Chemical analysis: An advanced text and reference
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Düsseldorf
McGraw-Hill
1975
|
| Ausgabe: | 2. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | McGraw-Hill series in advanced chemistry |
| Beschreibung: | XIX, 611 S. |
Internformat
MARC
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| 100 | 1 | |a Laitinen, Herbert A. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Chemical analysis |b An advanced text and reference |c Herbert A. Laitinen ; Walter A. Harris* |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a Düsseldorf |b McGraw-Hill |c 1975 | |
| 300 | |a XIX, 611 S. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a McGraw-Hill series in advanced chemistry | ||
| 650 | 4 | |a Analyse quantitative (Chimie) | |
| 650 | 4 | |a Chemistry Techniques, Analytical | |
| 650 | 4 | |a Chemistry, Analytic |x Quantitative | |
| 650 | 0 | 7 | |a Analytische Chemie |0 (DE-588)4129906-1 |2 gnd |9 rswk-swf |
| 689 | 0 | 0 | |a Analytische Chemie |0 (DE-588)4129906-1 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Harris, Walter A. |e Verfasser |4 aut | |
| 856 | 4 | 2 | |m HBZ Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005993094&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-005993094 | ||
Datensatz im Suchindex
| _version_ | 1804123410108776448 |
|---|---|
| adam_text | Titel: Chemical analysis
Autor: Laitinen, Herbert A
Jahr: 1975
CONTENTS
Preface
xvii
1
The
Operations
of
Analysis
1
2
Equilibrium
and
Activity
5
2-1
The
Condition
of
Equilibrium
5
2-2
Activity
and
the
Standard
State
6
2-3
The
Debye-Hiickel
Theory
9
2-4
Activity
Coefficients
at
High
Ionic
Strengths
15
2-5
Activity
Coefficients
in
Mixed
Electrolytes
16
2-6
Salt
Effects
on
Equilibrium
Constants
17
2-7
Nonelectrolytes
and
Activity
19
References
23
Problems
24
3
Acid-Base
Equilibria
in
Water
27
3-1
Methods
of
Dealing
with
Equilibria
28
3-2
Equilibrium
in
Pure
Water
29
viii
CONTENTS
3-3
Definition
of
the
pH
Scale
30
3-4
Equilibria
in
a
Single
Acid-Base
System
in
Water
33
3-5
Equilibria
in
Multiple
Acid-Base
Systems
37
3-6
Calculation
of
Concentrations
of
Species
Present
at
a
Given
pH
41
3-7
Titration
Curves
43
3-8
Microscopic
Ionization
Constants
45
3-9
Effect
of
Temperature
on
Acid-Base
Equilibria
47
3-10
Acid-Base
Indicators
48
3-
11
Acidity
in
Heavy
Water
51
References
52
Problems
54
4
Acid-Base
Equilibria
in
Nonaqueous
Solvents
56
4-
1
The
Standard-State
Problem
and
Nonaqueous
Solvents
57
4-2
Dielectric
Constant
60
4-3
Specific
Solute-Solvent
Interactions
and
Proton
Transfer
Reactions
62
4-4
Electrolytic
Dissociation
67
4-5
Equilibrium
Expressions
Used
in
pH
Calculations
69
4-6
Acid-Base
Equilibria
in
Glacial
Acetic
Acid
71
4-7
Acid-Base
Equilibria
in
Ethylenediamine
74
4-8
Acid-Base
Equilibria
in
Acetonitrile
79
4-9
Acids
and
Bases
in
Alcohol-Water
Mixtures
84
4-10
pH
Measurements
in
Nonaqueous
Solvents
85
4-11
Acid-Base
Indicators
in
Solvents
of
Low
Dielectric
Constant
88
4-
12
Acidity
and
Strongly
Acid
Solutions.
