100 and more basic NMR experiments: a practical course
Gespeichert in:
| Späterer Titel: | Berger, Stefan 200 and more NMR experiments |
|---|---|
| Hauptverfasser: | , , |
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
Weinheim [u.a.]
VCH
1996
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 2. Aufl. u.d.T.: Braun, Siegmar: 150 and more basic NMR experiments |
| Beschreibung: | XII, 418 S. zahlr. graph. Darst. |
| ISBN: | 3527290915 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV010511110 | ||
| 003 | DE-604 | ||
| 005 | 20131017 | ||
| 007 | t | ||
| 008 | 951127s1996 gw d||| |||| 00||| ger d | ||
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| 100 | 1 | |a Braun, Siegmar |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a 100 and more basic NMR experiments |b a practical course |c S. Braun ; H.-O Kalinowski ; S. Berger |
| 246 | 1 | 3 | |a Hundred and more basic NMR experiments |
| 264 | 1 | |a Weinheim [u.a.] |b VCH |c 1996 | |
| 300 | |a XII, 418 S. |b zahlr. graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a 2. Aufl. u.d.T.: Braun, Siegmar: 150 and more basic NMR experiments | ||
| 650 | 0 | 7 | |a Experiment |0 (DE-588)4015999-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Magnetische Kernresonanz |0 (DE-588)4037005-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Praktikum |0 (DE-588)4127380-1 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Magnetische Kernresonanz |0 (DE-588)4037005-7 |D s |
| 689 | 0 | 1 | |a Praktikum |0 (DE-588)4127380-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |D s |
| 689 | 1 | 1 | |a Praktikum |0 (DE-588)4127380-1 |D s |
| 689 | 1 | |5 DE-604 | |
| 689 | 2 | 0 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |D s |
| 689 | 2 | 1 | |a Experiment |0 (DE-588)4015999-1 |D s |
| 689 | 2 | |5 DE-604 | |
| 700 | 1 | |a Kalinowski, Hans-Otto |e Verfasser |4 aut | |
| 700 | 1 | |a Berger, Stefan |d 1946-2023 |e Verfasser |0 (DE-588)124698107 |4 aut | |
| 785 | 0 | 0 | |i Spätere Ausg. u.d.T. |a Berger, Stefan |t 200 and more NMR experiments |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007006340&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-007006340 | |
Datensatz im Suchindex
| _version_ | 1807230000128065536 |
|---|---|
| adam_text |
IX
CONTENTS
PREFACE
CHAPTER
1
THE
NMR
SPECTROMETER
1
1.1
PRINCIPLES
OF
AN
NMR
SPECTROMETER
1
1.1.1
THE
MAGNET
1
1.1.2
THE
SPECTROMETER
CONSOLE
2
1.1.3
THE
WORK-STATION
3
1.1.4
MAINTENANCE
3
1.2
TUNINGAPROBE-HEAD
3
1.2.1
TUNING
AND
MATCHING
WITH
A
REFLECTION
METER
3
1.2.2
TUNING
AND
MATCHING
WITH
AN
R.F.
BRIDGE
AND
AN
OSCILLOSCOPE
4
1.2.3
TUNING
AND
MATCHING
WITH
A
WOBBLE
GENERATOR
5
1.3
THE
LOCK
CHANNEL
6
1.4
THE
ART
OF
SHIMMING
7
1.4.1
THE
SHIM
GRADIENTS
8
1.4.2
THE
SHIMMING
PROCEDURE
9
CHAPTER
2
DETERMINATION
OF
THE
PULSE-LENGTH
13
EXP.
2.1:
DETERMINATION
OF
THE
90
TRANSMITTER
PULSE-LENGTH
14
EXP.
2.2:
DETERMINATION
OF
THE
90
1
3
C
TRANSMITTER
PULSE-LENGTH
17
EXP.
2.3:
DETERMINATION
OF
THE
90
1R
DECOUPLER
PULSE-LENGTH
20
EXP.
2.4:
THE
90
1H
PULSE
WITH
INVERSE
SPECTROMETER
CONFIGURATION
23
EXP.
