Modern ESCA: the principles and practice of X-ray photoelectron spectroscopy
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Boca Raton u.a.
CRC Press
1994
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 358 S. Ill., graph. Darst. |
| ISBN: | 0849386535 |
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| adam_text | MODERN ESCA THE PRINCIPLES AND PRACTICE OFX-RAY PHOTOELECTRON
SPECTROSCOPY TERY L. BARR CRC PRESS BOCA RATON ANN ARBOR LONDON TOKYO
TABLE OF CONTENTS CHAPTER 1 INTRODUCTION 1 I. INTRODUCTORY STATEMENT 1
II. HISTORICAL PERSPECTIVE 1 REFERENCES 3 CHAPTER 2 THE ESCA PROCESS 5
I. BASIC PRINCIPLES AND PROCEDURES 5 II. PROBLEMS: RELAXATION AND
SATELLITES 6 III. PROBLEMS: INTRODUCTION TO CHARGING AND FERMI EDGE
COUPLING 8 IV. INTRODUCTION TO THE CHEMICAL SHIFT 12 V. RECENT EXAMPLES
OF THE USE OF CHEMICAL SHIFTS 18 A. BINDING ENERGY PROGRESSIONS FOR
SIMPLE OXIDES AND THEIR SIGNIFICANCE 18 1. THE PROGRESSIVE CHANGES IN
THE CHEMICAL SHIFTS OF THE M SPECIES 19 2. THE CHEMICAL SHIFTS
EXPERIENCES BY O(LS) FOR THE DIFFERENT OXIDES 20 B. MIXED OXIDE SYSTEMS
20 1. CORE LEVEL SHIFTS FOR THE METALLIC SPECIES 21 2. CHEMICAL SHIFTS
OF O(LS) FOR COMPLEX OXIDES 21 C. OXIDE ION SIZE AND SHAPE
POLARIZATION 24 D. CHEMICAL SHIFTS AND ZEOLITE STRUCTURE AND ACIDITY
25 VI. SUMMARY OF THE PROS AND CONS OF CONVENTIONAL ESCA 26 REFERENCES
28 CHAPTER 3 THE ESCA SPECTROMETER AND ITS USE 31 I. INTRODUCTION TO THE
BASIC SYSTEM 31 IL EXTENSIONS AND IMPROVEMENTS 31 A. MONOCHROMATORS *
HIGH RESOLUTION AND ACUTE SENSITIVITY 31 B. OTHER DEVELOPMENTS * SPATIAL
RESOLUTION 33 III. THE PRESENT PERFORMANCE FRONTIER 33 IV. STANDARD
USAGE OF THE ESCA SYSTEM 36 A. INTRODUCTION 36 B. VACUUM AND SYSTEM
MAINTENANCE 37 C. BASIC CALIBRATIONS 38 D. MORE EXACTING CALIBRATIONS 38
E. SURVEY SCANS 44 F. NARROW SCANS 45 G. NARROW SCANS * ADDENDUM 46 H.
OPERATIONS UNDER LESS THAN OPTIMAL CONDITIONS 47 I. WHAT ARE THE LIMITS?
47 J. PROBLEMS 47 1. CHARGING 47 2. X-RAY SATELLITES 48 3. SAMPLE DAMAGE
48 4. POOR VACUUM 51 5. GHOST PEAKS AND MYSTERY SHIFTS 51 6. OTHER
PROBLEMS 53 REFERENCES 54 CHAPTER 4 QUANTUM MECHANICAL ARGUMENTS 57 I.
INTRODUCTION TO THE TOTAL (PRIMARY ELASTIC) PROCESS 57 II. INELASTIC
SCATTERING PROCESSES 59 A. RELAXATIONS 59 1. FROZEN ORBIT APPROXIMATION
59 2. MODIFICATION OF KOOPMANS THEOREM FOR SLOW ELECTRONS 62 B.
