Holdings: Polarographic techniques

Polarographic techniques:

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Bibliographic Details
Main Author:	Meites, Louis (Author)
Format:	Book
Language:	English
Published:	New York [u.a.] Interscience Publ. 1965
Edition:	2. ed.
Subjects:	Polarography Elektrochemie Technologie Chemisches Element Elektrochemisches Verfahren Amperometrische Titration Polarographie
Online Access:	Inhaltsverzeichnis
Physical Description:	XVII, 752 S. Ill., graph. Darst.

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MARC


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Record in the Search Index

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adam_text	CONTENTS 1. The Nature and Applications of Polarography..... 1 2. Polarographs and Other Apparatus.......... 7 I. Polarographic Circuits............ 7 II. Commercially Available Polarographs..... 35 III. Polarographic Cells............. 57 IV. Dropping Electrodes ............ 73 V. Auxiliary Equipment and Laboratory Design . . 83 References.................... 92 3. The Limiting Current............... 95 I. The Residual Current............ 96 II. The Migration Current........... 105 III. Theory of the Diffusion Current....... Ill IV. Factors Affecting the Diffusion Current .... 125 A. The Concentration of the Electroactive Sub- stance ................ 125 B. The Capillary Characteristics and the Factors Affecting Them............ 131 C. Temperature.............. 138 D. The Solvent and Supporting Electrolyte . . 141 E. Polarographic Diffusion Coefficients .... 144 V. Techniques for Measuring Wave Heights .... 150 VI. Estimation of n-Values from Diffusion-Current Data.................. 165 VII. Kinetic Currents.............. 176 VIII. Catalytic Currents............. 182 IX. Adsorption Waves ............. 187 xiii iv CONTENTS X. Non-Additive Currents........... 189 XI. Capacity Waves and Related Phenomena . . . 196 References.................... 198 4. Theory of the Current-Potential Curve........ 203 I. Reversible Processes Involving Simple or Complex Metal Ions and Metals Soluble in Mercury . . 204 II. Reversible Processes Involving a Solid Insoluble in Mercury................. 211 III. Reversible Processes Involving Only Dissolved Species................. 214 IV. Criteria of Reversibility........... 217 V. Irreversible Processes............ 232 VI. Quasireversible Processes........... 253 VII. The Structure of the Double Layer and Its Effects on Kinetic Parameters........... 254 References.................... 264 5. Interpretation of Half-Wave Potentials........ 267 I. Half-Wave Potentials for Reversible Reductions of Simple and Complex Metal Ions to Metals Soluble in Mercury............ 267 II. Half-Wave Potentials for Reversible Processes In- volving Only Dissolved Species....... 278 III. Half-Wave Potentials for Irreversible Processes. Correlations between Half-Wave Potential and Structure................ 284 IV. Summary of Factors Affecting the Half-Wave Potential ................ 288 V. Qualitative Polarographic Analysis...... 293 References.................... 300 6. Maxima and Maximum Suppressors......... 303 I. The Characteristics and Practical Significance of Maxima................. 304 II. The Interpretation of Maxima........ 312 CONTENTS XV III. Maximum Suppressors............ 319 IV. The Effects of Maximum Suppressors..... 323 V. Analytical Applications of Maxima and Maximum Suppressors............... 329 References.................... 331 7. Quantitative Polarographic Analysis......... 333 I. Selection of Conditions for Measuring the Wave Height ................. 334 A. Selection of the Solvent......... 334 B. Selection of the Supporting Electrolyte . . . 341 i. The Problem of Wave Separation ... 341 ii. The Problem of Wave Order..... 348 iii. The Examination of a New Compound . 354 II. Indirect Methods of Analysis ........ 357 III. Separations Preceding Polarographic Analyses . . 363 A. Precipitation.............. 365 B. Extraction............... 366 C. Chromatographic and Related Techniques . 367 D. Other Physical Techniques........ 370 E. Chemical Reduction........... 370 F. Electrolytic Techniques......... 371 IV. Techniques of Practical Analysis....... 376 A. Problems of Polarographic Trace Analysis . 376 B. Special Techniques for Handling Unstable Solutions............... 382 i. Solutions of Strong Reducing Agents . . 382 ii. Solutions of Strong Oxidizing Agents . . 385 iii. Solutions That React with the Salt Bridge.............. 388 V. The Interpretation of the Wave Height .... 391 A. The Absolute Method......... 391 B. Comparative Methods.......... 394 i. The Standard Curve Method..... 395 ii. The Standard Sample Method .... 