Fundamental principles of chemical analysis:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Amsterdam [u.a.]
Elsevier
1966
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | IX, 270 S. |
Internformat
MARC
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Datensatz im Suchindex
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|---|---|
| adam_text | FUNDAMENTAL PRINCIPLES
OF
CHEMICAL ANALYSIS
BY
WILLIAM F PICKERING
Department of Chemistry, University of Newcastle,
Australia
ELSEVIERPUBLISHINGCOMPANY
AMSTERDAM - LONDON - NEW YORK
Contents
PREFACE v
Chapter 1 INTRODUCTION 1
Chapter 2 DETERMINATIONS BASED ON PHASE SEPA
RATIONS 7
2 1 Introduction 7
2 2 Solid-liquid separations 8
2 3 Gas-solid separations 23
2 4 Liquid-liquid separations 26
2 5 Gas-liquid separations 29
Chapter 3 ELECTRICAL TRANSFORMATIONS 32
3 1 Standard reduction potentials 32
3 2 Oxidation-reduction titrations 36
3 3 Electroanalytical techniques 36
3 4 Potentiometric titrations 40
3 5 Electrodeposition 43
3 6 Coulometric analysis 51
3 7 Polarography 53
3 8 Conductimetric titrations 59
3 9 Special techniques 61
Chapter 4 IONIC EQUIL1BRIA IN SOLUTION 65
4 1 Titrimetric analysis 65
4 2 Titration curves 66
4 3 Chemical equilibria calculations 68
4 4 Indicators 77
4 5 Solvent effects 81
4 6 Limitations of titrimetric techniques 82
Chapter 5 ENERGY TRANSITIONS 85
5 1 Introduction 85
VIIICONTENTS
52 Electromagnetic radiation 86
5 3 The emission and absorption of electromagnetic
radiation 88
5 4 Emission spectroscopy involving visible and
ultraviolet radiations 93
5 5 X-Ray emission spectroscopy 100
5 6 Absorption spectroscopy 106
5 7 Absorption of X-rays 110
5 8 Absorption of ultraviolet and visible radiation 112
5 9 Absorption of infrared radiation 115
5 10 Atomic absorption spectroscopy 117
5 11 Radioactive decay 119
Chapter 6 PHYSICAL PROPERTIES OF MATTER 142
6 1 Introduction 124
6 2 The determination of mass 124
6 3 Mass spectrometry 127
6 4 Differential thermal analysis 131
6 5 Thermal conductivity of gases 133
6 6 Ionisation of gases 136
6 7 Refractivity and dispersion 137 ^
6 8 Polarimetry 139
Chapter 7 STATISTICS, SAMPLING AND SOLUTION OF
SAMPLES 124
7 1 Statistics 142
7 2 Sampling 146
7 3 Solution of samples 152
Chapter 8 SELECTIVE CHEMICAL REACTIONS 157
8 1 Interference effects 157
8 2 Separations based on selective precipitation 158
8 3 Complex formation and masking 162
8 4 Pre-oxidation and reduction procedures 169
8 5 Volatilisation procedures 176
Chapter 9 HETEROGENEOUS EQUILIBRIUM REACTIONS 178
9 1 Introduction 178
9 2 Ion exchange 181
9 3 Solvent extraction 189
CONTENTSIX
j Chapter 10 CHROMATOGRAPHIC SEPARATIONS 204
| 10 1 Introduction 204
10 2 Chromatographic development 206
| 10 3 Distribution equilibria 209
10 4 Factors influencing zone sharpness 212
10 5 Chromatographic techniques 216
10 6 The role of chromatography 225
Chapter 11 SELECTION OF ANALYTICAL METHODS 228
11 1 Introduction 228
11 2 Summary of available methods 229
11 3 Selection of methods 230
11 4 Development of a new analytical method 232
11 5 Equilibrium studies 236
11 6 Kinetic studies 241
11 7 Project planning 244
Chapter 12 TUTORIAL PROBLEMS 247
Appendix RECENT PUBL1 CATIONS-ANALYTICAL CHEM
ISTRY 257
INDEX 260
|
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| spelling | Pickering, William F. Verfasser aut Fundamental principles of chemical analysis Amsterdam [u.a.] Elsevier 1966 IX, 270 S. txt rdacontent n rdamedia nc rdacarrier Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005988478&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
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| title | Fundamental principles of chemical analysis |
| title_auth | Fundamental principles of chemical analysis |
| title_exact_search | Fundamental principles of chemical analysis |
| title_full | Fundamental principles of chemical analysis |
| title_fullStr | Fundamental principles of chemical analysis |
| title_full_unstemmed | Fundamental principles of chemical analysis |
| title_short | Fundamental principles of chemical analysis |
| title_sort | fundamental principles of chemical analysis |
| topic | Chemistry, Analytic Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Chemistry, Analytic Analytische Chemie |
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