SATELLITES * THE LOSS PROCESS 63 1. THE SUDDEN APPROXIMATION 63 2. THE
TWO EXTREME CASES 65 REFERENCES 67 CHAPTER 5 ESTABLISHED ESCA PROCEDURES
71 I. QUANTIFICATION 71 II. ANGULAR RESOLUTION-PHOTOELECTRON
SPECTROSCOPY (AR-PES) 75 A. BACKGROUND 75 B. AR DEVELOPMENT AND
PROCEDURE 76 C. THE USE OF ANGULAR RESOLUTION 76 III. ESCA AND ION
SPUTTER ETCHING 81 A. IDEAL CASE 81 B. PREFERENTIAL SPUTTERING 83 C.
SPECIFIC CASES OF SPUTTER ALTERATION 85 RV. ULTRAVIOLET PHOTOELECTRON
SPECTROSCOPY (UPS) AND GAS PHASE ANALYSIS 86 REFERENCES 90 CHAPTER 6
LOSS SPECTROSCOPY IN ESCA: ITS CAUSES AND UTILIZATION 93 I. INTRODUCTION
93 A. RELATED PLASMON-TYPE TRANSITIONS 94 B. THE EARLY HISTORY OF LOSS
SPECTROSCOPY AND PLASMONS 95 II. UTILIZATION OF XPS-INDUCED LOSS
SPECTROSCOPY (ESCALOSS): ADVANTAGES AND DISADVANTAGES 95 A. CHARGING AND
FERMI EDGE DECOUPLING 95 B. LARGE, RELATIVELY EASY TO DISCERN SHIFTS,
WITH CHANGES IN CHEMISTRY 96 C. NONCHEMICAL BASIS FOR CHEMICAL SHIFTS 96
III. THE PLASMON DOMINATION ARGUMENT 97 IV. GENERAL QUANTUM MECHANICAL
BASIS FOR ESCALOSS 98 A. THE PINES AND NOZIERES ARGUMENTS (EXTRINSIC
ONLY) 98 1. H * THE VARIOUS MODELS 99 2. H 1 * THE VARIOUS TYPES OF
ELECTRON INTERACTIONS 100 B. LOSS SPECTRAL DEVELOPMENT FOLLOWING
PHOTOELECTRON EJECTION (INCLUSION OF INTRINSIC PROCESSES) 102 C. FURTHER
ARGUMENTS ON THE NATURE OF THE ELECTRON-INDUCED DISPERSIONS IN LOSS
SPECTROSCOPY 104 D. ON THE SEPARATION OF THE HOLE AND ELECTRON-INDUCED
LOSSES 105 E. ESCALOSS 106 1. E L AND AE L FOR MATERIALS WITH NONZERO E
G 106 2. RELAXATIONS AND LOSS PEAKS INSIDE THE FREE ELECTRON MODEL 106
3. SUMMARY OF PHOTOELECTRON LOSS SPLITTINGS FOR DIFFERENT MODELS 108 F.
THE INFLUENCE OF DISPERSIONS ON RELAXATION EFFECTS IN E L 111 G. FINAL
ARGUMENT FOR EFFECTS OF DISPERSION 112 V. EXAMPLES OF THE USE OF
ESCALOSS IN CHEMICAL ANALYSIS 113 A. ELEMENTAL SYSTEMS 113 B. INDIUM
COMPOUNDS 113 C. SI0 2 -SI 0 AND A1 2 0 3 -A1 SYSTEMS 114 D. GENERAL
FEATURES 116 VI. AN ADDITIONAL, IMPORTANT ESCALOSS SPECTROSCOPY EXAMPLE
* THE CARBON PROBLEM 116 A. INTRODUCTION 116 B. GRAPHITE 121 C.
CARBON-BASED SYSTEMS DEVOID OF AROMATIC STRUCTURE * POLYPROPYLENE 122 D.
