Special trends in thermal analysis:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester u.a.
Wiley
1995
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVII, 459 S. Ill., zahlr. graph. Darst. |
| ISBN: | 0471957690 |
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Datensatz im Suchindex
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| adam_text | SPECIAL TRENDS IN THERMAL ANALYSIS FERENC PAULIK JOHN WILEY& SONS
CHICHESTER * NEW YORK * BRISBANE * TORONTO * SINGAPORE CONTENTS PREFACE
XV ACKNOWLEDGEMENTS XVI COMMEMORATION XVII PART I: SIMULTANEOUS
THERMOANALYTICAL EXAMINATIONS UNDER CONVENTIONAL CONDITIONS 1
1.IIMTRODUCTION 3 1.1. BACKGROUND OFTHE ELABORATION OF DERIVATIVE AND
SIMULTANEOUS METHODS 3 1.2. MULTIPLICATION OF INFORMATION BY THE USE OF
SIMULTANEOUS METHODS 3 1.3. RESOLUTION OF THERMOANALYTICAL CURVES 5 2.
DERIVATIVE THERMOGRAVIMETRY (DTG) 6 2.1. THE DERIVING THERMOBALANCE 6
2.2. EFFECTS OFTHE EXPERIMENTAL CONDITIONS ON THE COURSE OF THERMO-
ANALYTICAL CURVES 8 3. SIMULTANEOUS DTA, TG AND DTG 10 3.1. THE
DERIVATOGRAPH, AN APPARATUSFOR SIMULTANEOUS TG, DTG AND DTA.W 3.2.
INTERPRETATION AND EVALUATION OF SIMULTANEOUSLY RECORDED CURVES 11 3.3.
RELIABILITY OFTHE DETECTION AND THE ACCURACY OFTHE DETERMINATION IN THE
CASE OF OVERLAPPING REACTIONS 13 3.4. PRACTICA! EXAMPLES 16 A) SODIUM
METAPHOSPHATE (NAPOI) 16 B) URANIUM TRIOXIDE (UO3) 17 C) EFFECT
OFGRINDING ON THE STRUCTURE AND COMPOSITION OFKAOLINITE 18 D) COBALT
TETRAMETHYLPYRAZINE THIOCYANATE [CO(MP)4NCS) 2 ] 19 E) CRHEDTA(HLO) AND
[CRHPDTA(HJ))]H& 20 F) POTASSIUM AND COBALTAMMINE CYANOMETALLATE
COMPLEXES 22 G) RANEY NICKEL 24 H) POLYETHYLENE 24 I) MINERAL COALS 25
J) HYDRATION OFCEMENTS, SOLIDIFICATION OFCONCRETE 26 VM 4. DERIVATIVE
DIIATOMETRY (DTD) 28 4.1. METHODFOR SIMULTANEOUS TD, DTD AND DTA 29 4.2.
METHODFOR SIMULTANEOUS TD, DTD, TG, DTG AND DTA MEASUREMENTS 31 4.3.
PRACTICA! EXAMPLES 32 AJKAOLINITE 33 B) BARIUM CHLORIDE DIHYDRATE
(BACH2HJO) 34 C) AMMONIUM NILRATE (NH4NO1) 34 D) CALCIUM SULPHATE
DIHYDRATE (CAS0T2H&) 35 E) GIBBSITE 36 F) CALCIUM OXALATE MONOHYDRATE
(CACJOFHIO) 38 G) CLAYMINERALS 39 5. SELECTIVITY OF THE MEASUREMENTS 40
5.1. MEANS OF INCREASING THE SELECTIVITY 40 5.2. MULTIPLATE SAMPLE
HOLDER 41 5.3. LABYRINTH CRUCIBLE 44 5.4. KINETICS OF OVERLAPPING
REACTIONS IN DIFFERENT SAMPLE HOLDERS 46 5.5. ATTAINMENT OFACTIVE AND
INERT GAS ATMOSPHERES 51 5.6. PRACTICA! EXAMPLES 54 A) SODIUM