Hammett
Acidity
Function
H
0
90
References
92
Problems
95
5
Chemical
Standards
97
5-
1
History
97
5-2
Operational
Standards:
Silver
and
the
Coulomb
99
5-3
Pure
Materials
101
5-
4
Standard
Samples
103
References
104
Problems
105
6
Applications
of
Acid-Base
Titrations
107
6-
1
Preparation
of
Standard
Acid
108
6-2
Preparation
of
Standard
Base
108
6-3
Standardization
of
Acids
and
Bases
109
CONTENTS
IX
6-4
Applications
of
Aqueous
Acid-Base
Titrations
112
6
-
5
Applications
of
Nonaqueous
Acid-Base
Titrations
115
References
121
Problems
124
7
Solubility
of
Precipitates
125
7
-
1
Solubility,
Intrinsic
Solubility,
and
Solubility
Product
126
7-2
Solubility
of
a
Precipitate
in
Pure
Solution
or
With
a
Common
Ion
128
7-3
Effect
of
Hydrogen
Ion
Concentration
129
7-4
Effect
of
Hydrolysis
of
the
Anion
in
Unbuffered
Solution
129
7-5
Effect
of
Hydrolysis
of
the
Cation
130
7-6
Effect
of
Foreign
Complexing
Agents
132
7-7
Effect
of
Complex
Formation
with
Precipitating
Anion
133
7-8
Solubility
of
Metastable
Forms
of
Precipitates
137
7-9
Solubility
and
Particle
Size
137
7
-
10
The
Diverse
Ion
Effect
139
References
139
Problems
140
8
Formation
and
Properties
of
Precipitates
142
8
-
1
Nucléation
142
8-2
The
Mechanism
of
Nucléation
146
8-3
Crystal
Growth
150
8-4
Aging
153
8-5
Physical
Properties
of
Colloids
157
8
-
6
The
Electrical
Double
Layer
and
Colloid
Stability
159
References
162
9
Contamination
of
Precipitates
166
9
-
1
Adsorption
167
9-2
Contamination
by
Adsorption
169
9-3
Occlusion
by
Adsorption
171
9-4
Occlusion
by
Solid-Solution
Formation
171
References
176
Problems
177
10
Practical
Aspects
of
Precipitation
Reactions
178
10-1
Gravimetric
Methods
178
10-2
Precipitation
from
Homogeneous
Solution
179
10-3
Ignition
of
Precipitates
181
X
CONTENTS
10
-
4
Titration
Methods
185
References
186
Problems
188
11
Complexation
Equilibria:
Theory
and
Applications
189
11
-
1
Definitions
and
General
Background
190
11-2
Ethylenediaminetetracetic
Acid
(EDTA)
191
11-3
EDTA
Titration
Curves
197
11-4
Titration
Error
199
11-5
Metal
Ion
Indicators
200
11-6
End-Point
Detection
by
the
Mercury-EDTA
Electrode
203
11-7
Applications
of
EDTA
Titrations
207
11-8
Masking
209
11
-
9
Other
Chelating
Reagents
211
References
212
Problems
214
12
Electrode
Potentials
217
12
-
1
General
Background
217
12-2
Electromotive
Force
of
a
Cell
and
Potential
of
a
Half-Cell
218
12-3
The
Nernst
Equation
221
12-4
Combination
of
Half-Reactions
to
form
New
Half-Reactions
223
12-5
Combination
of
Half-Reactions
to
form
a
Whole
Reaction
224
12-6
Equilibrium
Constant
of
a
Redox
Chemical
Reaction
226
12-7
Effect
of
Complex
Formation
on
Electrode
Potentials
227
12-8
Dependence
of
Potential
on
pH
231
12
-
9
Reversibility
of
Electrode
Reactions
233
References
237
Problems
237
13
Membrane
Potentials
and
Ion-Selective
Electrodes
239
13
-
1
Membranes
Permeable
to
a
Single
Species
240
13-2
The
Glass
Electrode
241
13-3
Liquid
Membranes
244
13-4
Other
Solid-State
Membranes
247
13-5
Enzyme
Electrodes
248
13-6
Miscellaneous
Ion-Selective
Electrodes
248
13-7
Reference
and
Standard
Solutions
249
CONTENTS
XÎ
13
-
8
Applications
of
Ion-Selective
Electrodes
253
References
254
Problems
256
14
Electrolytic
Separations
and
Determinations
257
14
-
1
Definitions
257
14-2
Basic
Principles
258
14-3
Concentration
Overpotential
259
14-4
Activation
Overpotential
262
14-5
Effects
of
Complexation
and
Addition
Agents
269
14-6
Separation
at
Constant
Current
270
14-7
Examples
of
Determinations
by
Electrodeposition
at
Constant
Current
271
14-8
Separations
by
Electrodeposition
at
Controlled
Potential
273
14-9
Examples
of
Analysis
by
Controlled-Potential
Electrolysis
275
14
-
10
Titrations
with
Coulometrically
Generated
Reagents
277
References
278
Problems
280
15
Oxidation-Reduction
Reactions
282
15
-
1
Titration
Curves
283
15-2
Theoretical
Properties
of