ADVENTITIOUS CARBON 123 E. UTILITY 127 F. RATIONALE 128 REFERENCES 129
CHAPTER 7 OLD PROBLEM AREAS * NEW ESCA ANALYSIS METHODS 133 I. THE
CHARGING SHIFT AND FERMI EDGE REFERENCING AS TOOLS 133 A. FUNDAMENTALS
OF THE CHARGING SHIFT 133 B. DIFFERENTIAL CHARGING 133 C. MORPHOLOGICAL
CONSIDERATIONS 134 1. LAYERED STRUCTURES 134 2. THE SIIMPLANTED IN SI0
2 SYSTEMS 136 D. ADDITIONAL MORPHOLOGICAL CONSIDERATIONS 138 1. DEPTH OF
FIELDS 138 2. DISPERSIONS AND CLUSTERS 140 3. THE OPTIMAL REDUCED
PT-Y-AL 2 0 3 SYSTEM 141 UE. ESCA-INDUCED VALENCE BAND SPECTRA 143 A.
INTRODUCTION 143 B. TECHNICALITIES OF THE METHOD 143 C. XPS-VALENCE BAND
ANALYSES OF CONDUCTIVE SYSTEMS 145 D. VALENCE BANDS OF NONCONDUCTIVE
COMPOUNDS 145 1. TRANSITION METAL OXIDES 145 2. VALENCE BAND STUDIES OF
TETRAHEDRAL COMPOUND SEMICONDUCTORS 146 3. VALENCE BAND STUDIES OF
SILICA AND ALUMINA 149 4. VALENCE BAND STUDIES OF GERMANIUM OXIDES 149
5. VALENCE BAND STUDIES FOR INDIUM OXIDES 156 6. VALENCE BAND STUDIES OF
ION-ALTERED TIN AND OXIDES 162 7. VALENCE BAND STUDIES OF ZEOLITES 162
REFERENCES 169 CHAPTER 8 AREAS OF ESCA APPLICATION 173 I. INTRODUCTION
173 II. ESCA STUDIES OF ELEMENTAL OXIDATION 174 A. THE NATURAL
PASSIVATION OF ELEMENTAL METALS: ORIGIN AND CONSEQUENCES 174 B. VALENCE
BAND STUDIES OF THE OXIDATION OF SELECT METALS 176 1. THE ZN-0 SYSTEM
176 2. THECD-0 SYSTEM 181 III. ESCA STUDIES OF INORGANIC SYSTEMS 184 A.
GENERAL BONDING CONCEPTS OF SIMPLE OXIDE SYSTEMS 184 B. BONDING IN MIXED
OR COMPLEX OXIDES 190 1. INTRODUCTION TO THE PROBLEM OF COMPLEX OXIDES
190 2. FURTHER ON THE MIXED OXIDE BONDING CONCEPT 191 3. ESCA
VERIFICATION OF THE CONCEPT 192 4. EXTENT AND LIMITATION OF THE MIXED
OXIDE BONDING CONCEPT 192 5. THE ACID-BASE CONNECTION 194 IV. XPS AND
CORROSION SCIENCE 195 A. ALLOYS: NATURAL PASSIVATION AND CORROSION 196
B. THE SPECIAL CASE OF MIXED HYDROXIDES 200 C. NATURAL PASSIVATION OF
SEMICONDUCTORS 201 D. NATURAL PASSIVATION AND CORROSION OF INERT
POLYMERS * BIOLOGY AND THE WORLD AT LARGE 203 1. GENERALITY 204 E.
ADDITIONAL IMPLICATIONS OF NATURAL PASSIVATION 205 1. TERMINATION OF
PASSIVATION 205 2. METALS AT OR NEAR THE LTO LIMIT * THE CATALYTIC
CONNECTION 205 V. ESCA STUDIES OF THE CARBONACEOUS SYSTEMS INVOLVED IN
POLYMERS, COMPOSITES, AND RELATED CHEMISTRIES 207 A. FUNDAMENTAL
PROBLEMS 207 1. ANALYSIS OF SELECT ESCA-BASED METHODS FOR C-C AND C-H
BOND IDENTIFICATION 210 2. C(LS) BINDING ENERGY 210 3. CHARGING AND
CONDUCTIVITY 210 4. TT . * 71* TRANSITIONS 210 5. CHARACTER OF THE
VALENCE BANDS 211 6. CARBON(LS) (PLASMON-DOMINATED) LOSS SPECTRA 212 7.