HYDROGENSULPHATE MONOHYDRATE (NAHSOFHJO) 54 B) BORIC ACID (H3BO3) 54 C)
CALCIUM LACTATE PENTAHYDRATE 55 D) POLYETHYLENE 56 E) PYRITE (FES^ 58 F)
COPPER SULPHATE PENTAHYDRATE (CUSOF5HJO) 59 6.THERMO-GASTITRIMETRY(TGT)
61 6.1. GENERAL ASPECTS OFTHE USE OF SIMULTANEOUS TGT, DTGT, TG, DTG AND
DTA 61 6.2. STRUCTURE AND OPERATION OFTHE DERIVATOGRAPH APPROPRIATE FOR
SIMULTANEOUS TGT, DTGT, TG, DTG AND DTA STUDIES 63 6.3. TGT STUDIES TO
INCREASE THE RELIABILITY OFDETECTION 71 6.4. ACCURACY OF TGT STUDIES 74
6.5. PRACTICAL EXAMPLES 74 A) ZINC AMMONIUM PHOSPHATE SSNNH^O^ 74 IX B)
BARIUM OXALATE HEMIHYDRATE (BACJOTO.SHJO) 75 C)SIDERITE 77 D)
TETRAMMINEPLATINUM(II) CHLORIDE MONOHYDRATE (PT(NH3)HH ) 79 E) BAUXITE
81 FTMANGANESE CARBONATE HYDRATE SSDNCORXHJO) 83 H) REACTIONS OFNAP0 3
WITH NACL 84 I) BASIC IRON(III) ACETATE 85 7. A CONTINUOUS AND SELECTIVE
WATER DETECTOR 86 7.1. THE INSTRUMENT AND ITS OPERATION 86 7.2.
PRACTICAL EXAMPLES 88 7.2.1. ION-EXCHANGE RESINS 88 7.2.2. ION-EXCHANGED
Y-ZEOLITE CATALYST 88 7.2.3. TRANSITION METAL COMPLEXES 88 7.2.4.
INTERCALATEDKAOLINITES 91 8. EVOLVED GAS ANALYSIS BY MEANS OF A Q-MS
COUPLED WITH A DERIVATOGRAPH 92 8.1. STRUCTURE AND OPERATION OFTHE
COUPLED INSTRUMENT 92 8.2. PRACTICAL EXAMPLES 92 A) CROSS-LINKED
DEXTRAN POLYMER 94 B) SPORADIC BONE FLNDS 95 9. DETERMINATION OF
IGNITION TEMPERATURE WITH A MODIFIED DERIVATOGRAPH 96 9.1. THE UNIT AND
ITS OPERATION 97 9.2. PRACTICAL EXAMPLES 98 9.2.1. POLYETHYLENE (PE)
ANDFLAME-RETARDEDPE 98 9.2.2. CELLULOSE-TYPE MATERIALS 99 PART 11:
KINETICS AND MECHANISM OF THERMAL REACTIONS 101 10. KINETICS AND
MECHANISM 103 10.1. THERMAL DECOMPOSUION OF SOLID INORGANIC COMPOUNDS
LEADING TO EQUILIBRIUM 103 10.2. DEHYDRATION OF SAH HYDRATES 116 10.3.
DEHYDRATION-DEHYDROXYLATION WITH SPECIAL REGARD TO MINER ALS 127 { X A)
OCCLUDED WATER 12 7 B) WATER BOUND IN A SOLID SOLUTION 128 C) WATER
BOUND BY ADSORPTION 129 D) WATER BOUND BY CAPILLARY CONDENSATION 129 E)
WATER BOUND BY CHEMISORPTION 130 F) WATER OF CRYSTALLIZATION 130 G)
DEHYDRATION OF ACID SALTS 131 H) INTERLAYER WATER 131 I) ZEOLITIC WATER
132 J) GEL WATER 133 K) DEHYDROXYLATION 136 10.4. EXOTHERNUEC
NON-EQUILIBRIUM REACTIONS TAKINGPLACE BETWEEN SOLID PHASES 140 10.5.
EXOTHERNUEC SOLID-PHASE NON-EQUILIBRIUM REACTIONS WITH THE ACTIVE
PARTICIPATION OFGASES 148 10.6. EXOTHERNUEC NON-EQUILIBRIUM SOLID-PHASE
REACTIONS WITH THE ACTIVE PARTICIPATION OF A LIQUID PHASE 151 10.7.
