_full | Chemistry and technology of isocyanates Henri Ulrich |
| title_fullStr | Chemistry and technology of isocyanates Henri Ulrich |
| title_full_unstemmed | Chemistry and technology of isocyanates Henri Ulrich |
| title_short | Chemistry and technology of isocyanates |
| title_sort | chemistry and technology of isocyanates |
| topic | Diisocyanaten gtt Isocyanaten gtt Isocyanates ram Polyuréthanes ram Isocyanates Isocyanate (DE-588)4162492-0 gnd |
| topic_facet | Diisocyanaten Isocyanaten Isocyanates Polyuréthanes Isocyanate |
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