2.5:
THE
90
^
3
C
DECOUPLER
PULSE
WITH
INVERSE
CONFIGURATION
26
EXP.
2.6:
DETERMINATION
OF
RADIOFREQUENCY
POWER
29
CHAPTER
3
ROUTINE
NMR
SPECTROSCOPY
AND
STANDARD
TESTS
33
EXP.
3.1:
THE
STANDARD
NMR
EXPERIMENT
34
EXP.
3.2:
THE
STANDARD
1
3
C
NMR
EXPERIMENT
39
EXP.
3.3:
LINE-SHAPE
TEST
FOR
NMR
SPECTROSCOPY
44
EXP.
3.4:
RESOLUTION
TEST
FOR
NMR
SPECTROSCOPY
47
EXP.
3.5:
SENSITIVITY
TEST
FOR
NMR
SPECTROSCOPY
50
EXP.
3.6:
LINE-SHAPE
TEST
FOR
1$C
NMR
SPECTROSCOPY
53
EXP.
3.7:
ASTM
SENSITIVITY
TEST
FOR
^
3
C
NMR
SPECTROSCOPY
56
EXP.
3.8:
SENSITIVITY
TEST
FOR
1
3
C
NMR
SPECTROSCOPY
59
EXP.
3.9:
QUADRATURE
IMAGE
TEST
62
EXP.
3.10:
DYNAMIC
RANGE
TEST
FOR
SIGNAL
AMPLITUDES
65
CHAPTER
4
DECOUPLING
TECHNIQUES
68
EXP.
4.1:
DECOUPLER
CALIBRATION
FOR
HOMONUCLEAR
DECOUPLING
69
EXP.
4.2:
DECOUPLER
CALIBRATION
FOR
HETERONUCLEAR
DECOUPLING
72
EXP.
4.3:
LOW
POWER
CALIBRATION
FOR
HETERONUCLEAR
DECOUPLING
75
X
EXP.
4.4:
HOMONUCLEAR
DECOUPLING
78
EXP.
4.5:
THE
HOMONUCLEAR
SPT
EXPERIMENT
81
EXP.
4.6:
THE
HETERONUCLEAR
SPT
EXPERIMENT
84
EXP.
4.7:
ID
NUCLEAR
OVERHAUSER
DIFFERENCE
SPECTROSCOPY
87
EXP.
4.8:
ID
NOE
SPECTROSCOPY
WITH
MULTIPLE
SELECTIVE
IRRADIATION
90
EXP.
4.9:
1H
OFF-RESONANCE
DECOUPLED
1$C
NMR
SPECTRA
93
EXP.
4.10:
THE
GATED
^H-DECOUPLING
TECHNIQUE
96
EXP.
4.11:
THE
INVERSE
GATED
^H-DECOUPLING
TECHNIQUE
99
EXP.
4.12:
I
R
SINGLE
FREQUENCY
DECOUPLING
OF
L^C
NMR
SPECTRA
1H
LOW-POWER
DECOUPLING
OF
I
'
C
NMR
SPECTRA
102
EXP.
4.13:
105
EXP.
4.14:
MEASUREMENT
OF
THE
HETERONUCLEAR
OVERHAUSER
EFFECT
108
CHAPTER
5
DYNAMIC
NMR
SPECTROSCOPY
111
EXP.
5.1:
LOW
TEMPERATURE
CALIBRATION
WITH
METHANOL
112
EXP.
5.2:
HIGH
TEMPERATURE
CALIBRATION
WITH
1,2-ETHANEDIOL
DYNAMIC
1H
NMR
SPECTROSCOPY
ON
DIMETHYLFORMAMIDE
115
EXP.
5.3:
118
EXP.
5.4:
THE
SATURATION
TRANSFER
EXPERIMENT
121
CHAPTER
6
ID
MULTIPULSE
SEQUENCES
124
EXP.
6.1:
MEASUREMENT
OF
THE
SPIN-LATTICE
RELAXATION
TIME
125
EXP.
6.2:
MEASUREMENT
OF
THE
SPIN-SPIN
RELAXATION
TIME
?2
129
EXP.