PHASE CHANGES LEADING TO EQUILIBRIUM IN MULTICOMPONENT SYSTEMS. .155
10.8. AUTOCATALYTIC DECOMPOSITION REACTIONS 158 10.9. EFFECTS OFCHANGE
OFMODIFICATION ANDPHYSICAL STATE, OFRECRYSTALLIZATION ANDSINTERING ON
THE COURSE OF REACTIONS 161 10.10. CALCULATION OFREACTION
KINETICPARAMETERS 16 8 PART UI: THERMOANALYTICAL STUDIES UNDER
QUASI-ISOTHERMAL, QUASI-ISOBARIC CONDITIONS 175 11. NORMALIZATION AND
STANDARDIZATION OF THE EXPERIMENTAL CONDITIONS 177 12. THERMOGRAVIMETRY
UNDER QUASI-ISOTHERMAL, QUASI-ISOBARIC CONDITIONS (Q-TG) 177 12.1.
APPARATUSFOR Q-TG EXAMINATIONS 177 12.2. INTERPRETATION OF Q-TG CURVES
181 12.2.1. GENERAL FEATURES OF Q-TG CURVES 181 12.2.2. CLASSIFICATION
OFPROCESSES ACCORDING TO THE COURSE OFTHE Q-TG CURVES 182 12.2.3. BASIC
TRANSFORMATIONS WITH A QUASI-ISOTHERMAL COURSE 186 XI 12.2.4. BASIC
TRANSFORMATIONS WITH ANON-ISOTHERMAL COURSE 187 12.2.5. COURSES OFTHE
Q-TG CURVES OFREACTIONS INVOLVINGSMALL AND LARGE MASS CHANGES 187 12.3.
BISTORTION OFQ-TG CURVES BY RECRYSTALTIZATION AND SINTERING 189 12.3.1.
DEHYDROXYLATION OFMG(OH) 2 189 12.3.2. EFFECT OF WATER VAPOUR
ATMOSPHERE ON THE RECRYSTALLIZATION OFMNNHTFOTHLO 190 12.3.3. EFFECT OFA
WATER VAPOUR ATMOSPHERE ON RECRYSTALLIZATION AND SINTERING PROCESSES IN
THE CASE OFCASOE4-2HIO 19 3 12.4. RETARDED FORMATION ANDGROWTH OFNUCLEI
193 12.4.1. SPONTANEOUSLY RETARDEDNUCLEATION 194 12.4.2.
NUCLEATION-RETARDINGEFFECT OFGASEOUS DECOMPOSITION PRODUCTS 195 12.5.
ACCELERATORY AND DECELERATORY (PROMOTING OR DELAYING) EFFECTS OFFOREIGN
GASES AND SOLID SURFACE CONTAMINANTS ON DECOMPOSITION REACTIONS 196
12.6. TRANSFORMATIONS INVOLVING SEVERAL CONSECUTIVE REACTIONS 197
12.6.1. DEHYDRATION OFINORGANIC GEH 197 12.6.2. IRREGULAER THERMAL
BEHAVIOUR OFWATER-CONTAINING MINER ALS ANDROCKS 198 12.7. Q-TG CURVES OF
SPECIAL SHAPE 200 12.7.1. COMPETITIVEREACTIONS 200 12.7.2. ROLE
OFHIGH-ACTIVITY SITES IN THE EXTRAORDINARY COURSE OFTHE DECOMPOSITION
OFMETAL SULPHIDES 202 12.8. EFFECTS OFCHANGES IN THE EXPERIMENTAL
CONDITIONS ON THE MECHANISM OFREACTIONS 203 12.8.1. ZNEDTA CHELATE 203
12.8.2. SECONDARY REACTIONS OF SOLID AND GASEOUS DECOMPOSITION PRODUCTS
205 12.8.3. RESULTANT Q-TG CURVEFOR OVERLAPPING REACTIONS 206 12.8.4.
CONDITIONS OFPREPARATION OF CYCLO-CUMGP4012 20 8 12.9. DEHYDRATION OF
SAH HYDRATES 210 12.9.1. EVOLUTION OF WATER DURING THE QUASI-ISOTHERMAL
BOILING OF A SATURATED SOLUTION 211 12.9.2. EVOLUTION OF WATER VAPOUR
DURING THE NON-ISOTHERMAL BOILING OFAN UNSATURATED SOLUTION 212 XU
12.9.3. CRUST FORMATTON ON THE SURFACE OFWATER-SOLUBLE SALT SYSTEMS 215
12.9.4. ROLE OFMETASTDBLE INTERMEDIATES IN THE FORMATION AND
DECOMPOSITION OFSALT HYDRATES , 217 12.10. APPLICATION OFTHE Q-TG
TECHNIQUE TO SUPPLEMENT OR REVISEPHASE DIAGRAM DATA 219 12.10.1.
