Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine: Synthese, Strukturaufklärung und Stabilitätsuntersuchungen
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | German |
| Veröffentlicht: |
1995
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | VII, 181 S. graph. Darst. |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV010689047 | ||
| 003 | DE-604 | ||
| 007 | t | ||
| 008 | 960328s1995 d||| m||| 00||| gerod | ||
| 016 | 7 | |a 945726759 |2 DE-101 | |
| 035 | |a (OCoLC)258332119 | ||
| 035 | |a (DE-599)BVBBV010689047 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a ger | |
| 049 | |a DE-91 |a DE-29T |a DE-355 |a DE-11 |a DE-188 | ||
| 100 | 1 | |a Hiebl, Wilfried |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine |b Synthese, Strukturaufklärung und Stabilitätsuntersuchungen |c Wilfried Hiebl |
| 264 | 1 | |c 1995 | |
| 300 | |a VII, 181 S. |b graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |a Ulm, Univ., Diss., 1995 | ||
| 650 | 0 | 7 | |a Cyclole |0 (DE-588)4433831-4 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Chemische Synthese |0 (DE-588)4133806-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Cyclopeptide |0 (DE-588)4148612-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Tripeptide |0 (DE-588)4186193-0 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Tripeptide |0 (DE-588)4186193-0 |D s |
| 689 | 0 | 1 | |a Cyclopeptide |0 (DE-588)4148612-2 |D s |
| 689 | 0 | 2 | |a Chemische Synthese |0 (DE-588)4133806-6 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Cyclole |0 (DE-588)4433831-4 |D s |
| 689 | 1 | 1 | |a Chemische Synthese |0 (DE-588)4133806-6 |D s |
| 689 | 1 | |5 DE-604 | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007135158&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-007135158 | |
Datensatz im Suchindex
| _version_ | 1807773912094736384 |
|---|---|
| adam_text |
-III
INHALTSVERZEICHNIS
ABKUERZUNGEN
1
A
ZUSAMMENFASSUNG
3
B
EINFUEHRUNG
7
1.
BEDEUTUNG
VON
AMINOSAEUREN,
PEPTIDEN
UND
PROTEINEN
7
2.
EIGENSCHAFTEN,
REAKTIONEN
UND
SYNTHESE
CYCLISCHER
PEPTIDE
11
C
AUFGABENSTELLUNG
17
D
ALLGEMEINER
TEIL
18
1.
SYNTHESEPLAN
18
2.
SYNTHESE
DER
LINEAREN
UND
CYCLISCHEN
PEPTID-VORSTUFEN
20
2.1.
N-BENZYLOXYCARBONYL-AMINOSAEUREN
20
2.2.
AMINOSAEUREMETHYLESTER-HYDROCHLORIDE
21
2.3.
N-BENZYLOXYCARBONYL-DIPEPTIDMETHYLESTER
23
2.4.
DIKETOPIPERAZINE
25
2.4.1.
SYNTHESE
25
2.4.2.
CYDO-(GLYCYL-L-PROLYL)
(C-(GLY-L-PRO))
28
2.4.3.
CYCLO-(GLYCYL-D-PROLYL)
(C-(GLY-D-PRO))
29
2.4.4.
CYCLO-(L-PROLYL-L-VALYL)
(C-(L-PRO-L-VAL))
30
2.4.5.
CYCLO-(D-PROLYL-L-VALYL)
(C-(D-PRO-L-VAL))
31
2.4.6.
CYCLO-(GLYCYL-L-VALYL)
(C-(GLY-L-VAL))
32
2.4.7.
CYCLO-(L-VALYL-L-VALYL)
(C-(L-VAL-L-VAL))
33
2.5.
N-TRIMETHYLSILYL-DIKETOPIPERAZINE
34
2.6.
N,N'-BIS-(TRIMETHYLSILYL)-DIKETOPIPERAZINE
36
2.7.
N-BENZYLOXYCARBONYL-AMINOSAEURECHLORIDE
37
-IV
2.8.
