Sodium resistant binder carbon for aluminium reduction cell cathodes:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Düsseldorf
VDI-Verl.
1996
|
| Edition: | Als Ms. gedr. |
| Series: | Verein Deutscher Ingenieure: [Fortschritt-Berichte VDI / 21]
208 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | 184 S. graph. Darst. |
| ISBN: | 3183208210 |
Staff View
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Record in the Search Index
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| adam_text | Titel: Sodium resistant binder carbon for aluminium reduction cell cathodes
Autor: Jurić, Drago Dragutin
Jahr: 1996
SCHRITT- m ÈfW^n BERICHTEmM^jB Drago Dragutinjuri?, Bulleen, Vic. Sodium Resistant Binder Carbon for Aluminium Reduction Cell Cathodes Reihe 21: Elektrotechnik Nr. 208 VW VERLAS
1 INTRODUCTION 1.1 Service Demands on Aluminium Reduction Cell Cathodes 1 1.2 Properties and Formation of Sodium Resistant Carbon 4 1.2.1 Carbon Structure and Properties 4 1.2.2 Formation of High Fermi Level Carbon 6 1.3 Possible Alternative Routes to Sodium Resistant Carbon 7 1.3.1 Pyrolysis Mechanism 7 1.3.2 Strain Ordering 8 1.3.3 Incorporation of Nitrogen 9 1.4 Objectives and Hypothesis 10 2 EXPERIMENTAL 2.1 Materials Used in This Study 11 2.1.1 Reagents 11 2.1.2 Gases 12 2.2 Analytical Methods 13 2.2.1 Size Exclusion Chromatography 13 2.2.2 Fourier Transformed Infrared Spectroscopy 13 2.2.3 Nuclear Magnetic Resonance Spectroscopy 14 2.2.4 pH Measurement 15 2.2.5 Elemental Analysis 16 2.2.6 Thermal Analysis 16 2.2.7 Gas Analysis 17 2.2.8 Autoclave Tests 19 2.2.9 X-ray Diffraction 20 2.2.10 X-ray Photoelectron Spectroscopy 21 2.2.11 Mercury Intrusion Porosimetry 22 2.2.12 Microporosity 22
2.2.13 Laser Raman Spectroscopy 22 2.2.14 Transmission Electron Microscopy 22 2.3 Preparative Procedures 23 2.3.1 Sample Preparation 23 2.3.2 Titanium Diboride Reactivity in Resin Environment 24 2.3.3 Curing 24 2.3.4 Pyrolysis 26 3 RESULTS 3.1 Resin Curing Studies 27 3.1.1 Novolac-Hexamine System 27 3.1.2 Furfuryl Alcohol-Hexamine Reactions 33 3.1.3 Novolac-Furfuryl Alcohol-Hexamine 35 3.1.3.1 Thermal Analysis 35 3.1.3.2 Factors Influencing Curing 38 3.1.3.3 Chemical Changes During Curing 44 3.1.3.4 Structural Changes During Curing 48 3.1.3.5 Physical Changes During Curing 54 3.1.3.6 Optimum Binder Composition 60 3.2 Effect of Titanium Diboride on Curing of Novolak-Furfuryl Alcohol Binder 62 3.2.1 Characterisation of Titanium Diboride Powder 62 3.2.2 Titanium Diboride - Resin Interactions 65 3.2.3 Effect of Impurities on Curing Reaction 67 3.2.3.1 Boron Oxide 67 3.2.3.2 Organo-Titanium Catalyst 70 3.2.3.3 Titanium Diboride 70 3.2.3.4 Boron Oxide/Hexamine 71
3.2.4 Evolved Gas Analysis 74 3.2.4.1 Boron Oxide 74 3.2.4.2 Titanium Diboride 76 3.2.5 Structure of Polymer 77 3.2.5.1 Boron Oxide 77 3.2.5.2 Organo-Titanium Catalyst 78 3.2.5.3 Titanium Diboride 79 3.2.6 Curing Yield 80 Pyrolysis Studies 83 3.3.1 Thermal Analysis 83 3.3.1.1 Conventional Resin Systems 83 3.3.1.2 Hexamine Cured Novolak-Furfuryl Alcohol Polymer 87 3.3.1.3 Factors Affecting Pyrolysis 90 3.3.1.4 Pyrolysis Kinetics 93 3.3.2 Structural Changes of Char During Baking 95 3.3.2.1 Thermal Analysis of Polymer 95 3.3.2.2 Infra-red Spectra 96 3.3.2.2.1 Novolak-Furfuryl Alcohol Polymer 96 3.3.2.2.2 Boron Oxide 99 3.3.2.3 Organo-Titanium Catalyst 102 3.3.3 Evolved Gas Analysis 103 3.3.4 Chemical Changes of Char During Pyrolysis 110 3.3.4.1 Factors Affecting Carbon Retention 111 3.3.4.1.1 Composition 111 3.3.4.1.2 Effect of Impurities 112 3.3.4.2 Factors Affecting Nitrogen Retention 114 Structure of Carbon Formed 116 3.4.1 Pore Size Distribution 116 3.4.1.1 Char from Pure Resins 116
3.4.1.2 Titanium Diboride - Carbon Composite 118 3.4.2 Microstructure of Carbons Formed 119 3.4.2.1 Carbon from Pure Resins 119 3.4.2.2 Titanium Diboride - Carbon Composite 123 3.4.3 X-ray Diffraction Analysis 124 3.4.3.1 Char from Pure Resins 124 3.4.3.2 Titanium Diboride - Carbon Composite 127 3.4.4 Laser Raman Spectroscopy 129 3.4.4.1 Char from Pure Resins 129 3.4.4.2 Titanium Diboride - Carbon Composite 131 4 DISCUSSION 133 APPENDIX 1 143 APPENDIX 2 147 APPENDIX 3 161 APPENDIX 4 177 APPENDIX 5 180 BIBLIOGRAPHY 181 Biography 185
