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HPLC: a practical user's guide

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Bibliographic Details
Main Author:	McMaster, Marvin C. (Author)
Format:	Book
Language:	English
Published:	New York u.a. VCH 1994
Subjects:	High performance liquid chromatography HPLC
Online Access:	Inhaltsverzeichnis
Physical Description:	XII, 211 S. graph. Darst.
ISBN:	1560816368

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MARC


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adam_text	HPL C A PRACTICAL USER'S GUID E MARVIN C . MCMASTER PART I : AN HPLC PRIMER 1 1. WHY HPLC? ADVANTAGES AND DISADVANTAGES 3 1 .1 HOW DOES IT WORK? 4 1 .2 HOW ELSE COULD I GET MY SEPARATION? 1 0 2. SELECTING AN HPLC SYSTEM 1 5 2.1 WHAT DO I LOOK FOR IN A SYSTEM? 1 5 2.2 FROM WHOM DOIBUYIT? 1 7 2 .3 WHAT WILL IT COST? 18 2.4 COLUMNS 20 3. RUNNING YOUR CHROMATOGRAPH 2 5 3 .1 SETUP AND START-UP 2 5 3.2 SAMPLE PREPARATION AND COLUMN CALIBRATION 35 3.3 YOUR FIRST CHROMATOGRAM 3 7 PART II : HPLC OPTIMIZATION 4 3 4. SEPARATION MODELS 4 5 4 .1 PARTITION 4 5 4 .2 ION-EXCHANGE CHROMATOGRAPHY 56 4 .3 SIZE-EXCLUSION CHROMATOGRAPHY 57 4 .4 AFFINITY CHROMATOGRAPHY 5 9 5. COLUMN PREPARATION 6 1 5.1 COLUMN VARIATIONS 6 1 5 .2 PACKING MATERIALS AND HARDWARE 6 4 5.3 COLUMN SELECTION 6 6 6. COLUMN AGING, DIAGNOSIS, AND HEALING 7 1 6 .1 PACKING DEGRADATION-BONDED-PHASE LOSS 7 3 6 .2 DISSOLVING PACKING MATERIAL-END VOIDS 7 4 6.3 BOUND MATERIAL 7 6 6 .4 PRESSURE INCREASES 7 9 6.5 COLUMN CHANNELING-CENTER VOIDS 8 0 6 .6 NORMAL PHASE, ION EXCHANGE, AND SIZE COLUMNS 82 7. MODIFICATIONS OF PARTITION CHROMATOGRAPHY 8 5 7 .1 REVERSE PHASE 85 7.2 ACIDIC-PHASE SILICA 89 7 .3 PARTITION MODE SELECTION 8 9 7 .4 HYDROPHILIC SEPARATIONS 90 8. "NONPARTITION" CHROMATOGRAPHY 9 3 8.1 ION EXCHANGE 93 8.2 SIZE EXCLUSION 9 5 8 .3 AFFINITY CHROMATOGRAPHY 9 7 9. HARDWARE SPECIFICS 9 9 9.1 SYSTEM PROTECTION 9 9 9.2 PUMPING 10 2 9.3 INJECTORS AND AUTOSAMPLERS 10 9 9 .4 DETECTORS 10 9 9 .5 FRACTION COLLECTORS 11 5 9 .6 DATA COLLECTION AND PROCESSING 11 6 10. TROUBLESHOOTING AND OPTIMIZATION 11 7 10 .1 HARDWARE AND TOOLS-SYSTEM PACIFICATION 11 7 10 .2 REVERSE ORDER DIAGNOSIS 12 1 10 .3 INTRODUCTION TO DATA ACQUISITION 123 PART III : HPLC UTILIZATION 12 7 11. PREPARATIVE CHROMATOGRAPHY 12 9 11 .1 ANALYTICAL PREPARATIVE 130 11 .2 SEMIPREPARATIVE 13 1 11 .3 "TRUE" PREPARATIVE 13 1 12. SAMPLE PREPARATION AND METHODS DEVELOPMENT 13 5 12 .1 SAMPLE PREPARATION 135 12 .2 METHODS DEVELOPMENT 143 12 .3 GRADIENT DEVELOPMENT 148 13. APPLICATION LOGIC : SEPARATIONS OVERVIEW 15 1 13 .1 FAT-SOLUBLE VITAMINS, STEROIDS, AND LIPIDS 15 1 13 .2 WATER-SOLUBLE VITAMINS, CARBOHYDRATES, AND ACIDS 152 13 .3 DNA FAMILY: NUCLEIC ACIDS, NUCLEOSIDES/NUCLEOTIDES, AND RNA / DNA 152 13.4 PROTEIN FAMILY: AMINO ACIDS, PEPTIDES, AND PROTEINS 154 13 .5 CLINICAL DRUG MONITORING, TOXICOLOGY, AND FORENSICS 155 13 .6 ENVIRONMENTAL AND REACTION MONITORING 15 5 13 .7 APPLICATION TRENDS 15 