6.3:
EDITING
L^C
NMR
SPECTRA
WITH
SEFT
132
EXP.
6.4:
EDITING
1$C
NMR
SPECTRA
WITH
APT
135
EXP.
6.5:
THE
BASIC
INEPT
TECHNIQUE
138
EXP.
6.6:
INEPT+
141
EXP.
6.7:
REFOCUSED
INEPT
144
EXP.
6.8:
REVERSE
INEPT
147
EXP.
6.9:
EDITING
L^C
NMR
SPECTRA
WITH
DEPT
150
EXP.
6.10:
EDITING
L^C
NMR
SPECTRA
WITH
PENDANT
154
EXP.
6.11:
ID-INADEQUATE
157
EXP.
6.12:
THE
BIRD
FILTER
161
EXP.
6.13:
TANGO
164
EXP.
6.14:
THE
HETERONUCLEAR
DOUBLE
QUANTUM
FILTER
167
EXP.
6.15:
WATER
SUPPRESSION
BY
PRESATURATION
170
EXP.
6.16:
WATER
SUPPRESSION
BY
DIE
JUMP
AND
RETURN
METHOD
173
CHAPTER
7
NMR
SPECTROSCOPY
WITH
SELECTIVE
PULSES
176
EXP.
7.1:
DETERMINATION
OF
A
SHAPED
90
1H
TRANSMITTER
PULSE
177
EXP.
7.2:
DETERMINATION
OF
A
SHAPED
90
^H
DECOUPLER
PULSE
180
EXP.
7.3:
DETERMINATION
OF
A
SHAPED
90
1$C
DECOUPLER
PULSE
183
EXP.
7.4:
SELECTIVE
EXCITATION
WITH
DANTE
186
EXP.
7.5:
SELECTIVE
COSY
189
EXP.
7.6:
SELINCOR:
SELECTIVE
INVERSE
H,C
CORRELATION
VIA
V(C,H)
192
EXP.
7.7:
SELINQUATE
195
XI
EXP.
7.8:
SELECTIVE
TOCSY
199
EXP.
7.9:
INAPT
203
EXP.
7.10:
DETERMINATION
OF
LONG
RANGE
C,H
COUPLING
CONSTANTS
206
EXP.
7.11:
SELRESOLV
209
EXP.
7.12:
SERF
212
CHAPTER
8
AUXILIARY
REAGENTS,
QUANTITATIVE
DETERMINATIONS,
215
AND
REACTION
MECHANISM
EXP.
8.1:
SIGNAL
SEPARATION
USING
A
LANTHANIDE
SHIFT
REAGENT
216
EXP.
8.2:
SIGNAL
SEPARATION
OF
ENANTIOMERS
USING
A
CHIRAL
SHIFT
REAGENT
219
EXP.
8.3:
SIGNAL
SEPARATION
OF
ENANTIOMERS
USING
A
CHIRAL
SOLVATING
AGENT
222
EXP.
8.4:
DETERMINATION
OF
ENANTIOMERIC
PURITY
WITH
PIRKLE
'
S
REAGENT
225
EXP.
8.5:
THE
RELAXATION
REAGENT
CR(ACAC)3
228
EXP.
8.6:
QUANTITATIVE
1H
NMR
SPECTROSCOPY:
DETERMINATION
OF
THE
231
ALCOHOL
CONTENT
OF
POLISH
VODKA
EXP.
8.7:
QUANTITATIVE
NMR
SPECTROSCOPY
WITH
INVERSE
GATED
234
1H-DECOUPLING
EXP.
8.8:
DETERMINATION
OF
PARAMAGNETIC
SUSCEPTIBILITY
BY
NMR
237
EXP.
8.9:
THE
CIDNP
EFFECT
240
CHAPTER
9
HETERONUCLEAR
NMR
SPECTROSCOPY
243
EXP.
9.1:
1H-DECOUPLED
I5
N
NMR
SPECTRA
WITH
DEPT
248
EXP.
9.2:
^H-COUPLED
NMR
SPECTRA
WITH
DEPT
251
EXP.
9.3:
NMR
SPECTROSCOPY
254
EXP.