Redox
Titration
Curves
285
15-3
Experimental
Titration
Curves
286
15-4
Theory
of
Redox
Indicators
290
15-5
Examples
of
Redox
Indicators
291
15-6
Redox
Reactions
in
Nonaqueous
Solvents
293
15-7
Catalyzed
Reactions
295
15
-
8
Induced
Reactions
297
References
303
Problems
305
16
Prior
Oxidation
and
Reduction
307
16
-
1
Oxidizing
Agents
308
16-2
Reducing
Agents
312
16-3
Oxidation
of
Organic
Matter
317
16-4
Redox
Resins
319
References
320
Problems
323
xil
CONTENTS
17
Permanganate
and
Dichromate
as
Oxidants
324
17-1
Half-Reactions
324
17-2
The
Permanganate-Oxalate
Reaction
326
17-3
The
Iron(II)-Dichromate
Reaction
328
17-4
Applications
of
Permanganate
329
17
-
5
Applications
of
Dichromate
333
References
334
Problems
335
18
Cerium(IV)
337
18
-
1
Half-Reactions
and
Electrode
Potentials
337
18-2
The
Cerium(IV)-Oxalate
Reaction
340
18-3
The
Cerium(IV)-Hydrogen
Peroxide
Reaction
342
18-4
Other
Cerium(IV)
Reactions
342
18-5
Standard
Cerium(IV)
Solutions
344
18
-
6
Applications
of
Cerium(IV)
Oxidations
345
References
348
19
Iodine
351
19
-
1
Electrode
Potential
351
19-2
Standard
Solutions
and
Primary
Standards
353
19-3
Starch
as
an
Indicator
354
19-4
The
Iodine-Thiosulfate
Reaction
355
19-5
The
Iodine-Arsenic(III)
Reaction
357
19-6
Determination
of
Copper
358
19-7
Oxygen:
Winkler
Method
360
19-8
Water:
Karl
Fischer
Method
361
19-9
Amplification
Reactions
363
19
-
10
Other
Methods
364
References
365
20
Other
Oxidants
and
Reductants
368
20
-
1
Potassium
Iodate
368
20-2
Potassium
Bromate
370
20-3
Periodate
371
20-4
Other
Oxyhalogens
373
20-5
Other
Oxidants
374
20-6
Titanium(III)
375
CONTENTS
XÎii
20-7
Chromium(II)
376
20
-
8
Other
Reductants
377
References
378
Problems
381
21
Reaction
Rates
in
Chemical
Analysis
382
21
-
1
Rates
of
Reactions
383
21-2
Single-Component
Analysis
386
21-3
Mixtures
:
Simultaneous
Analysis
389
21-4
Precision
of
Measurements
393
21
-
5
Applications
396
References
402
Problems
404
22
Separations:
Introduction
407
22
-
1
Recovery
and
Enrichment
Factors
408
22-2
Precipitation
409
22-3
Organic
Reagents
412
22-4
Selected
Examples
of
Organic
Reagents
in
Precipitation
415
22
-
5
Distillation
and
Volatilization
417
References
423
Problems
425
23
Liquid-Liquid
Extractions
and
Separations
426
23
-
1
Distribution
Constant
and
Distribution
Ratio
427
23-2
Batch
Liquid-Liquid
Extractions
429
23-3
Countercurrent
Liquid-Liquid
Extraction
432
23-4
Continuous
Liquid-Liquid
Countercurrent
Extraction
440
23-5
Distribution
Ratios
for
Complexes
443
23
-
6
Selected
Applications
of
Extractions
453
References
458
Problems
461
24
Chromatography
463
24
-
1
Some
Chromatographic
Terms
464
24-2
Band
Broadening
and
the
Theoretical
Plate
466
24-3
Temperature
and
Band
Broadening
474
24-4
Sample-Injection
Effects
480
xiv
CONTENTS
24-5
Other
Factors
and
Peak
Broadening
483
24-6
Resolution:
Its
Relation
to
Relative
Retention,
Partition
Ratio,
and
Plate
Number
485
24
-
7
Complex
Mixtures:
Gradient
Elution
and
Temperature
Programming
490
References
494
Problems
496
25
Applications
of
Chromatography
499
25
-
1
Ion
Exchange
500
25-2
Analytical
Applications
of
Ion
Exchange
503
25-3
Adsorption
Chromatography
506
25-4
Liquid-Liquid
Chromatography
510
25-5
Gel
and
Exclusion
Chromatography
512
25-6
Thin-Layer
and
Paper
Chromatography
514
25-7
Gas
Chromatography
517
25
-
8
Identification
and
Measurement
521
References
525
Problems
529
26
Statistics
531
26
-
1
Methods
of
Data
Reduction
532
26-2
Errors
in
Quantitative
Analysis
534
26-3
The
Gaussian
Distribution
534
26-4
Gaussian
Distribution
Applied
to
a
Finite
Sample
536
26-5
Measures
of
Central
Value
and
Dispersion
537
26-6
Error
of
a
Computed
Result
538
26-7
Standard
Error
of
the
Mean
539
26-8
Measure
of
Precision
of
a
Mean
and
of
a
Standard
Deviation:
Confidence
Intervals
540
26-9
Combination
of
Observations
542
26-10
Tests
of