OXIDATION OF SELECT CARBONACEOUS SYSTEMS 213 8. 0(LS)RESULTS 214 9.
ANALYSIS OF THE 0(2S) REGION 214 10. COMPARISONS WITH OTHER OXIDES 215
11. COMPARATIVE SUMMARY OF THE DIFFERENT METHODS 217 B. ESCA
CHARACTERIZATION OF CARBON MICRO-FIBERS AS REINFORCEMENTS FOR VARIOUS
EPOXY RESINS 218 VI. ESCA AND CATALYSIS 220 A. ESCA STUDIES OF ZEOLITES
AND CLAYS 220 1. ZEOLITES 220 2. ESCA STUDIES OF SELECT CLAYS 225 B.
ESCA STUDIES OF ACRYLONITRILE (ACN) CATALYSTS 232 C. STUDIES OF PT METAL
CATALYSIS BY HIGH-RESOLUTION ESCA 235 1. ANALYSIS OF THE ALUMINA SUPPORT
236 2. OXIDIZED PT ON A1 2 0 3 SYSTEM 236 3. METALS REDUCTION AND
DISPERSION 237 4. BIMETALLIC CASES 238 VII. ESCA IN BIOLOGY AND MEDICINE
239 A. BIOMEDICAL ESCA STUDIES 239 B. UNCONVENTIONAL USE OF ESCA IN
BIOLOGICAL RESEARCH 241 C. INVESTIGATIONS IN BOTANY 241 1. ESCAOF LEAVES
241 2. VACUUM AND X-RAY DAMAGE 242 3. LEAVES IN VARIOUS STAGES OF
SENESCENCE 242 VIII. XPS STUDIES IN HIGH T C SUPERCONDUCTORS 253 A.
BONDING AND ELECTRONIC STRUCTURE 253 1. INTRODUCTION 253 2. SIMPLE
COPPER OXIDES 254 3. SUPERCONDUCTING COPPER-CONTAINING OXIDES 254 4.
CONNECTIONS BETWEEN THE GENERAL OXIDE ARGUMENTS AND THE SUPERCONDUCTORS
257 5. MECHANISTIC SUGGESTIONS 258 B. STUDIES OF THE OXYGEN INTENSITY IN
1-2-3 SYSTEMS 259 REFERENCES 265 CHAPTER 9 SURVEY OF ADDITIONAL
PROMISING NEW METHODS 273 I. MODERN ESCA AND THE CONTINUING UPPSALA
CONNECTION 273 II. INVERSE PHOTOEMISSION AND TWO-PHOTON PHOTOEMISSION
273 A. INTRODUCTION 273 B. INVERSE PHOTOEMISSION 274 C. TWO-PHOTON
SPECTROSCOPY 276 D. EMPTY STATE ANALYSIS * GENERAL CONSIDERATIONS 276
III. PHOTOELECTRON DIFFRACTION (PED) 276 IV. SPIN-POLARIZED PHENOMENA
281 A. SPIN-POLARIZED PHOTOEMISSION SPECTROSCOPY (SPPES) 281 B.
SPIN-POLARIZED INVERSE PHOTOEMISSION SPECTROSCOPY (SPIPES) 281 C.
SPIN-POLARIZED PHOTOELECTRON DIFFRACTION (SPPED) 282 V. PHOTOELECTRON
MICROSCOPY 282 VI. PHOTOEMISSION OF ADSORBED XENON (PAX) 288 VII.