6 14. AUTOMATION : SEPARATIONS AND DATA ACQUISITION 159 14 .1 ANALOG-TO-DIGITAL INTERFACING 15 9 14 .2 DIGITAL INFORMATION EXCHANGE 16 1 14 .3 HPLC SYSTEM CONTROL AND AUTOMATION 16 1 14 .4 DATA COLLECTION AND INTERPRETATION 16 2 14 .5 AUTOMATED METHODS DEVELOPMENT 16 4 14.6 DATA EXPORTATION TO THE REAL WORLD 16 8 15. WHERE DO WE GO FROM HERE? 17 1 15 .1 MICROSYSTEMS AND SUPERDETECTORS 17 1 15 .2 LC/MS PRIMER 17 2 15.3 NEW COLUMN DIRECTIONS 18 1 15 .4 DEDICATED SYSTEMS : PUSHBUTTON CLINICAL AND THE PERSONAL HPL C 18 2 APPENDIXES 18 3 A. PERSONAL SEPARATION GUIDE 18 5 B. A GLOSSARY OF HPLC TERMS 187 C. HPLC TROUBLESHOOTING QUICK REFERENCE 193 D. LABORATORY EXPERIMENTS 19 7 LABORATORY 1-SYSTEM START-UP AND COLUMN QC 19 7 LABORATORY 2-SAMPLE PREPARATION AND METHOD DEVELOPMEN T 199 LABORATORY 3-COLUMN AND SOLVENT SWITCHING AND PACIFICATIO N 200 E. SELECTED REFERENCE LIST 20 3 INDEX 205
any_adam_object	1
author	McMaster, Marvin C.
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callnumber-first	Q - Science
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dewey-ones	543 - Analytical chemistry
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dewey-sort	3543 3894
dewey-tens	540 - Chemistry and allied sciences
discipline	Chemie / Pharmazie Biologie Chemie
format	Book
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illustrated	Illustrated
indexdate	2025-01-07T13:02:25Z
institution	BVB
isbn	1560816368
language	English
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physical	XII, 211 S. graph. Darst.
publishDate	1994
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publisher	VCH
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spelling	McMaster, Marvin C. Verfasser (DE-588)113962231 aut HPLC a practical user's guide Marvin C. McMaster New York u.a. VCH 1994 XII, 211 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier High performance liquid chromatography HPLC (DE-588)4072641-1 gnd rswk-swf HPLC (DE-588)4072641-1 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006363753&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	McMaster, Marvin C. HPLC a practical user's guide High performance liquid chromatography HPLC (DE-588)4072641-1 gnd
subject_GND	(DE-588)4072641-1
title	HPLC a practical user's guide
title_auth	HPLC a practical user's guide
title_exact_search	HPLC a practical user's guide
title_full	HPLC a practical user's guide Marvin C. McMaster
title_fullStr	HPLC a practical user's guide Marvin C. McMaster
title_full_unstemmed	HPLC a practical user's guide Marvin C. McMaster
title_short	HPLC
title_sort	hplc a practical user s guide
title_sub	a practical user's guide
topic	High performance liquid chromatography HPLC (DE-588)4072641-1 gnd
topic_facet	High performance liquid chromatography HPLC
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=006363753&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT mcmastermarvinc hplcapracticalusersguide

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