9.4:
29SI
NM
R
SPECTROSCOPY
WITH
DEPT
257
EXP.
9.5:
1
L^SN
NMR
SPECTROSCOPY
261
EXP.
9.6:
2
H
NMR
SPECTROSCOPY
264
EXP.
9.7:
NMR
SPECTROSCOPY
267
EXP.
9.8:
L^O
NMR
SPECTROSCOPY
WITH
RIDE
270
CHAPTER
10
THE
SECOND
DIMENSION
273
EXP.
10.1:
2D
J-RESOLVED
1H
NMR
SPECTROSCOPY
277
EXP.
10.2:
2D
J-RESOLVED
L^C
NMR
SPECTROSCOPY
280
EXP.
10.3:
THE
BASIC
H.H-COSY
EXPERIMENT
283
EXP.
10.4:
LONG-RANGE
COSY
286
EXP.
10.5:
PHASE-SENSITIVE
COSY
289
EXP.
10.6:
PHASE-SENSITIVE
COSY-45
292
EXP.
10.7:
DOUBLE
QUANTUM
FILTERED
COSY
WITH
PRESATURATION
295
EXP.
10.8:
C,H
CORRELATION
BY
POLARIZATION
TRANSFER
(HETCOR)
299
EXP.
10.9:
LONG-RANGE
C,H
CORRELATION
BY
POLARIZATION
TRANSFER
302
EXP.
10.10:
C,H
CORRELATION
VIA
LONG-RANGE
COUPLINGS
(COLOC)
305
EXP.
10.11:
THE
BASIC HMQC
EXPERIMENT
308
EXP.
10.12:
PHASE-SENSITIVE
HMQC
WITH
BIRD
SELECTION
AND
312
GARP
DECOUPLING
XII
EXP.
10.13:
PHASE-SENSITIVE
HMBC
WITH
BIRD
SELECTION
315
EXP.
10.14:
THE
BASIC
HSQC
EXPERIMENT
318
EXP.
10.15:
THE
HOHAHA
OR
TOCSY
EXPERIMENT
322
EXP.
10.16:
THE
NOESY
EXPERIMENT
326
EXP.
10.17:
THE
CAMELSPIN
OR
ROESY
EXPERIMENT
330
EXP.
10.18:
THE
HOESY
EXPERIMENT
334
EXP.
10.19:
2D-INADEQUATE
337
EXP.
10.20:
THE
EXSY
EXPERIMENT
341
CHAPTER
11
NMR
SPECTROSCOPY
WITH
PULSED
FIELD
GRADIENTS
344
EXP.
11.1:
CALIBRATION
OF
PULSED
FIELD
GRADIENTS
346
EXP.
11.2:
THE
PULSED
GRADIENT
SPIN-ECHO
EXPERIMENT
349
EXP.
11.3:
GRADIENT-SELECTED
H,H-COSY
352
EXP.
11.4:
GRADIENT-SELECTED
PHASE-SENSITIVE
DQF
COSY
356
EXP.
11.5:
GRADIENT-SELECTED
HMQC
360
EXP.
11.6:
GRADIENT-SELECTED
HMBC
364
EXP.
11.7:
PHASE-SENSITIVE
GRADIENT-SELECTED
HSQC
368
EXP.
11.8:
GRADIENT-SELECTED
TOCSY
372
EXP.
11.9:
GRADIENT-SELECTED
HMQC-TOCSY
376
EXP.
11.10:
GRADIENT-SELECTED
^H-DETECTED
2D
INEPT-INADEQUATE
380
EXP.
11.11:
GRADIENT-SELECTED
SELINCOR
384
EXP.
11.12:
GRECCO
387
EXP.
11.13:
WATERGATE
390
CHAPTER
12
THE
THIRD
DIMENSION
393
EXP.
12.1:
3DHMQC-COSY
394
EXP.
12.2:
3D
GRADIENT-SELECTED
HSQC-TOCSY
398
EXP.
