Verfügbarkeit: Quantitative methods in soil mineralogy

Quantitative methods in soil mineralogy: proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990

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Format:	Buch
Sprache:	Undetermined
Veröffentlicht:	Madison, Wis. SSSA 1994
Schriftenreihe:	SSSA miscellaneous publication
Schlagworte:	Bodenanalyse Mineralboden Konferenzschrift > 1990 > San Antonio Tex.
Online-Zugang:	Inhaltsverzeichnis
Beschreibung:	XXI, 462 S. graph. Darst.
ISBN:	0891188061

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Datensatz im Suchindex

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adam_text	CONTENTS Foreword ................................................ xi Preface .................................................. xiii Contributors .............................................. xv Conversion Factors for SI and non-SI Units .......................... xvii 1 Nondestructive Techniques for Bulk Elemental Analysis J.E. Amonette and R. W. Sanders ............................ 1 Spectroscopic Fundamentals ................................... 2 Physics ............................................. 2 Х -Ray Production ....................................... 3 Absolute Yield Equations .................................. 9 Excitation Sources ...................................... 11 Detection ............................................ 14 Specimen Preparation .................................... 19 Survey of Analytical Techniques ................................ 20 Х -Ray Fluorescence ..................................... 20 Particle-Induced Х -Ray Emission ............................. 24 Particle-Induced Gamma Emission ............................ 27 Synchrotron-Radiation-Induced Х -Ray Emission .................... 31 Comparisons Among the Analytical Techniques ....................... 32 Theoretical Comparisons ................................... 32 Experimental Comparison of Х -Ray Fluorescence and Particle-Induced Х -Ray Emission Results ...................... 37 Economic and Logistical Comparisons .......................... 42 Future Developments .........................*..........· ■ · · 43 Summary .............................................. 44 2 Dissolution and Elemental Analysis of Minerals, Soils, and Environmental Samples B. L. Sawhney and D. E. Stilwell............................. 49 Decomposition and Dissolution ................................. 49 Fusion with Alkali Salts ................................... 49 Digestion with Acids ..................................... 51 Microwave Dissolution ................................... 52 Separation and Preconcentration of Trace Elements .................... 53 Standard Solutions and Reference Materials ......................... 54 Environmental Samples and Soil Extracts ........................... 55 Environmental Samples ................................... 55 Soil Extracts .......................................... 55 Atomic Spectroscopy ....................................... 55 Basic Principles ........................................ 56 Temperature Effects ..................................... 58 The Atomization Process .................................. 58 Analytical Performance in Atomic Spectroscopy .................... 61 Atomic-Absorption Spectrometry ................................ 66 Instrumentation ......................................... 67 Background Correction ................................... 70 Inductively Coupled Plasma-Atomic Emission Spectrometry ............... 73 Instrumentation ......................................... 73 Inductively Coupled Plasma-Mass Spectrometry .................... 75 Summary and Conclusion ..................................... 77 vi CONTENTS 3 Quantitative Oxidation-State Analysis of Soils J. E. Amonette, F. A. Khan, H. Gan, J. W. Stucki, and A. D. Scott ....... 83 General Principles ......................................... 84 Sampling ............................................ 84 Standards ............................................ 84 Analytical Tecbniques .................................... 85 Specific Chemical Methods ................................... 90 Iron(II) and Iron(III) ..................................... 90 ManganeseCII), Manganese(III), and Manganese(IV) .................. 96 ChromiumOII) and ChromiumCVI) ............................ 97 Nonspecific Measurements ................................. 98 Experimental Comparison .................................... 98 Materials and Methods .................................... 98 Results and Discussion .................................... 100 Future Developments ....................................... 107 Summary .............................................. 108 4 Structural Formulae of Layer Silicates B. Číčel and P. Komadel .................................. 114 Structural Formulae from Bulk Chemical Analyses ..................... 115 Method I ............................................ 116 Method II ........................................... 118 Effect of Free Oxides .................................... 118 Effect of Layer Silicates ................................... 119 Evaluation of Bulk Chemical Methods ........................... 119 Structural Formulae Derived from Acid Dissolution .................... 121 Advantages and Limitations of Acid Dissolution Technique ............. 122 Infrared Identification of Octahedral Cations ......................... 124 Advantages and Limitations of the Infrared Method .................. 125 Determination of Tetrahedral Aluminum by Magic-Angle Spinning- Nuclear Magnetic Resonance Spectroscopy ....................... 125 Advantages and Limitations of Magic-Angle Spinning-Nuclear Magnetic Resonance Spectroscopy .......................... 129 Distribution of Iron from Iron-57 Mössbauer Spectroscopy ................ 129 Advantages and Limitations of Mössbauer Spectroscopy ............... 130 Future Developments ....................................... 130 Summary .............................................. 130 Appendix .............................................. 133 Definitions of Symbols and Values ............................. I33 Calculations of Structural Formulae of Layer Silicates ................ I34 5 Light Microscopic Techniques in Quantitative Soil Mineralogy L. R. Drees and M. D. Ransom ....................... 137 Historical Developments .............................. ,30 Analysis and Preparation .................................. 138 Measurement Techniques ....................... ...... ,,„ Optical Methods of Quantification ............................... 143 Quantification Considerations ................... ........ 14o Grain Mounts ................... Thin Sections ........ .............................. ).„ ................................. 148 CONTENTS vu Computer-Assisted Image Analysis............................... 157 Pattern Recognition ...................................... 158 Types of Image Analyzers ................................. 159 Problems in Mineral Identification ............................ 161 Applications of Image Analysis .............................. 162 Future Trends ........................................... 168 Fluorescence Microscopy .................................. 168 Computer-Assisted Image Analysis ............................ 169 Mathematical Concepts .................................... 169 New Microscopic Techniques ............................... 170 Conclusions ............................................. 171 6 Transmission Electron Microscope Analysis of Soil Materials R. J. Gilkes .......................................... 177 The Transmission Electron Microscope ............................ 177 The Interactions of an Electron Beam with Crystals .................... 179 Diffracted Electrons ..................................... 179 Forward-Scattered Electrons ................................ 185 Surface-Backscattered and Secondary Electrons ..................... 185 Х -Rays ............................................. 186 Transmitted Electrons .................................... 186 Specimen Preparation ....................................... 188 Deposition of Dispersed Particles ............................. 188 Microtomed and Ion-Beam-Thinned Samples ...................... 188 Examples of Transmission Electron Microscope Studies of Soil Minerals ....... 189 Investigations of Dispersed Particles ........................... 189 Studies of Undisturbed Mineral Assemblages and Fabrics .............. 194 Amorphous Soil Constituents ................................ 200 Future Directions ......................................... 200 7 Analysis of Soil Surfaces by Х -Ray Photoelectron Spectroscopy D. L. Соске, R. K. Vempati and R. H. Loeppert ................... 205 Theory ................................................ 205 Basic Х -Ray Photoelectron Spectroscopy ......................... 205 Experimental Techniques..................................... 215 Instrumentation ........................................ 215 Sample Handling ....................................... 217 Quantitative Studies ..................................... 217 Sputtering Method ...................................... 218 Angle-Resolved Х -Ray Photoelectron Spectroscopy .................. 220 Applications ............................................. 221 Semi-Quantitative Analysis ................................. 221 Qualitative Analysis ...................................... 222 Future Developments ....................................... 231 Summary .............................................. 231 CONTENTS vin 8 Preconcentration Techniques in Soil Mineralogical Analyses D. A. Laird and R. H. Dowdy .............................. 236 Particle-Size Techniques ..................................... 236 Pretreatments and Dispersion ................................ 237 Stokes Law .......................................... 238 Size Fractionation of Soil Clays .............................. 240 Density Techniques ........................................ 241 Density of Soil Minerals .................................. 241 Density-Fractionation Techniques ............................. 241 Density Separation of Soil Minerals ............................ 246 Magnetic Techniques ....................................... 248 Magnetic Separation of Fine Materials .......................... 248 Magnetic Separation of Soil Minerals ........................... 251 Electrophoretic Techniques ................................... 254 Smoluchowski Equation ................................... 255 Electrophoretic Techniques ................................. 255 Electrophoretic Separation of Soil Materials ....................... 256 Other Methods of Mineral Separation ............................. 261 Conclusions ............................................. 262 9 Quantitative Х -Ray Diffraction Analysis of Soils D. L. Bish ........................................... 267 Sample Preparation ........................................ 268 Particle-Size Requirements ................................. 268 Sample Grinding ....................................... 270 Sample Mounting ....................................... 272 Conventional Quantitative Analysis .............................. 273 Reference Intensity Ratio Method ............................. 274 Absorption-Diffraction Method ............................... 275 Method of Known Additions ................................ 275 Standards ............................................ 276 Intensity Measurement .................................... 276 Amorphous Components .................................. 277 Simultaneous Linear Equations Methods ........................... 277 Full-Pattern Fitting Methods .................................. 278 The Rietveld Method ..................................... 279 Observed Patterns ....................................... 290 Conclusions and Future Developments ............................ 291 10 Analysis of Minerals in Oxide-Rich Soils by Х -Ray Diffraction R. C Jones and H. U. Malik ............................... 296 Sample Preparation ................................... 297 Dispersion ................................. 297 Clay Subfractions ............................. 299 High-Iron Soils .......................... ........... .......................... 3qq Sample Pretreatments .................................... 300 Specimen Mounts ................. ....................... 302 Bulk Powder Cavity Mount ................................. Paste on Glass Slide .............. , _..................... Paste on Molybdenum Slide ................................ CONTENTS ix Paste on Zero-Background Mounts ............................ 304 Powder on Zero-Background Mounts ........................... 304 Data Collection .......................................... 304 Integration Interval ...................................... 304 Step Size ............................................ 305 Theta-Compensating and Fixed Divergence Slits .................... 306 Corrections for Specimen Surface Displacement .................... 306 Mineral Identification ....................................... 307 Halloysite and Kaolinite ................................... 307 Illitic Minerals ......................................... 309 Interstratified Phyllosilicates ................................ 309 Short-Range-Order Materials ................................ 