SUPPLEMENTATION ANDREVISION OFPHASE DIAGRAM DATA THROUGH THE USE OF Q-TG
CURVES 220 12.10.2. APPLICATION OFTHE Q-TG TECHNIQUE FOR THE PREPARATION
OFA SALT-WATER SYSTEM OFDEFLNED COMPOSITION 222 13. SIMULTANEOUS Q-TG
AND Q-TGT STUDIES 222 13.1. THE INSTRUMENT AND ITS OPERATION 222 13.2.
APRACTICA! EXAMPLE 223 14. QUASI-ISOTHERMAL DIIATOMETRY (Q-TD) 225 14.1.
STRUCTURE ANDFUNCTION OFTHE DEVICE 225 14.2. PRACTICAL EXAMPLES 226 15.
QUASI-ISOTHERMAL DTA METHOD (Q-DTA) 230 15.1. PRINCIPLE OFTHE METHOD,
CONSTRUCTION AND OPERATION OFTHE INSTRUMENT 230 15.2. ADVANTAGES OFTHE
TECHNIQUE 234 15.3. FIELDS OFAPPLICATION OFTHE TECHNIQUE 234 15.3.1.
ENDOTHERMIC PHASE TRANSFORMATIONS LEADING TO EQUILIBRIUM 235 15.3.2.
EXOTHERMIC SOLID-PHASE REACTIONS ANDSTRUCTURAL TRANSFORMATIONS 235
15.3.3. ENDOTHERMIC DECOMPOSITION OF SOLID COMPOUNDS, LEADING TO
EQUILIBRIUM ANDINVOLVING A CHANGE IN MASS 238 16. Q-TG METHOD FOR THE
MICRODISTILLATION OFLIQUIDS 240 16.1. PRINCIPLE ANDCOURSE OFTHE
EXPERIMENT 240 16.2. MODEL EXPERIMENTS 245 17. DESORPTION OF THE VAPOUR
OF A LIQUID FROM A SOLID SURFACE (Q-TG!,,.) 245 17.1. FIELDS OF
APPLICATION OFTHE METHOD 246 17.2. PRACTICAL EXAMPLES 246 XIII 18.
THERMOMAGNETIC MEASUREMENTS (TMM) USING NON-ISOTHERMALAND
QUASI-ISOTHERMAL HEATING TECHNIQUE 247 18.1. INSTRUMENT AND METHOD 248
REFERENCES 250 LIST OF PUBLICATIONS 253 SUBJECT INDEX 397
|
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| indexdate | 2024-07-09T17:52:40Z |
| institution | BVB |
| isbn | 0471957690 |
| language | English |
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| spelling | Paulik, Ferenc Verfasser aut Special trends in thermal analysis Ferenc Paulik Chichester u.a. Wiley 1995 XVII, 459 S. Ill., zahlr. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Analyse thermique ram Thermogravimétrie ram Thermal analysis Thermoanalyse (DE-588)4135675-5 gnd rswk-swf Thermoanalyse (DE-588)4135675-5 s DE-604 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006961281&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Paulik, Ferenc Special trends in thermal analysis Analyse thermique ram Thermogravimétrie ram Thermal analysis Thermoanalyse (DE-588)4135675-5 gnd |
| subject_GND | (DE-588)4135675-5 |
| title | Special trends in thermal analysis |
| title_auth | Special trends in thermal analysis |
| title_exact_search | Special trends in thermal analysis |
| title_full | Special trends in thermal analysis Ferenc Paulik |
| title_fullStr | Special trends in thermal analysis Ferenc Paulik |
| title_full_unstemmed | Special trends in thermal analysis Ferenc Paulik |
| title_short | Special trends in thermal analysis |
| title_sort | special trends in thermal analysis |
| topic | Analyse thermique ram Thermogravimétrie ram Thermal analysis Thermoanalyse (DE-588)4135675-5 gnd |
| topic_facet | Analyse thermique Thermogravimétrie Thermal analysis Thermoanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006961281&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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