12.3:
3D
H,C,P-CORRELATION
402
APPENDIX
1
405
INSTRUMENT
DIALECTS
406
APPENDIX
2
409
ELEMENTARY
PRODUCT
OPERATOR
FORMALISM
RULES
409
GLOSSARY
AND
INDEX
411 |
| any_adam_object | 1 |
| author | Braun, Siegmar Kalinowski, Hans-Otto Berger, Stefan 1946-2023 |
| author_GND | (DE-588)124698107 |
| author_facet | Braun, Siegmar Kalinowski, Hans-Otto Berger, Stefan 1946-2023 |
| author_role | aut aut aut |
| author_sort | Braun, Siegmar |
| author_variant | s b sb h o k hok s b sb |
| building | Verbundindex |
| bvnumber | BV010511110 |
| classification_rvk | VG 9500 VG 9501 |
| ctrlnum | (OCoLC)450971128 (DE-599)BVBBV010511110 |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV010511110 |
| illustrated | Illustrated |
| indexdate | 2024-08-13T00:27:08Z |
| institution | BVB |
| isbn | 3527290915 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-007006340 |
| oclc_num | 450971128 |
| open_access_boolean | |
| owner | DE-29T DE-20 DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-83 DE-11 DE-188 |
| owner_facet | DE-29T DE-20 DE-355 DE-BY-UBR DE-19 DE-BY-UBM DE-83 DE-11 DE-188 |
| physical | XII, 418 S. zahlr. graph. Darst. |
| publishDate | 1996 |
| publishDateSearch | 1996 |
| publishDateSort | 1996 |
| publisher | VCH |
| record_format | marc |
| spelling | Braun, Siegmar Verfasser aut 100 and more basic NMR experiments a practical course S. Braun ; H.-O Kalinowski ; S. Berger Hundred and more basic NMR experiments Weinheim [u.a.] VCH 1996 XII, 418 S. zahlr. graph. Darst. txt rdacontent n rdamedia nc rdacarrier 2. Aufl. u.d.T.: Braun, Siegmar: 150 and more basic NMR experiments Experiment (DE-588)4015999-1 gnd rswk-swf Magnetische Kernresonanz (DE-588)4037005-7 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Praktikum (DE-588)4127380-1 gnd rswk-swf Magnetische Kernresonanz (DE-588)4037005-7 s Praktikum (DE-588)4127380-1 s DE-604 NMR-Spektroskopie (DE-588)4075421-2 s Experiment (DE-588)4015999-1 s Kalinowski, Hans-Otto Verfasser aut Berger, Stefan 1946-2023 Verfasser (DE-588)124698107 aut Spätere Ausg. u.d.T. Berger, Stefan 200 and more NMR experiments DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007006340&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Braun, Siegmar Kalinowski, Hans-Otto Berger, Stefan 1946-2023 100 and more basic NMR experiments a practical course Experiment (DE-588)4015999-1 gnd Magnetische Kernresonanz (DE-588)4037005-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Praktikum (DE-588)4127380-1 gnd |
| subject_GND | (DE-588)4015999-1 (DE-588)4037005-7 (DE-588)4075421-2 (DE-588)4127380-1 |
| title | 100 and more basic NMR experiments a practical course |
| title_alt | Hundred and more basic NMR experiments |
| title_auth | 100 and more basic NMR experiments a practical course |
| title_exact_search | 100 and more basic NMR experiments a practical course |
| title_full | 100 and more basic NMR experiments a practical course S. Braun ; H.-O Kalinowski ; S. Berger |
| title_fullStr | 100 and more basic NMR experiments a practical course S. Braun ; H.-O Kalinowski ; S. Berger |
| title_full_unstemmed | 100 and more basic NMR experiments a practical course S. Braun ; H.-O Kalinowski ; S. Berger |
| title_new | Berger, Stefan 200 and more NMR experiments |
| title_short | 100 and more basic NMR experiments |
| title_sort | 100 and more basic nmr experiments a practical course |
| title_sub | a practical course |
| topic | Experiment (DE-588)4015999-1 gnd Magnetische Kernresonanz (DE-588)4037005-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Praktikum (DE-588)4127380-1 gnd |
| topic_facet | Experiment Magnetische Kernresonanz NMR-Spektroskopie Praktikum |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=007006340&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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