N-(BENZYLOXYCARBONYL-AMINOACYL)-DIKETOPIPERAZINE
39
2.8.1.
SYNTHESE
39
2.8.2.
N-(BENZYLOXYCARBONYL-D-PROLYL)-CYDO-(GLYCYL-L-PROLYL
)
(Z-D-PRO-C-(GLY-L-PRO))
42
2.8.3.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(GLYCYL-D~PROLYL)
(Z-L-PRO-C-(GLY-D-PRO))
43
2.8.4.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYDO-(L-VALYL-L-PROLYL)
(Z-L-PRO-C-(L-VAL-L-PRO))
44
2.8.5.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(L-VALYL-D-PROLYL)
(Z-L-PRO-C-(L-VAL-D-PRO))
45
2.8.6.
N-(BENZYLOXYCARBONY1-L-PROLY
1
)-CYCLO-(GLYCYL-L-VALYL
)
(Z-L-PRO-C-(GLY-L-VAL))
46
2.8.7.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(L-VALYL-L-VALYL)
(Z-L-PRO-C-(L-VAL-L-VAL))
47
2.9.
N,N'-BIS-(BENZYLOXYCARBONYL-AMINOACYL)-DIKETOPIPERAZINE
48
3.
AMINOACYLEINLAGERUNGEN
51
3.1.
VORGEHEN
51
3.2.
AMINOACYLEINLAGERUNG
VON
Z-L-PRO-C-(L-VAL-L-PRO)
53
3.2.1.
SYNTHESEERGEBNISSE
53
3.2.2.
CHARAKTERISIERUNG
VOM
CYCLOTRIPEPTID
C-(L-PRO-L-VAL-L-PRO)
55
3.2.3.
STABILITAETSUNTERSUCHUNGEN
AM
CYCLOTRIPEPTID
C-(L-PRO-L-VAL-L-PRO)
68
3.2.4.
CHARAKTERISIERUNG
VOM
CYCLOL
L-PRO-L-VAL-L-PRO
72
3.2.5.
STABILITAETSUNTERSUCHUNGEN
AM
CYCLOL
L-PRO-L-VAL-L-PRO
79
3.2.6.
UMWANDLUNGSVERSUCHE
ZWISCHEN
CYCLOL
UND
CYCLOTRIPEPTID
DER
SEQUENZ
L-PRO-L-VAL-L-PRO
82
3.3.
AMINOACYLEINLAGERUNG
VON
Z-L-PRO-C-(L-VAL-D-PRO)
83
3.3.1.
SYNTHESEERGEBNISSE
83
3.3.2.
CHARAKTERISIERUNG
VOM
CYCLOL
L-PRO-L-VAL-D-PRO
85
3.3.3.
STABILITAETSUNTERSUCHUNGEN
AM
CYCLOL
L-PRO-L-VAL-D-PRO
88
3.4.
AMINOACYLEINLAGERUNG
VON
Z-L-PRO-C-(L-VAL-L-VAL)
90
3.4.1.
SYNTHESEERGEBNISSE
90
3.4.2.
CHARAKTERISIERUNG
VOM
CYCLOL
L-VAL-L-VAL-L-PRO
92
3.4.3.
STABILITAETSUNTERSUCHUNGEN
AM
CYCLOL
L-VAL-L-VAL-L-PRO
99
3.5.
AMINOACYLEINLAGERUNG
VON
Z-D-PRO-C-(GLY-L-PRO)
102
3.5.1.
SYNTHESEERGEBNISSE
102
3.5.2.
CHARAKTERISIERUNG
VOM
CYCLOL
D-PRO-GLY-L-PRO
103
3.5.3.
STABILITAETSUNTERSUCHUNGEN
AM
CYCLOL
D-PRO-GLY-L-PRO
110
-V
3.6.
AMINOACYLEINLAGERUNG
VON
Z-L-PRO-C-(GLY-D-PRO)
113
3.6.1.
SYNTHESEERGEBNISSE
113
3.6.2.
CHARAKTERISIERUNG
VOM
KETENAMINAL
L-PRO-GLY-D-PRO
115
3.7.
