Polarographic techniques:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
Interscience Publ.
1965
|
| Ausgabe: | 2. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVII, 752 S. Ill., graph. Darst. |
Internformat
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| 100 | 1 | |a Meites, Louis |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Polarographic techniques |c Louis Meites. With a foreword by I. M. Kolthoff |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a New York [u.a.] |b Interscience Publ. |c 1965 | |
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Datensatz im Suchindex
| _version_ | 1804123401710731264 |
|---|---|
| adam_text | CONTENTS
1. The Nature and Applications of Polarography..... 1
2. Polarographs and Other Apparatus.......... 7
I. Polarographic Circuits............ 7
II. Commercially Available Polarographs..... 35
III. Polarographic Cells............. 57
IV. Dropping Electrodes ............ 73
V. Auxiliary Equipment and Laboratory Design . . 83
References.................... 92
3. The Limiting Current............... 95
I. The Residual Current............ 96
II. The Migration Current........... 105
III. Theory of the Diffusion Current....... Ill
IV. Factors Affecting the Diffusion Current .... 125
A. The Concentration of the Electroactive Sub-
stance ................ 125
B. The Capillary Characteristics and the Factors
Affecting Them............ 131
C. Temperature.............. 138
D. The Solvent and Supporting Electrolyte . . 141
E. Polarographic Diffusion Coefficients .... 144
V. Techniques for Measuring Wave Heights .... 150
VI. Estimation of n-Values from Diffusion-Current
Data.................. 165
VII. Kinetic Currents.............. 176
VIII. Catalytic Currents............. 182
IX. Adsorption Waves ............. 187
xiii
iv CONTENTS
X. Non-Additive Currents........... 189
XI. Capacity Waves and Related Phenomena . . . 196
References.................... 198
4. Theory of the Current-Potential Curve........ 203
I. Reversible Processes Involving Simple or Complex
Metal Ions and Metals Soluble in Mercury . . 204
II. Reversible Processes Involving a Solid Insoluble in
Mercury................. 211
III. Reversible Processes Involving Only Dissolved
Species................. 214
IV. Criteria of Reversibility........... 217
V. Irreversible Processes............ 232
VI. Quasireversible Processes........... 253
VII. The Structure of the Double Layer and Its Effects
on Kinetic Parameters........... 254
References.................... 264
5. Interpretation of Half-Wave Potentials........ 267
I. Half-Wave Potentials for Reversible Reductions
of Simple and Complex Metal Ions to Metals
Soluble in Mercury............ 267
II. Half-Wave Potentials for Reversible Processes In-
volving Only Dissolved Species....... 278
III. Half-Wave Potentials for Irreversible Processes.
Correlations between Half-Wave Potential and
Structure................ 284
IV. Summary of Factors Affecting the Half-Wave
Potential ................ 288
V. Qualitative Polarographic Analysis...... 293
References.................... 300
6. Maxima and Maximum Suppressors......... 303
I. The Characteristics and Practical Significance of
Maxima................. 304
II. The Interpretation of Maxima........ 312
CONTENTS XV
III. Maximum Suppressors............ 319
IV. The Effects of Maximum Suppressors..... 323
V. Analytical Applications of Maxima and Maximum
Suppressors............... 329
References.................... 331
7. Quantitative Polarographic Analysis......... 333
I. Selection of Conditions for Measuring the Wave
Height ................. 334
A. Selection of the Solvent......... 334
B. Selection of the Supporting Electrolyte . . . 341
i. The Problem of Wave Separation ... 341
ii. The Problem of Wave Order..... 348
iii. The Examination of a New Compound . 354
II. Indirect Methods of Analysis ........ 357
III. Separations Preceding Polarographic Analyses . . 363
A. Precipitation.............. 365
B. Extraction............... 366
C. Chromatographic and Related Techniques . 367
D. Other Physical Techniques........ 370
E. Chemical Reduction........... 370
F. Electrolytic Techniques......... 371
IV. Techniques of Practical Analysis....... 376
A. Problems of Polarographic Trace Analysis . 376
B. Special Techniques for Handling Unstable
Solutions............... 382
i. Solutions of Strong Reducing Agents . . 382
ii. Solutions of Strong Oxidizing Agents . . 385
iii. Solutions That React with the Salt
Bridge.............. 388
V. The Interpretation of the Wave Height .... 391
A. The Absolute Method......... 391
B. Comparative Methods.......... 394
i. The Standard Curve Method..... 395
ii. The Standard Sample Method .... 397
iii. Standard Addition Methods..... 398
Xvi CONTENTS
iv. The Pilot-Ion Method........ 404
v. Kinetic Methods.......... 406
References.................... 408
8. Other Voltammetric Indicator Electrodes....... 411