397 iii. Standard Addition Methods..... 398 Xvi CONTENTS iv. The Pilot-Ion Method........ 404 v. Kinetic Methods.......... 406 References.................... 408 8. Other Voltammetric Indicator Electrodes....... 411 I. Electrode Configurations........... 412 II. Noble-Metal Electrodes........... 428 III. Other Solid Electrodes............ 439 IV. Mercury Electrodes............. 445 References.................... 461 9. Amperometric Titrations.............. 465 I. Amperometric Precipitation Titrations. Theory of Amperometric Titration Curves....... 465 II. Other Kinds of Amperometric Titrations .... 486 A. Redox Titrations............ 486 B. Complexometric and Chelometric Titrations 491 C. Compensation and Diffusion-Layer Titrations 495 III. Apparatus and Techniques.......... 498 IV. Amperometric Titrations with Two Polarized Electrodes................ 502 References.................... 507 10. Related Techniques................ 511 I. Controlled-Potential Electrolysis....... 511 II. Coulometry at Controlled Potential...... 523 III. Coulometry at Voltammetric Indicator Electrodes 532 IV. Other Voltammetric Current-Time Curves . _. . 536 V. Stripping Analysis ............. 538 VI. Coulometric Titrations ........... 546 VII. Chronopotentiometry............ 556 VIII. Differential and Derivative Voltammetry ... 571 IX. Cyclic and Pulse Techniques......... 577 References.................... 593 CONTENTS XV11 Appendix A. Trouble-Shooting in Polarographic Circuits . 601 Appendix B. Polarographic Characteristics of Inorganic Sub- stances ................ 615 Appendix C. Polarographic Characteristics of Organic Sub- stances ................ 671 Author Index..................... 713 Subject Index..................... 727
any_adam_object	1
author	Meites, Louis
author_facet	Meites, Louis
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author_sort	Meites, Louis
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dewey-full	544.9
dewey-hundreds	500 - Natural sciences and mathematics
dewey-ones	544 - [Unassigned]
dewey-raw	544.9
dewey-search	544.9
dewey-sort	3544.9
dewey-tens	540 - Chemistry and allied sciences
discipline	Chemie / Pharmazie
edition	2. ed.
format	Book
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publisher	Interscience Publ.
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spelling	Meites, Louis Verfasser aut Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff 2. ed. New York [u.a.] Interscience Publ. 1965 XVII, 752 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polarography Elektrochemie (DE-588)4014241-3 gnd rswk-swf Technologie (DE-588)4059276-5 gnd rswk-swf Chemisches Element (DE-588)4009874-6 gnd rswk-swf Elektrochemisches Verfahren (DE-588)4151772-6 gnd rswk-swf Amperometrische Titration (DE-588)4142271-5 gnd rswk-swf Polarographie (DE-588)4174994-7 gnd rswk-swf Polarographie (DE-588)4174994-7 s DE-604 Amperometrische Titration (DE-588)4142271-5 s 1\p DE-604 Elektrochemisches Verfahren (DE-588)4151772-6 s 2\p DE-604 Chemisches Element (DE-588)4009874-6 s 3\p DE-604 Technologie (DE-588)4059276-5 s 4\p DE-604 Elektrochemie (DE-588)4014241-3 s 5\p DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005986899&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 5\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk
spellingShingle	Meites, Louis Polarographic techniques Polarography Elektrochemie (DE-588)4014241-3 gnd Technologie (DE-588)4059276-5 gnd Chemisches Element (DE-588)4009874-6 gnd Elektrochemisches Verfahren (DE-588)4151772-6 gnd Amperometrische Titration (DE-588)4142271-5 gnd Polarographie (DE-588)4174994-7 gnd
subject_GND	(DE-588)4014241-3 (DE-588)4059276-5 (DE-588)4009874-6 (DE-588)4151772-6 (DE-588)4142271-5 (DE-588)4174994-7
title	Polarographic techniques
title_auth	Polarographic techniques
title_exact_search	Polarographic techniques
title_full	Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff
title_fullStr	Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff
title_full_unstemmed	Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff
title_short	Polarographic techniques
title_sort	polarographic techniques
topic	Polarography Elektrochemie (DE-588)4014241-3 gnd Technologie (DE-588)4059276-5 gnd Chemisches Element (DE-588)4009874-6 gnd Elektrochemisches Verfahren (DE-588)4151772-6 gnd Amperometrische Titration (DE-588)4142271-5 gnd Polarographie (DE-588)4174994-7 gnd
topic_facet	Polarography Elektrochemie Technologie Chemisches Element Elektrochemisches Verfahren Amperometrische Titration Polarographie
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005986899&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT meiteslouis polarographictechniques

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