AMINOACYLEINLAGERUNG
VON
Z-L-PRO-C-(GLY-L-VAL)
118
3.7.1.
SYNTHESEERGEBNISSE
118
3.7.2.
CHARAKTERISIERUNG
VOM
ACYLAMIDIN
L-VAL-GLY-L-PRO
119
E
EXPERIMENTELLER
TEIL
122
1.
LOESUNGSMITTEL
UND
CHEMIKALIEN
122
1.1.
LOESUNGSMITTEL
122
1.2.
CHEMIKALIEN
123
2.
GERAETE
UND
METHODEN
125
2.1.
GERAETE
125
2.2.
SPEKTROSKOPIE
UND
ANALYTIK
125
2.3.
CHROMATOGRAPHISCHE
METHODEN
126
3.
SYNTHESE
DER
HILFSCHEMIKALIEN
128
3.1.
BENZYLOXYCARBONYLCHLORID
(Z-CHLORID
BZW.
Z-CL)
128
3.2.
N,O-BIS-(TRIMETHYLSILYL)-ACETAMID
(BSA)
129
3.3.
DICYDOHEXYLETHYLAMIN
(DCEA)
130
4.
SYNTHESE
DER
LINEAREN
UND
CYCLISCHEN
PEPTID-VORSTUFEN
131
4.1.
N-BENZYLOXYCARBONYL-AMINOSAEUREN
131
4.1.1.
ALLGEMEINE
ARBEITSVORSCHRIFT
131
4.1.2.
N-BENZYLOXYCARBONYL-GLYCIN
(Z-GLY)
132
4.1.3.
N-BENZYLOXYCARBONYL-L-PROLIN
(Z-L-PRO)
133
4.1.4.
N-BENZYLOXYCARBONYL-D-PROLIN
(Z-D-PRO)
134
4.1.5.
N-BENZYLOXYCARBONYL-L-VALIN
(Z-L-VAL)
135
4.2.
N-BENZYLOXYCARBONYL-AMINOSAEURECHLORIDE
136
4.2.1.
ALLGEMEINE
ARBEITSVORSCHRIFT
136
4.2.2.
N-BENZYLOXYCARBONYL-L-PROLYLCHLORID
(Z-L-PRO-CL)
136
4.2.3.
N-BENZYLOXYCARBONYL-D-PROLYLCHLORID
(Z-D-PRO-CL)
137
4.3.
AMINOSAEUREMETHYLESTER-HYDROCHLORIDE
137
4.3.1.
ALLGEMEINE
ARBEITSVORSCHRIFT
137
4.3.2.
L-PROLINMETHYLESTER-HYDROCHLORID
(L-PRO-OME
X
HCL)
138
-VI
4.3.3.
D-PROLINMETHYLESTER-HYDROCHLORID
(D-PRO-OME
X
HCL)
139
4.3.4.
L-VALINMETHYLESTER-HYDROCHLORID
(L-VAL-OME
X
HCL)
139
4.4.
N-BENZYLOXYCARBONYL-DIPEPTIDMETHYFESTER
140
4.4.1.
ALLGEMEINE
ARBEITSVORSCHRIFT
140
4.4.2.
N
-
BENZYFOXYCARBONYF-GFYCYF-L-PROFINMETHYFESTER
(Z-GLY-L-PRO-OME)
141
4.4.3.
N-BENZYLOXYCARBONYL-GLYCYL-D
-
PROLINMETHYFESTER
(Z-GFY-D-PRO-OME)
142
4.4.4.
N-BENZYFOXYCARBONYF-L-PROFYF-L-VAFINMETHYFESTER
(Z-L-PRO-L-VAF-OME)
143
4.4.5.
N-BENZYFOXYCARBONYF-D-PROFYF-L-VAFINMETHYFESTER
(Z-D-PRO-L-VAF-OME
)
143
4.4.6.
N-BENZYFOXYCARBONYF-GFYCYF-L-VAFINMETHYFESTER
(Z-GFY-L-VAF-OME)
144
4.4.7.