I. Electrode Configurations........... 412
II. Noble-Metal Electrodes........... 428
III. Other Solid Electrodes............ 439
IV. Mercury Electrodes............. 445
References.................... 461
9. Amperometric Titrations.............. 465
I. Amperometric Precipitation Titrations. Theory of
Amperometric Titration Curves....... 465
II. Other Kinds of Amperometric Titrations .... 486
A. Redox Titrations............ 486
B. Complexometric and Chelometric Titrations 491
C. Compensation and Diffusion-Layer Titrations 495
III. Apparatus and Techniques.......... 498
IV. Amperometric Titrations with Two Polarized
Electrodes................ 502
References.................... 507
10. Related Techniques................ 511
I. Controlled-Potential Electrolysis....... 511
II. Coulometry at Controlled Potential...... 523
III. Coulometry at Voltammetric Indicator Electrodes 532
IV. Other Voltammetric Current-Time Curves . _. . 536
V. Stripping Analysis ............. 538
VI. Coulometric Titrations ........... 546
VII. Chronopotentiometry............ 556
VIII. Differential and Derivative Voltammetry ... 571
IX. Cyclic and Pulse Techniques......... 577
References.................... 593
CONTENTS XV11
Appendix A. Trouble-Shooting in Polarographic Circuits . 601
Appendix B. Polarographic Characteristics of Inorganic Sub-
stances ................ 615
Appendix C. Polarographic Characteristics of Organic Sub-
stances ................ 671
Author Index..................... 713
Subject Index..................... 727
|
| any_adam_object | 1 |
| author | Meites, Louis |
| author_facet | Meites, Louis |
| author_role | aut |
| author_sort | Meites, Louis |
| author_variant | l m lm |
| building | Verbundindex |
| bvnumber | BV009046409 |
| classification_rvk | VG 8130 |
| ctrlnum | (OCoLC)573148 (DE-599)BVBBV009046409 |
| dewey-full | 544.9 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 544 - [Unassigned] |
| dewey-raw | 544.9 |
| dewey-search | 544.9 |
| dewey-sort | 3544.9 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 2. ed. |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-09T17:29:11Z |
| institution | BVB |
| language | English |
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| physical | XVII, 752 S. Ill., graph. Darst. |
| psigel | TUB-nveb |
| publishDate | 1965 |
| publishDateSearch | 1965 |
| publishDateSort | 1965 |
| publisher | Interscience Publ. |
| record_format | marc |
| spelling | Meites, Louis Verfasser aut Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff 2. ed. New York [u.a.] Interscience Publ. 1965 XVII, 752 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polarography Elektrochemie (DE-588)4014241-3 gnd rswk-swf Technologie (DE-588)4059276-5 gnd rswk-swf Chemisches Element (DE-588)4009874-6 gnd rswk-swf Elektrochemisches Verfahren (DE-588)4151772-6 gnd rswk-swf Amperometrische Titration (DE-588)4142271-5 gnd rswk-swf Polarographie (DE-588)4174994-7 gnd rswk-swf Polarographie (DE-588)4174994-7 s DE-604 Amperometrische Titration (DE-588)4142271-5 s 1\p DE-604 Elektrochemisches Verfahren (DE-588)4151772-6 s 2\p DE-604 Chemisches Element (DE-588)4009874-6 s 3\p DE-604 Technologie (DE-588)4059276-5 s 4\p DE-604 Elektrochemie (DE-588)4014241-3 s 5\p DE-604 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005986899&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 5\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Meites, Louis Polarographic techniques Polarography Elektrochemie (DE-588)4014241-3 gnd Technologie (DE-588)4059276-5 gnd Chemisches Element (DE-588)4009874-6 gnd Elektrochemisches Verfahren (DE-588)4151772-6 gnd Amperometrische Titration (DE-588)4142271-5 gnd Polarographie (DE-588)4174994-7 gnd |
| subject_GND | (DE-588)4014241-3 (DE-588)4059276-5 (DE-588)4009874-6 (DE-588)4151772-6 (DE-588)4142271-5 (DE-588)4174994-7 |
| title | Polarographic techniques |
| title_auth | Polarographic techniques |
| title_exact_search | Polarographic techniques |
| title_full | Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff |
| title_fullStr | Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff |
| title_full_unstemmed | Polarographic techniques Louis Meites. With a foreword by I. M. Kolthoff |
| title_short | Polarographic techniques |
| title_sort | polarographic techniques |
| topic | Polarography Elektrochemie (DE-588)4014241-3 gnd Technologie (DE-588)4059276-5 gnd Chemisches Element (DE-588)4009874-6 gnd Elektrochemisches Verfahren (DE-588)4151772-6 gnd Amperometrische Titration (DE-588)4142271-5 gnd Polarographie (DE-588)4174994-7 gnd |
| topic_facet | Polarography Elektrochemie Technologie Chemisches Element Elektrochemisches Verfahren Amperometrische Titration Polarographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005986899&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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