309 Curve-Fitting Procedures ..................................... 314 Pi o Pili Pa a ......................................... 314 Diffracting-Domain Size ................................... 318 Comparison with the Rietveld Refinement Technique ................. 321 Future Trends .............................................. 324 Summary and Conclusions .................................... 326 11 Qualitative and Quantitative Analysis of Clay Minerals in Soils R. E. Hughes, D. M. Moore, and H. D. Glass ..................... 330 Clay Minerals in Soils ....................................... 332 Methods ................................................ 335 Sample Preparation and Instrumentation .......................... 335 Methods of Analysis ...................................... 339 Interpretation of Results .................................... 342 Examples of Quantitative Representation ............................ 343 Oxidation and the Loss or Alteration of Chlorite ..................... 344 Loss of Carbonates ....................................... 346 Weathering of Expandables and Illite ............................ 347 Iron and Aluminum Oxides/Hydroxides .......................... 352 Future Developments ........................................ 354 Summary ............................................... 355 12 Quantitative Thermal Analysis of Soil Materials A.D. Karathanasis and W.G. Harris ........................... 360 Principles and Instrumentation ................................. 360 Thermogravimetry ...................................... 360 Differential Thermal Analysis ............................... 362 Differential Scanning Calorimetry ............................. 364 Thermomechanical Methods ................................ 364 Quantitative Applications of Thermal Analysis to Soil Materials ............. 366 Quantitative Estimation of Soil Minerals ......................... 370 Thermal Reaction Kinetics ................................. 390 Special Thermal Applications ................................ 399 Advantages and Limitations ................................... 402 Recent and Future Developments in Quantitative Thermal Analysis ........... 405 Summary and Conclusions .................................... 408 CONTENTS 13 Differential Х -Ray Diffraction Analysis of Soil Minerals D. G. Schulze ......................................... 412 Selective-Dissolution Procedures ................................ 412 Sample Preparation ........................................ 413 Identical Treatment ...................................... 413 Particle Size .......................................... 413 Particle Orientation ...................................... 414 Sample Thickness ....................................... 414 Oriented Slide Mounts .................................... 414 Data Collection .......................................... 415 Data Reduction ........................................... 415 Adjusting Intensities ..................................... 415 Aligning 2Θ Scales ...................................... 418 Identification of Mineral Phases ................................ 420 Goethite and Hematite .................................... 420 Ferrihydrite .......................................... 422 Poorly Crystallized Aluminosilicates ........................... 422 Carbonates ........................................... 425 Quantitative Analysis of Mineral Phases ........................... 425 Evaluation of Selective-Dissolution Techniques ........................ 426 Future Developments ....................................... 427 Summary .............................................. 427 Appendix .............................................. 428 14 Quantification of Allophane and Imogolite R. A. Dahlgren ........................................ 430 Principles and Techniques .................................... 431 Selective Dissolution ..................................... 431 Infrared Spectroscopy .................................... 436 Thermal Analysis ....................................... 440 Other Techniques ....................................... 442 Application to Soil Mineralogy ................................. 444 Sample Handling and Pretreatments ............................ 444 Standard Reference Materials ................................ 444 Example from Comparative Studies ............................ 446 Additional Topics ....................................... 446 Future Developments ....................................... 447 Summary and Conclusions .................................... 447 Subject Index .................................... 452
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spelling	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990 ed. committee: James E. Amonette ... Madison, Wis. SSSA 1994 XXI, 462 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier SSSA miscellaneous publication Bodenanalyse (DE-588)4146122-8 gnd rswk-swf Mineralboden (DE-588)4170022-3 gnd rswk-swf (DE-588)1071861417 Konferenzschrift 1990 San Antonio Tex. gnd-content Mineralboden (DE-588)4170022-3 s Bodenanalyse (DE-588)4146122-8 s DE-604 Amonette, James E. Sonstige oth Digitalisierung TU Muenchen application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006903075&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990 Bodenanalyse (DE-588)4146122-8 gnd Mineralboden (DE-588)4170022-3 gnd
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title	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990
title_auth	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990
title_exact_search	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990
title_full	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990 ed. committee: James E. Amonette ...
title_fullStr	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990 ed. committee: James E. Amonette ...
title_full_unstemmed	Quantitative methods in soil mineralogy proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990 ed. committee: James E. Amonette ...
title_short	Quantitative methods in soil mineralogy
title_sort	quantitative methods in soil mineralogy proceedings of a symposium sponsored by division s 9 of the soil science society of america the symposium was held in san antonio texas on october 23 34 1990
title_sub	proceedings of a symposium sponsored by Division S-9 of the Soil Science Society of America ; the symposium was held in San Antonio, Texas on October 23 - 34, 1990
topic	Bodenanalyse (DE-588)4146122-8 gnd Mineralboden (DE-588)4170022-3 gnd
topic_facet	Bodenanalyse Mineralboden Konferenzschrift 1990 San Antonio Tex.
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