N-BENZYFOXYCARBONYF-L-VAFYF-L-VAFINMETHYFESTER
(Z-L-VAF-L-VAF-OME)
145
4.5.
DIKETOPIPERAZINE
146
4.5.1.
AFFGEMEINE
ARBEITSVORSCHRIFT
146
4.5.2.
CYCFO-(GIYCYI-L-PROFYI)
(C-(GFY-L-PRO))
147
4.5.3.
CYCFO-(GIYCYI-D-PROFYI)
(C-(GFY-D-PRO))
148
4.5.4.
CYCFO-(L-PROFYF-L-VAFYF
)
(C-(L-PRO-L-VAF)
)
149
4.5.5.
CYCFO-(D-PROFYF-L-VAFYF)
(C-(D-PRO-L-VAL)
)
150
4.5.6.
CYCFO-(GFYCYF-L-VAFYF
)
(C-(GFY-L-VAF))
151
4.5.7.
CYCFO-(L-VAIYI-L-VAIYF)
(C-(L-VAF-L-VAF)
).
152
4.6.
N-TRIMETHYISIFYF-DIKETOPIPERAZINE
153
4.6.1.
AFFGEMEINE
ARBEITSVORSCHRIFT
153
4.6.2.
N-TRIMETHYISIIYF-CYCIO-(GIYCYI-L-PROIYI)
(TMS-C-(GFY-L-PRO))
153
4.6.3.
N-TRIMETHYISIIYL-CYCIO-(GLYCYL-D-PROFYI)
(TMS-C-(GFY-I -PROJ)
154
4.6.4.
N-TRIMETHYISIFYI-CYCIO-(L-VAIYL-L-PROIYI)
(TMS-C-(L-VAF-L-PRO)
)
154
4.6.5.
N-TRIMETHYFSIIYI-CYCIO-(L-VAIYI-D-PROIYI)
(TMS-C-(L-VAL-D-PRO))
155
4.7.
N
,
N'-BIS-(TRIMETHYFSILYF)-DIKETOPIPERAZINE
155
4.7.1.
AFFGEMEINE
ARBEITSVORSCHRIFT
155
4.7.2.
N
,
N
'
-BIS-(TRIMETHYFSIFYI
)-CYCIO-(GFYCYI-L-VAFYF
)
((TMS)
2
-C-(GFY-L-VAF))
156
4.7.3.
N
,
N
'
-BIS-(TRIMETHYISIIYI)-CYCFO-(L-VALYF-L-VAFY
1)
((TMS)
2
-C-(L-VAF)
2
)
156
4.8.
N-(BENZYFOXYCARBONYF-AMINOACYL)-DIKETOPIPERAZINE
157
4.8.1.
AFFGEMEINE
ARBEITSVORSCHRIFT
-
VARIANTE
A
157
4.8.2.
AFFGEMEINE
ARBEITSVORSCHRIFT
-
VARIANTE
B
158
4.8.3.
N-(BENZYIOXYCARBONYF-D-PROIYI)-CYCIO-(GIYCYI-L-PROIYI)
(Z-D-PRO-C-(GFY-L-PRO)
)
158
-VII
4.8.4.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(GLYCYL-D-PROLYL)
(Z-L-PRO-C-(GLY-D-PRO)
)
159
4.8.5.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(LVALYL~L-PROLYL)
(Z-L-PRO-C-(L-VAL-L-PRO)
)
160
4.8.6.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO~(L-VALYL~D-PROLYL)
(Z-L-PRO-C-(L-VAL-D-PRO
))
161
4.8.7.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(GLYCYL-L-VALYL)
(Z-L-PRO-C-(GLY-L-VAL)
)
162
4.8.8.
N-(BENZYLOXYCARBONYL-L-PROLYL)-CYDO-(L-VALYL-L-VALYL)
(Z-L-PRO-C-(L-VAL-L-VAL)
)
163
4.9.
N,N'-BIS-(BENZYLOXYCARBONYL-L-PROLYL)-CYCLO-(L-VALYL-L-VALYL)
(
(Z-L-PRO
)
2
-C
(
L-VAL
)
2
)
165
5.