PHOTOELCTRON SHIFTS DUE TO COMPONENT ORIENTATION 291 A. INTRODUCTION 291
B. SURFACE CORE-LEVEL SHIFTS: DISCOVERY AND THEORETICAL CONTROVERSY,
1978 TO 1983 294 1. SURFACE CORE-LEVEL SHIFTS * METALS 294 C.
INTERFACIAL SHIFTS 300 D. ALLOY FORMATION AND SURFACE RECONSTRUCTION 308
1. ALLOY FORMATION: INTERMEDIATE COMPOUNDS 308 2. SURFACE RECONSTRUCTION
308 E. SURFACE SHIFTS FOR SEMICONDUCTORS 308 F. SMALL CLUSTER SHIFTS 309
G. ALTERNATIVE REASONS FOR SOME OF THE ORIENTATION SHIFTS 316 1.
CHARGING 316 2. HYDROGEN CONTAMINATION 317 VIII. RESONANT PHOTOEMISSION
321 IX. LIQUID PHASE ESCA 322 REFERENCES 328 APPENDIX 1 337 APPENDIX II
339 INDEX 343
|
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| discipline | Chemie / Pharmazie Physik Chemie |
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| spelling | Barr, Tery L. Verfasser aut Modern ESCA the principles and practice of X-ray photoelectron spectroscopy Tery L. Barr Boca Raton u.a. CRC Press 1994 358 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Spectroscopie électronique Spectroscopie électronique ram Surfaces (Technologie) - Analyse Surfaces (technologie) - Analyse ram Electron spectroscopy Surfaces (Technology) Analysis Röntgen-Photoelektronenspektroskopie (DE-588)4076787-5 gnd rswk-swf Festkörperoberfläche (DE-588)4127823-9 gnd rswk-swf Elektronenspektroskopie (DE-588)4014332-6 gnd rswk-swf Röntgen-Photoelektronenspektroskopie (DE-588)4076787-5 s Festkörperoberfläche (DE-588)4127823-9 s DE-604 Elektronenspektroskopie (DE-588)4014332-6 s GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006529525&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Barr, Tery L. Modern ESCA the principles and practice of X-ray photoelectron spectroscopy Spectroscopie électronique Spectroscopie électronique ram Surfaces (Technologie) - Analyse Surfaces (technologie) - Analyse ram Electron spectroscopy Surfaces (Technology) Analysis Röntgen-Photoelektronenspektroskopie (DE-588)4076787-5 gnd Festkörperoberfläche (DE-588)4127823-9 gnd Elektronenspektroskopie (DE-588)4014332-6 gnd |
| subject_GND | (DE-588)4076787-5 (DE-588)4127823-9 (DE-588)4014332-6 |
| title | Modern ESCA the principles and practice of X-ray photoelectron spectroscopy |
| title_auth | Modern ESCA the principles and practice of X-ray photoelectron spectroscopy |
| title_exact_search | Modern ESCA the principles and practice of X-ray photoelectron spectroscopy |
| title_full | Modern ESCA the principles and practice of X-ray photoelectron spectroscopy Tery L. Barr |
| title_fullStr | Modern ESCA the principles and practice of X-ray photoelectron spectroscopy Tery L. Barr |
| title_full_unstemmed | Modern ESCA the principles and practice of X-ray photoelectron spectroscopy Tery L. Barr |
| title_short | Modern ESCA |
| title_sort | modern esca the principles and practice of x ray photoelectron spectroscopy |
| title_sub | the principles and practice of X-ray photoelectron spectroscopy |
| topic | Spectroscopie électronique Spectroscopie électronique ram Surfaces (Technologie) - Analyse Surfaces (technologie) - Analyse ram Electron spectroscopy Surfaces (Technology) Analysis Röntgen-Photoelektronenspektroskopie (DE-588)4076787-5 gnd Festkörperoberfläche (DE-588)4127823-9 gnd Elektronenspektroskopie (DE-588)4014332-6 gnd |
| topic_facet | Spectroscopie électronique Surfaces (Technologie) - Analyse Surfaces (technologie) - Analyse Electron spectroscopy Surfaces (Technology) Analysis Röntgen-Photoelektronenspektroskopie Festkörperoberfläche Elektronenspektroskopie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006529525&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT barrteryl modernescatheprinciplesandpracticeofxrayphotoelectronspectroscopy |