Significance
542
26-11
Analysis
of
Variance
548
26-12
Control
Charts
551
26-13
Regression
Analysis
553
26-14
Statistical
Design
of
Experiments
557
26-15
Rejection
of
Observations
560
References
561
Problems
562
XV
CONTENTS
27
Sampling
565
27-1
Statistical
Criteria
of
Valid
Sampling
566
27-2
Sampling
Units
567
27-3
Estimation
of
Required
Sample
Size
of
Particulate
Material
569
27-4
Stratified
Sampling
Opposed
to
Completely
Random
Sampling
574
27-5
Minimization
of
Cost
or
Variance
in
Stratified
Sampling
576
27-6
Sampling
Procedures
578
References
581
Problems
582
Index
583
|
| any_adam_object | 1 |
| author | Laitinen, Herbert A. Harris, Walter A. |
| author_facet | Laitinen, Herbert A. Harris, Walter A. |
| author_role | aut aut |
| author_sort | Laitinen, Herbert A. |
| author_variant | h a l ha hal w a h wa wah |
| building | Verbundindex |
| bvnumber | BV009053700 |
| callnumber-first | Q - Science |
| callnumber-label | QD101 |
| callnumber-raw | QD101.2 |
| callnumber-search | QD101.2 |
| callnumber-sort | QD 3101.2 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 5010 |
| ctrlnum | (OCoLC)1262846 (DE-599)BVBBV009053700 |
| dewey-full | 545 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 545 - [Unassigned] |
| dewey-raw | 545 |
| dewey-search | 545 |
| dewey-sort | 3545 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 2. ed. |
| format | Book |
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| id | DE-604.BV009053700 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T17:29:19Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-005993094 |
| oclc_num | 1262846 |
| open_access_boolean | |
| owner | DE-20 DE-706 DE-11 DE-188 |
| owner_facet | DE-20 DE-706 DE-11 DE-188 |
| physical | XIX, 611 S. |
| publishDate | 1975 |
| publishDateSearch | 1975 |
| publishDateSort | 1975 |
| publisher | McGraw-Hill |
| record_format | marc |
| spelling | Laitinen, Herbert A. Verfasser aut Chemical analysis An advanced text and reference Herbert A. Laitinen ; Walter A. Harris* 2. ed. Düsseldorf McGraw-Hill 1975 XIX, 611 S. txt rdacontent n rdamedia nc rdacarrier McGraw-Hill series in advanced chemistry Analyse quantitative (Chimie) Chemistry Techniques, Analytical Chemistry, Analytic Quantitative Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s DE-604 Harris, Walter A. Verfasser aut HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005993094&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Laitinen, Herbert A. Harris, Walter A. Chemical analysis An advanced text and reference Analyse quantitative (Chimie) Chemistry Techniques, Analytical Chemistry, Analytic Quantitative Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4129906-1 |
| title | Chemical analysis An advanced text and reference |
| title_auth | Chemical analysis An advanced text and reference |
| title_exact_search | Chemical analysis An advanced text and reference |
| title_full | Chemical analysis An advanced text and reference Herbert A. Laitinen ; Walter A. Harris* |
| title_fullStr | Chemical analysis An advanced text and reference Herbert A. Laitinen ; Walter A. Harris* |
| title_full_unstemmed | Chemical analysis An advanced text and reference Herbert A. Laitinen ; Walter A. Harris* |
| title_short | Chemical analysis |
| title_sort | chemical analysis an advanced text and reference |
| title_sub | An advanced text and reference |
| topic | Analyse quantitative (Chimie) Chemistry Techniques, Analytical Chemistry, Analytic Quantitative Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Analyse quantitative (Chimie) Chemistry Techniques, Analytical Chemistry, Analytic Quantitative Analytische Chemie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005993094&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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