AMINOACYLEINLAGERUNGEN
166
5.1.
ALLGEMEINE
ARBEITSVORSCHRIFT
166
5.2.
CYCLOTRIPEPTID
C-(L-PRO-L-VAL-L-PRO)
167
5.3.
CYCLOL
L-PRO-L-VAL-L-PRO
168
5.4.
CYCLOL
L-PRO-L-VAL-D-PRO
169
5.5.
CYCLOL
L-VAL-L-VAL-L-PRO
170
5.6.
CYCLOL
D-PRO-GLY-L-PRO
172
5.7.
KETENAMINAL
L-PRO-GLY-D-PRO
173
5.8.
ACYLAMIDIN
L-VAL-GLY-L-PRO
174
6.
RACEMISIERUNGSTESTS
175
LITERATURVERZEICHNIS
176 |
| any_adam_object | 1 |
| author | Hiebl, Wilfried |
| author_facet | Hiebl, Wilfried |
| author_role | aut |
| author_sort | Hiebl, Wilfried |
| author_variant | w h wh |
| building | Verbundindex |
| bvnumber | BV010689047 |
| ctrlnum | (OCoLC)258332119 (DE-599)BVBBV010689047 |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV010689047 |
| illustrated | Illustrated |
| indexdate | 2024-08-19T00:32:29Z |
| institution | BVB |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007135158 |
| oclc_num | 258332119 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-29T DE-355 DE-BY-UBR DE-11 DE-188 |
| owner_facet | DE-91 DE-BY-TUM DE-29T DE-355 DE-BY-UBR DE-11 DE-188 |
| physical | VII, 181 S. graph. Darst. |
| publishDate | 1995 |
| publishDateSearch | 1995 |
| publishDateSort | 1995 |
| record_format | marc |
| spelling | Hiebl, Wilfried Verfasser aut Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen Wilfried Hiebl 1995 VII, 181 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Ulm, Univ., Diss., 1995 Cyclole (DE-588)4433831-4 gnd rswk-swf Chemische Synthese (DE-588)4133806-6 gnd rswk-swf Cyclopeptide (DE-588)4148612-2 gnd rswk-swf Tripeptide (DE-588)4186193-0 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Tripeptide (DE-588)4186193-0 s Cyclopeptide (DE-588)4148612-2 s Chemische Synthese (DE-588)4133806-6 s DE-604 Cyclole (DE-588)4433831-4 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007135158&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hiebl, Wilfried Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen Cyclole (DE-588)4433831-4 gnd Chemische Synthese (DE-588)4133806-6 gnd Cyclopeptide (DE-588)4148612-2 gnd Tripeptide (DE-588)4186193-0 gnd |
| subject_GND | (DE-588)4433831-4 (DE-588)4133806-6 (DE-588)4148612-2 (DE-588)4186193-0 (DE-588)4113937-9 |
| title | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen |
| title_auth | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen |
| title_exact_search | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen |
| title_full | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen Wilfried Hiebl |
| title_fullStr | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen Wilfried Hiebl |
| title_full_unstemmed | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine Synthese, Strukturaufklärung und Stabilitätsuntersuchungen Wilfried Hiebl |
| title_short | Cyclole, Cyclotripeptide, Ketenaminale, Acylamidine |
| title_sort | cyclole cyclotripeptide ketenaminale acylamidine synthese strukturaufklarung und stabilitatsuntersuchungen |
| title_sub | Synthese, Strukturaufklärung und Stabilitätsuntersuchungen |
| topic | Cyclole (DE-588)4433831-4 gnd Chemische Synthese (DE-588)4133806-6 gnd Cyclopeptide (DE-588)4148612-2 gnd Tripeptide (DE-588)4186193-0 gnd |
| topic_facet | Cyclole Chemische Synthese Cyclopeptide Tripeptide Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007135158&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hieblwilfried cyclolecyclotripeptideketenaminaleacylamidinesynthesestrukturaufklarungundstabilitatsuntersuchungen |