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| any_adam_object | 1 |
| author | Jurić, Drago Dragutin |
| author_facet | Jurić, Drago Dragutin |
| author_role | aut |
| author_sort | Jurić, Drago Dragutin |
| author_variant | d d j dd ddj |
| building | Verbundindex |
| bvnumber | BV011027249 |
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| discipline | Hüttenwesen, Metallurgie |
| edition | Als Ms. gedr. |
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| spelling | Jurić, Drago Dragutin Verfasser aut Sodium resistant binder carbon for aluminium reduction cell cathodes Drago Dragutin Jurić Als Ms. gedr. Düsseldorf VDI-Verl. 1996 184 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Verein Deutscher Ingenieure: [Fortschritt-Berichte VDI / 21] 208 Zugl.: Karlsruhe, Univ., Diss., 1996 Aluminiumschmelzflusselektrolyse (DE-588)4128234-6 gnd rswk-swf Aushärtung Kunststoff (DE-588)4284851-9 gnd rswk-swf Furfurylalkohol (DE-588)4405813-5 gnd rswk-swf Kunstharz (DE-588)4033651-7 gnd rswk-swf Dünne Schicht (DE-588)4136925-7 gnd rswk-swf Novolak (DE-588)4321559-2 gnd rswk-swf Beschichten (DE-588)4005996-0 gnd rswk-swf Pyrolyse (DE-588)4047925-0 gnd rswk-swf Kathode (DE-588)4163451-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Aluminiumschmelzflusselektrolyse (DE-588)4128234-6 s Kathode (DE-588)4163451-2 s Beschichten (DE-588)4005996-0 s Kunstharz (DE-588)4033651-7 s DE-604 Novolak (DE-588)4321559-2 s Furfurylalkohol (DE-588)4405813-5 s Dünne Schicht (DE-588)4136925-7 s Aushärtung Kunststoff (DE-588)4284851-9 s Pyrolyse (DE-588)4047925-0 s 21] Verein Deutscher Ingenieure: [Fortschritt-Berichte VDI 208 (DE-604)BV001897864 208 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007383211&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Jurić, Drago Dragutin Sodium resistant binder carbon for aluminium reduction cell cathodes Aluminiumschmelzflusselektrolyse (DE-588)4128234-6 gnd Aushärtung Kunststoff (DE-588)4284851-9 gnd Furfurylalkohol (DE-588)4405813-5 gnd Kunstharz (DE-588)4033651-7 gnd Dünne Schicht (DE-588)4136925-7 gnd Novolak (DE-588)4321559-2 gnd Beschichten (DE-588)4005996-0 gnd Pyrolyse (DE-588)4047925-0 gnd Kathode (DE-588)4163451-2 gnd |
| subject_GND | (DE-588)4128234-6 (DE-588)4284851-9 (DE-588)4405813-5 (DE-588)4033651-7 (DE-588)4136925-7 (DE-588)4321559-2 (DE-588)4005996-0 (DE-588)4047925-0 (DE-588)4163451-2 (DE-588)4113937-9 |
| title | Sodium resistant binder carbon for aluminium reduction cell cathodes |
| title_auth | Sodium resistant binder carbon for aluminium reduction cell cathodes |
| title_exact_search | Sodium resistant binder carbon for aluminium reduction cell cathodes |
| title_full | Sodium resistant binder carbon for aluminium reduction cell cathodes Drago Dragutin Jurić |
| title_fullStr | Sodium resistant binder carbon for aluminium reduction cell cathodes Drago Dragutin Jurić |
| title_full_unstemmed | Sodium resistant binder carbon for aluminium reduction cell cathodes Drago Dragutin Jurić |
| title_short | Sodium resistant binder carbon for aluminium reduction cell cathodes |
| title_sort | sodium resistant binder carbon for aluminium reduction cell cathodes |
| topic | Aluminiumschmelzflusselektrolyse (DE-588)4128234-6 gnd Aushärtung Kunststoff (DE-588)4284851-9 gnd Furfurylalkohol (DE-588)4405813-5 gnd Kunstharz (DE-588)4033651-7 gnd Dünne Schicht (DE-588)4136925-7 gnd Novolak (DE-588)4321559-2 gnd Beschichten (DE-588)4005996-0 gnd Pyrolyse (DE-588)4047925-0 gnd Kathode (DE-588)4163451-2 gnd |
| topic_facet | Aluminiumschmelzflusselektrolyse Aushärtung Kunststoff Furfurylalkohol Kunstharz Dünne Schicht Novolak Beschichten Pyrolyse Kathode Hochschulschrift |
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